data_MR280 _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C29 H21 O P' _chemical_formula_weight 416.43 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0034 0.0017 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0114 0.0062 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1041 0.0961 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_H-M_alt 'P 21 21 21' _space_group_name_Hall 'P 2ac 2ab' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' _cell_length_a 8.31950(10) _cell_length_b 12.1199(2) _cell_length_c 42.2796(8) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 4263.12(12) _cell_formula_units_Z 8 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9556 _cell_measurement_theta_min 2.41 _cell_measurement_theta_max 25.70 _exptl_crystal_description 'block' _exptl_crystal_colour 'colourless' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.298 _exptl_crystal_F_000 1744 _exptl_transmission_factor_min 0.8923 _exptl_transmission_factor_max 0.9559 _exptl_crystal_size_max 0.440 _exptl_crystal_size_mid 0.210 _exptl_crystal_size_min 0.130 _exptl_absorpt_coefficient_mu 0.146 _shelx_estimated_absorpt_T_min 0.939 _shelx_estimated_absorpt_T_max 0.981 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'sealed tube' _diffrn_measurement_device_type 'D8 Venture, Bruker Photon CMOS Detector' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 21816 _diffrn_reflns_av_unetI/netI 0.0481 _diffrn_reflns_av_R_equivalents 0.0354 _diffrn_reflns_limit_h_min -6 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -47 _diffrn_reflns_limit_l_max 51 _diffrn_reflns_theta_min 2.216 _diffrn_reflns_theta_max 25.720 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 8076 _reflns_number_gt 7445 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.765 _reflns_Friedel_fraction_max 0.999 _reflns_Friedel_fraction_full 0.999 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Diamond 2.1e' _computing_publication_material 'Microsoft Word' _refine_special_details ; Refined as a 2-component inversion twin. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0298P)^2^+10.8142P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method 'SHELXL-2014/7 (Sheldrick 2014' _refine_ls_extinction_coef 0.0083(8) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.59(18) _chemical_absolute_configuration rm _refine_ls_number_reflns 8076 _refine_ls_number_parameters 543 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0685 _refine_ls_R_factor_gt 0.0631 _refine_ls_wR_factor_ref 0.1473 _refine_ls_wR_factor_gt 0.1444 _refine_ls_goodness_of_fit_ref 1.074 _refine_ls_restrained_S_all 1.074 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.1401(6) 0.4660(4) 0.63297(12) 0.0151(10) Uani 1 1 d . . . . . C2 C 0.1571(6) 0.3703(4) 0.61001(12) 0.0155(10) Uani 1 1 d . . . . . H2 H 0.2272 0.3077 0.6169 0.019 Uiso 1 1 calc R U . . . C3 C 0.1767(6) 0.4090(4) 0.57690(12) 0.0152(10) Uani 1 1 d . . . . . H3 H 0.1964 0.3585 0.5602 0.018 Uiso 1 1 calc R U . . . C4 C 0.1656(6) 0.5185(4) 0.57141(11) 0.0149(10) Uani 1 1 d . . . . . C5 C -0.1164(7) 0.5507(4) 0.60267(12) 0.0191(12) Uani 1 1 d . . . . . C6 C -0.1426(6) 0.4443(4) 0.61303(12) 0.0163(11) Uani 1 1 d . . . . . C7 C -0.0046(6) 0.3853(4) 0.62817(12) 0.0157(11) Uani 1 1 d . . . . . C8 C -0.0419(6) 0.3034(4) 0.65388(12) 0.0179(11) Uani 1 1 d . . . . . C9 C -0.1427(8) 0.3356(5) 0.67873(14) 0.0271(13) Uani 1 1 d . . . . . H9 H -0.1864 0.4080 0.6793 0.033 Uiso 1 1 calc R U . . . C10 C -0.1781(8) 0.2610(5) 0.70248(15) 0.0328(15) Uani 1 1 d . . . . . H10 H -0.2451 0.2829 0.7196 0.039 Uiso 1 1 calc R U . . . C11 C -0.1171(8) 0.1548(5) 0.70170(15) 0.0327(15) Uani 1 1 d . . . . . H11 H -0.1444 0.1037 0.7178 0.039 Uiso 1 1 calc R U . . . C12 C -0.0159(8) 0.1234(5) 0.67723(14) 0.0285(13) Uani 1 1 d . . . . . H12 H 0.0276 0.0510 0.6767 0.034 Uiso 1 1 calc R U . . . C13 C 0.0212(6) 0.1976(4) 0.65381(12) 0.0193(11) Uani 1 1 d . . . . . H13 H 0.0915 0.1760 0.6372 0.023 Uiso 1 1 calc R U . . . C14 C -0.2943(6) 0.3977(4) 0.60910(13) 0.0174(10) Uani 1 1 d . . . . . H14 H -0.3156 0.3248 0.6162 0.021 Uiso 1 1 calc R U . . . C15 C -0.4140(6) 0.4597(5) 0.59472(13) 0.0238(12) Uani 1 1 d . . . . . H15 H -0.5177 0.4282 0.5920 0.029 Uiso 1 1 calc R U . . . C16 C -0.3859(7) 0.5663(5) 0.58425(14) 0.0250(13) Uani 1 1 d . . . . . H16 H -0.4694 0.6074 0.5744 0.030 Uiso 1 1 calc R U . . . C17 C -0.2339(6) 0.6127(4) 0.58829(12) 0.0189(11) Uani 1 1 d . . . . . H17 H -0.2120 0.6857 0.5813 0.023 Uiso 1 1 calc R U . . . C18 C 0.2190(6) 0.4728(4) 0.66427(12) 0.0177(11) Uani 1 1 d . . . . . C19 C 0.3249(9) 0.3918(6) 0.67471(18) 0.0454(11) Uani 1 1 d . . . . . H19 H 0.3576 0.3344 0.6608 0.054 Uiso 1 1 calc R U . . . C20 C 0.3830(9) 0.3948(6) 0.70559(18) 0.0482(14) Uani 1 1 d . . . . . H20 H 0.4514 0.3375 0.7129 0.058 Uiso 1 1 calc R U . . . C21 C 0.3421(9) 0.4806(6) 0.72580(15) 0.0351(15) Uani 1 1 d . . . . . H21 H 0.3824 0.4828 0.7468 0.042 Uiso 1 1 calc R U . . . C22 C 0.2422(9) 0.5623(5) 0.71480(14) 0.0340(15) Uani 1 1 d . . . . . H22 H 0.2146 0.6218 0.7284 0.041 Uiso 1 1 calc R U . . . C23 C 0.1810(8) 0.5597(5) 0.68439(13) 0.0276(13) Uani 1 1 d . . . . . H23 H 0.1129 0.6175 0.6772 0.033 Uiso 1 1 calc R U . . . C24 C 0.1778(6) 0.5751(5) 0.54081(12) 0.0181(11) Uani 1 1 d . . . . . C25 C 0.1161(7) 0.6816(5) 0.53675(14) 0.0241(12) Uani 1 1 d . . . . . H25 H 0.0697 0.7193 0.5542 0.029 Uiso 1 1 calc R U . . . C26 C 0.1221(8) 0.7323(5) 0.50743(15) 0.0312(14) Uani 1 1 d . . . . . H26 H 0.0788 0.8043 0.5049 0.037 Uiso 1 1 calc R U . . . C27 C 0.1900(8) 0.6799(6) 0.48193(14) 0.0327(15) Uani 1 1 d . . . . . H27 H 0.1930 0.7153 0.4619 0.039 Uiso 1 1 calc R U . . . C28 C 0.2539(8) 0.5755(6) 0.48546(14) 0.0343(14) Uani 1 1 d . . . . . H28 H 0.3017 0.5392 0.4679 0.041 Uiso 1 1 calc R U . . . C29 C 0.2483(7) 0.5237(5) 0.51459(14) 0.0271(13) Uani 1 1 d . . . . . H29 H 0.2930 0.4520 0.5169 0.033 Uiso 1 1 calc R U . . . C30 C 0.4612(6) 0.9621(4) 0.63345(12) 0.0176(11) Uani 1 1 d . . . . . C31 C 0.4468(6) 0.8659(4) 0.61088(15) 0.0239(13) Uani 1 1 d . . . . . H31 H 0.3798 0.8021 0.6181 0.029 Uiso 1 1 calc R U . . . C32 C 0.4238(6) 0.9027(5) 0.57801(14) 0.0255(12) Uani 1 1 d . . . . . H32 H 0.4062 0.8509 0.5615 0.031 Uiso 1 1 calc R U . . . C33 C 0.4283(6) 1.0111(5) 0.57187(13) 0.0203(12) Uani 1 1 d . . . . . C34 C 0.7071(6) 1.0528(4) 0.60247(11) 0.0128(10) Uani 1 1 d . . . . . C35 C 0.7434(6) 0.9452(4) 0.61293(12) 0.0168(11) Uani 1 1 d . . . . . C36 C 0.6080(6) 0.8861(4) 0.62914(14) 0.0202(12) Uani 1 1 d . . . . . C37 C 0.6510(7) 0.8104(5) 0.65554(15) 0.0277(14) Uani 1 1 d . . . . . C38 C 0.7454(9) 0.8512(6) 0.67991(17) 0.0410(17) Uani 1 1 d . . . . . H38 H 0.7795 0.9260 0.6794 0.049 Uiso 1 1 calc R U . . . C39 C 0.7904(9) 0.7849(6) 0.70485(18) 0.0454(11) Uani 1 1 d . . . . . H39 H 0.8550 0.8125 0.7216 0.054 Uiso 1 1 calc R U . . . C40 C 0.7367(9) 0.6738(6) 0.70466(19) 0.0482(14) Uani 1 1 d . . . . . H40 H 0.7684 0.6261 0.7214 0.058 Uiso 1 1 calc R U . . . C41 C 0.6431(9) 0.6344(6) 0.68169(18) 0.0454(11) Uani 1 1 d . . . . . H41 H 0.6071 0.5600 0.6824 0.054 Uiso 1 1 calc R U . . . C42 C 0.5991(9) 0.7013(5) 0.65705(18) 0.0422(18) Uani 1 1 d . . . . . H42 H 0.5321 0.6729 0.6408 0.051 Uiso 1 1 calc R U . . . C43 C 0.8966(6) 0.9005(5) 0.60854(14) 0.0233(12) Uani 1 1 d . . . . . H43 H 0.9217 0.8288 0.6162 0.028 Uiso 1 1 calc R U . . . C44 C 1.0112(6) 0.9627(5) 0.59278(13) 0.0221(12) Uani 1 1 d . . . . . H44 H 1.1155 0.9329 0.5895 0.027 Uiso 1 1 calc R U . . . C45 C 0.9760(6) 1.0688(5) 0.58168(13) 0.0215(12) Uani 1 1 d . . . . . H45 H 1.0559 1.1099 0.5708 0.026 Uiso 1 1 calc R U . . . C46 C 0.8258(7) 1.1140(4) 0.58653(12) 0.0192(11) Uani 1 1 d . . . . . H46 H 0.8025 1.1862 0.5791 0.023 Uiso 1 1 calc R U . . . C47 C 0.3787(6) 0.9699(4) 0.66463(13) 0.0199(11) Uani 1 1 d . . . . . C48 C 0.2778(6) 0.8862(4) 0.67528(12) 0.0187(11) Uani 1 1 d . . . . . H48 H 0.2495 0.8274 0.6615 0.022 Uiso 1 1 calc R U . . . C49 C 0.2179(7) 0.8886(5) 0.70614(13) 0.0256(13) Uani 1 1 d . . . . . H49 H 0.1504 0.8309 0.7135 0.031 Uiso 1 1 calc R U . . . C50 C 0.2570(9) 0.9746(5) 0.72569(14) 0.0341(15) Uani 1 1 d . . . . . H50 H 0.2182 0.9756 0.7468 0.041 Uiso 1 1 calc R U . . . C51 C 0.3533(9) 1.0607(5) 0.71487(14) 0.0338(15) Uani 1 1 d . . . . . H51 H 0.3764 1.1214 0.7283 0.041 Uiso 1 1 calc R U . . . C52 C 0.4151(7) 1.0580(5) 0.68467(13) 0.0232(12) Uani 1 1 d . . . . . H52 H 0.4824 1.1161 0.6775 0.028 Uiso 1 1 calc R U . . . C53 C 0.4128(7) 1.0665(6) 0.54085(13) 0.0274(13) Uani 1 1 d . . . . . C54 C 0.4680(8) 1.1739(5) 0.53638(15) 0.0309(14) Uani 1 1 d . . . . . H54 H 0.5113 1.2137 0.5538 0.037 Uiso 1 1 calc R U . . . C55 C 0.4605(9) 1.2232(7) 0.50689(15) 0.0415(18) Uani 1 1 d . . . . . H55 H 0.5030 1.2953 0.5040 0.050 Uiso 1 1 calc R U . . . C56 C 0.3921(10) 1.1689(7) 0.48172(17) 0.050(2) Uani 1 1 d . . . . . H56 H 0.3849 1.2039 0.4617 0.060 Uiso 1 1 calc R U . . . C57 C 0.3336(9) 1.0628(8) 0.48576(16) 0.053(2) Uani 1 1 d . . . . . H57 H 0.2873 1.0249 0.4683 0.063 Uiso 1 1 calc R U . . . C58 C 0.3422(8) 1.0108(6) 0.51524(16) 0.0389(17) Uani 1 1 d . . . . . H58 H 0.3006 0.9384 0.5179 0.047 Uiso 1 1 calc R U . . . O1 O 0.1496(4) 0.6965(3) 0.61590(8) 0.0193(8) Uani 1 1 d . . . . . O2 O 0.4418(4) 1.1922(3) 0.61524(9) 0.0200(8) Uani 1 1 d . . . . . P1 P 0.09575(14) 0.58289(10) 0.60747(3) 0.0143(3) Uani 1 1 d . . . . . P2 P 0.49797(15) 1.07973(11) 0.60736(3) 0.0152(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.010(2) 0.016(2) 0.020(3) 0.001(2) 0.001(2) 0.002(2) C2 0.014(2) 0.013(2) 0.019(3) 0.003(2) 0.000(2) 0.0024(19) C3 0.010(2) 0.014(2) 0.022(2) -0.003(2) 0.0008(19) -0.001(2) C4 0.008(2) 0.021(3) 0.016(2) -0.002(2) -0.0004(19) 0.000(2) C5 0.020(3) 0.015(3) 0.022(3) -0.008(2) -0.001(2) -0.005(2) C6 0.016(2) 0.015(3) 0.017(2) 0.000(2) 0.004(2) -0.001(2) C7 0.016(3) 0.016(3) 0.015(2) 0.001(2) 0.001(2) -0.003(2) C8 0.015(2) 0.017(3) 0.021(3) 0.001(2) -0.002(2) -0.003(2) C9 0.031(3) 0.022(3) 0.028(3) 0.003(2) 0.006(3) -0.002(3) C10 0.039(4) 0.034(3) 0.025(3) 0.000(3) 0.017(3) 0.004(3) C11 0.043(4) 0.023(3) 0.032(3) 0.014(3) 0.004(3) 0.000(3) C12 0.033(3) 0.017(3) 0.036(3) 0.007(2) 0.000(3) 0.008(2) C13 0.018(3) 0.019(3) 0.021(3) 0.001(2) -0.001(2) 0.003(2) C14 0.015(2) 0.012(2) 0.025(3) 0.002(2) 0.004(2) 0.003(2) C15 0.010(2) 0.032(3) 0.029(3) -0.002(3) -0.002(2) -0.007(2) C16 0.015(3) 0.027(3) 0.033(3) 0.007(3) 0.000(2) 0.008(2) C17 0.014(2) 0.019(3) 0.024(3) 0.003(2) 0.002(2) 0.001(2) C18 0.015(3) 0.020(3) 0.018(3) 0.004(2) 0.001(2) -0.002(2) C19 0.038(2) 0.047(2) 0.051(3) 0.022(2) 0.015(2) 0.012(2) C20 0.043(3) 0.047(3) 0.055(3) 0.031(3) 0.013(2) 0.021(3) C21 0.046(4) 0.039(4) 0.021(3) -0.001(3) -0.010(3) -0.006(3) C22 0.053(4) 0.030(3) 0.019(3) -0.004(2) -0.002(3) 0.004(3) C23 0.038(3) 0.024(3) 0.020(3) 0.002(2) -0.001(3) 0.000(3) C24 0.015(2) 0.020(3) 0.019(2) 0.003(2) 0.001(2) -0.007(2) C25 0.017(3) 0.028(3) 0.028(3) 0.006(2) 0.002(2) -0.002(2) C26 0.024(3) 0.032(3) 0.037(4) 0.012(3) 0.000(3) -0.006(3) C27 0.028(3) 0.046(4) 0.024(3) 0.010(3) -0.001(3) -0.012(3) C28 0.035(3) 0.045(4) 0.024(3) -0.001(3) 0.004(3) -0.010(3) C29 0.025(3) 0.030(3) 0.026(3) 0.002(2) 0.005(2) -0.001(3) C30 0.015(2) 0.014(2) 0.024(3) -0.002(2) 0.003(2) 0.000(2) C31 0.015(3) 0.018(3) 0.038(3) -0.013(3) 0.011(3) -0.005(2) C32 0.015(3) 0.031(3) 0.030(3) -0.010(3) 0.007(2) -0.002(3) C33 0.008(2) 0.027(3) 0.026(3) -0.008(2) 0.000(2) -0.001(2) C34 0.010(2) 0.015(2) 0.014(2) 0.0033(19) -0.0006(19) -0.0048(19) C35 0.016(2) 0.014(3) 0.020(3) -0.001(2) 0.001(2) -0.006(2) C36 0.017(3) 0.009(2) 0.035(3) -0.001(2) 0.010(2) -0.002(2) C37 0.023(3) 0.018(3) 0.042(4) 0.011(3) 0.015(3) 0.004(2) C38 0.032(4) 0.042(4) 0.048(4) 0.020(3) 0.008(3) 0.005(3) C39 0.038(2) 0.047(2) 0.051(3) 0.022(2) 0.015(2) 0.012(2) C40 0.043(3) 0.047(3) 0.055(3) 0.031(3) 0.013(2) 0.021(3) C41 0.038(2) 0.047(2) 0.051(3) 0.022(2) 0.015(2) 0.012(2) C42 0.052(4) 0.017(3) 0.057(4) 0.013(3) 0.030(4) 0.014(3) C43 0.019(3) 0.026(3) 0.025(3) -0.001(3) 0.003(2) 0.006(2) C44 0.010(2) 0.026(3) 0.031(3) -0.005(2) 0.002(2) -0.003(2) C45 0.012(2) 0.028(3) 0.024(3) -0.001(2) 0.007(2) -0.003(2) C46 0.024(3) 0.011(2) 0.022(3) 0.001(2) 0.002(2) -0.003(2) C47 0.016(3) 0.017(3) 0.027(3) -0.004(2) 0.004(2) 0.004(2) C48 0.020(3) 0.014(3) 0.022(3) -0.005(2) 0.006(2) -0.002(2) C49 0.030(3) 0.020(3) 0.026(3) 0.004(2) 0.015(2) 0.001(2) C50 0.047(4) 0.034(3) 0.021(3) 0.005(3) 0.009(3) -0.003(3) C51 0.052(4) 0.028(3) 0.021(3) 0.001(2) -0.002(3) -0.007(3) C52 0.026(3) 0.019(3) 0.024(3) 0.002(2) 0.001(2) -0.004(2) C53 0.013(3) 0.047(4) 0.022(3) -0.004(3) 0.000(2) 0.008(3) C54 0.025(3) 0.040(4) 0.029(3) 0.001(3) 0.000(3) 0.013(3) C55 0.040(4) 0.054(4) 0.030(4) 0.009(3) 0.003(3) 0.026(4) C56 0.051(5) 0.070(6) 0.030(4) 0.006(4) -0.001(3) 0.036(4) C57 0.039(4) 0.096(7) 0.023(3) -0.019(4) -0.018(3) 0.029(4) C58 0.023(3) 0.056(4) 0.038(4) -0.014(3) -0.008(3) 0.010(3) O1 0.0203(19) 0.0145(18) 0.0229(19) 0.0003(15) -0.0010(16) 0.0000(15) O2 0.0152(18) 0.0183(18) 0.026(2) 0.0037(16) 0.0015(16) 0.0043(15) P1 0.0119(6) 0.0129(6) 0.0181(6) 0.0018(6) -0.0004(5) 0.0019(5) P2 0.0104(6) 0.0155(6) 0.0198(6) -0.0004(6) 0.0022(5) 0.0014(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C18 1.480(7) . ? C1 C2 1.519(7) . ? C1 C7 1.564(7) . ? C1 P1 1.818(5) . ? C2 C3 1.485(7) . ? C2 C7 1.560(7) . ? C2 H2 1.0000 . ? C3 C4 1.350(7) . ? C3 H3 0.9500 . ? C4 C24 1.468(7) . ? C4 P1 1.809(5) . ? C5 C17 1.375(8) . ? C5 C6 1.379(7) . ? C5 P1 1.819(5) . ? C6 C14 1.393(7) . ? C6 C7 1.496(7) . ? C7 C8 1.505(7) . ? C8 C13 1.385(8) . ? C8 C9 1.400(8) . ? C9 C10 1.383(8) . ? C9 H9 0.9500 . ? C10 C11 1.384(9) . ? C10 H10 0.9500 . ? C11 C12 1.387(9) . ? C11 H11 0.9500 . ? C12 C13 1.373(8) . ? C12 H12 0.9500 . ? C13 H13 0.9500 . ? C14 C15 1.387(8) . ? C14 H14 0.9500 . ? C15 C16 1.386(8) . ? C15 H15 0.9500 . ? C16 C17 1.395(8) . ? C16 H16 0.9500 . ? C17 H17 0.9500 . ? C18 C23 1.391(8) . ? C18 C19 1.392(9) . ? C19 C20 1.393(11) . ? C19 H19 0.9500 . ? C20 C21 1.388(10) . ? C20 H20 0.9500 . ? C21 C22 1.373(9) . ? C21 H21 0.9500 . ? C22 C23 1.383(8) . ? C22 H22 0.9500 . ? C23 H23 0.9500 . ? C24 C25 1.399(8) . ? C24 C29 1.400(8) . ? C25 C26 1.385(8) . ? C25 H25 0.9500 . ? C26 C27 1.373(9) . ? C26 H26 0.9500 . ? C27 C28 1.381(10) . ? C27 H27 0.9500 . ? C28 C29 1.383(8) . ? C28 H28 0.9500 . ? C29 H29 0.9500 . ? C30 C47 1.489(7) . ? C30 C31 1.512(7) . ? C30 C36 1.541(7) . ? C30 P2 1.828(5) . ? C31 C32 1.472(9) . ? C31 C36 1.566(8) . ? C31 H31 1.0000 . ? C32 C33 1.339(8) . ? C32 H32 0.9500 . ? C33 C53 1.479(8) . ? C33 P2 1.811(5) . ? C34 C46 1.407(7) . ? C34 C35 1.410(7) . ? C34 P2 1.782(5) . ? C35 C43 1.397(7) . ? C35 C36 1.501(7) . ? C36 C37 1.488(8) . ? C37 C38 1.386(10) . ? C37 C42 1.392(9) . ? C38 C39 1.378(9) . ? C38 H38 0.9500 . ? C39 C40 1.418(11) . ? C39 H39 0.9500 . ? C40 C41 1.334(11) . ? C40 H40 0.9500 . ? C41 C42 1.371(9) . ? C41 H41 0.9500 . ? C42 H42 0.9500 . ? C43 C44 1.387(8) . ? C43 H43 0.9500 . ? C44 C45 1.400(8) . ? C44 H44 0.9500 . ? C45 C46 1.380(8) . ? C45 H45 0.9500 . ? C46 H46 0.9500 . ? C47 C48 1.391(7) . ? C47 C52 1.397(7) . ? C48 C49 1.397(7) . ? C48 H48 0.9500 . ? C49 C50 1.370(9) . ? C49 H49 0.9500 . ? C50 C51 1.393(9) . ? C50 H50 0.9500 . ? C51 C52 1.377(8) . ? C51 H51 0.9500 . ? C52 H52 0.9500 . ? C53 C54 1.393(10) . ? C53 C58 1.405(8) . ? C54 C55 1.384(9) . ? C54 H54 0.9500 . ? C55 C56 1.375(11) . ? C55 H55 0.9500 . ? C56 C57 1.385(12) . ? C56 H56 0.9500 . ? C57 C58 1.398(10) . ? C57 H57 0.9500 . ? C58 H58 0.9500 . ? O1 P1 1.491(4) . ? O2 P2 1.479(4) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C18 C1 C2 124.9(4) . . ? C18 C1 C7 119.5(4) . . ? C2 C1 C7 60.8(3) . . ? C18 C1 P1 125.2(4) . . ? C2 C1 P1 103.6(3) . . ? C7 C1 P1 104.7(3) . . ? C3 C2 C1 111.8(4) . . ? C3 C2 C7 121.5(4) . . ? C1 C2 C7 61.0(3) . . ? C3 C2 H2 116.7 . . ? C1 C2 H2 116.7 . . ? C7 C2 H2 116.7 . . ? C4 C3 C2 117.7(5) . . ? C4 C3 H3 121.1 . . ? C2 C3 H3 121.1 . . ? C3 C4 C24 127.3(5) . . ? C3 C4 P1 107.5(4) . . ? C24 C4 P1 124.3(4) . . ? C17 C5 C6 122.6(5) . . ? C17 C5 P1 128.4(4) . . ? C6 C5 P1 108.6(4) . . ? C5 C6 C14 119.0(5) . . ? C5 C6 C7 117.5(5) . . ? C14 C6 C7 123.6(4) . . ? C6 C7 C8 117.8(4) . . ? C6 C7 C2 120.4(4) . . ? C8 C7 C2 117.2(4) . . ? C6 C7 C1 110.3(4) . . ? C8 C7 C1 118.5(4) . . ? C2 C7 C1 58.2(3) . . ? C13 C8 C9 119.1(5) . . ? C13 C8 C7 122.1(5) . . ? C9 C8 C7 118.8(5) . . ? C10 C9 C8 119.3(5) . . ? C10 C9 H9 120.3 . . ? C8 C9 H9 120.3 . . ? C9 C10 C11 120.8(6) . . ? C9 C10 H10 119.6 . . ? C11 C10 H10 119.6 . . ? C10 C11 C12 119.7(5) . . ? C10 C11 H11 120.1 . . ? C12 C11 H11 120.1 . . ? C13 C12 C11 119.6(5) . . ? C13 C12 H12 120.2 . . ? C11 C12 H12 120.2 . . ? C12 C13 C8 121.3(5) . . ? C12 C13 H13 119.3 . . ? C8 C13 H13 119.3 . . ? C15 C14 C6 118.9(5) . . ? C15 C14 H14 120.5 . . ? C6 C14 H14 120.5 . . ? C16 C15 C14 121.6(5) . . ? C16 C15 H15 119.2 . . ? C14 C15 H15 119.2 . . ? C15 C16 C17 119.3(5) . . ? C15 C16 H16 120.3 . . ? C17 C16 H16 120.3 . . ? C5 C17 C16 118.6(5) . . ? C5 C17 H17 120.7 . . ? C16 C17 H17 120.7 . . ? C23 C18 C19 119.0(6) . . ? C23 C18 C1 119.2(5) . . ? C19 C18 C1 121.7(5) . . ? C18 C19 C20 119.9(7) . . ? C18 C19 H19 120.0 . . ? C20 C19 H19 120.0 . . ? C21 C20 C19 120.8(6) . . ? C21 C20 H20 119.6 . . ? C19 C20 H20 119.6 . . ? C22 C21 C20 118.7(6) . . ? C22 C21 H21 120.7 . . ? C20 C21 H21 120.7 . . ? C21 C22 C23 121.5(6) . . ? C21 C22 H22 119.3 . . ? C23 C22 H22 119.3 . . ? C22 C23 C18 120.1(6) . . ? C22 C23 H23 120.0 . . ? C18 C23 H23 120.0 . . ? C25 C24 C29 117.8(5) . . ? C25 C24 C4 120.9(5) . . ? C29 C24 C4 121.2(5) . . ? C26 C25 C24 120.4(6) . . ? C26 C25 H25 119.8 . . ? C24 C25 H25 119.8 . . ? C27 C26 C25 120.8(6) . . ? C27 C26 H26 119.6 . . ? C25 C26 H26 119.6 . . ? C26 C27 C28 119.8(6) . . ? C26 C27 H27 120.1 . . ? C28 C27 H27 120.1 . . ? C27 C28 C29 119.9(6) . . ? C27 C28 H28 120.0 . . ? C29 C28 H28 120.0 . . ? C28 C29 C24 121.2(6) . . ? C28 C29 H29 119.4 . . ? C24 C29 H29 119.4 . . ? C47 C30 C31 124.8(5) . . ? C47 C30 C36 120.5(5) . . ? C31 C30 C36 61.7(4) . . ? C47 C30 P2 124.2(4) . . ? C31 C30 P2 103.5(4) . . ? C36 C30 P2 105.2(3) . . ? C32 C31 C30 111.8(5) . . ? C32 C31 C36 121.9(5) . . ? C30 C31 C36 60.1(3) . . ? C32 C31 H31 116.7 . . ? C30 C31 H31 116.7 . . ? C36 C31 H31 116.7 . . ? C33 C32 C31 118.5(5) . . ? C33 C32 H32 120.8 . . ? C31 C32 H32 120.8 . . ? C32 C33 C53 128.0(5) . . ? C32 C33 P2 107.4(4) . . ? C53 C33 P2 123.6(4) . . ? C46 C34 C35 119.2(5) . . ? C46 C34 P2 130.1(4) . . ? C35 C34 P2 110.0(4) . . ? C43 C35 C34 120.8(5) . . ? C43 C35 C36 124.0(5) . . ? C34 C35 C36 115.1(5) . . ? C37 C36 C35 117.2(5) . . ? C37 C36 C30 118.0(5) . . ? C35 C36 C30 111.3(4) . . ? C37 C36 C31 118.6(5) . . ? C35 C36 C31 119.5(5) . . ? C30 C36 C31 58.2(3) . . ? C38 C37 C42 118.7(6) . . ? C38 C37 C36 118.3(5) . . ? C42 C37 C36 123.0(6) . . ? C39 C38 C37 121.0(7) . . ? C39 C38 H38 119.5 . . ? C37 C38 H38 119.5 . . ? C38 C39 C40 117.7(8) . . ? C38 C39 H39 121.2 . . ? C40 C39 H39 121.2 . . ? C41 C40 C39 121.9(7) . . ? C41 C40 H40 119.1 . . ? C39 C40 H40 119.1 . . ? C40 C41 C42 119.8(8) . . ? C40 C41 H41 120.1 . . ? C42 C41 H41 120.1 . . ? C41 C42 C37 120.9(8) . . ? C41 C42 H42 119.5 . . ? C37 C42 H42 119.5 . . ? C44 C43 C35 118.7(5) . . ? C44 C43 H43 120.7 . . ? C35 C43 H43 120.7 . . ? C43 C44 C45 121.1(5) . . ? C43 C44 H44 119.4 . . ? C45 C44 H44 119.4 . . ? C46 C45 C44 120.3(5) . . ? C46 C45 H45 119.9 . . ? C44 C45 H45 119.9 . . ? C45 C46 C34 119.9(5) . . ? C45 C46 H46 120.1 . . ? C34 C46 H46 120.1 . . ? C48 C47 C52 119.5(5) . . ? C48 C47 C30 121.2(5) . . ? C52 C47 C30 119.0(5) . . ? C47 C48 C49 120.2(5) . . ? C47 C48 H48 119.9 . . ? C49 C48 H48 119.9 . . ? C50 C49 C48 119.7(5) . . ? C50 C49 H49 120.2 . . ? C48 C49 H49 120.2 . . ? C49 C50 C51 120.6(6) . . ? C49 C50 H50 119.7 . . ? C51 C50 H50 119.7 . . ? C52 C51 C50 120.1(6) . . ? C52 C51 H51 119.9 . . ? C50 C51 H51 119.9 . . ? C51 C52 C47 120.0(5) . . ? C51 C52 H52 120.0 . . ? C47 C52 H52 120.0 . . ? C54 C53 C58 118.8(6) . . ? C54 C53 C33 121.1(5) . . ? C58 C53 C33 120.1(6) . . ? C55 C54 C53 120.7(6) . . ? C55 C54 H54 119.6 . . ? C53 C54 H54 119.6 . . ? C56 C55 C54 120.6(8) . . ? C56 C55 H55 119.7 . . ? C54 C55 H55 119.7 . . ? C55 C56 C57 119.6(7) . . ? C55 C56 H56 120.2 . . ? C57 C56 H56 120.2 . . ? C56 C57 C58 120.7(7) . . ? C56 C57 H57 119.7 . . ? C58 C57 H57 119.7 . . ? C57 C58 C53 119.5(7) . . ? C57 C58 H58 120.3 . . ? C53 C58 H58 120.3 . . ? O1 P1 C4 120.2(2) . . ? O1 P1 C1 121.1(2) . . ? C4 P1 C1 95.7(2) . . ? O1 P1 C5 121.1(2) . . ? C4 P1 C5 97.2(2) . . ? C1 P1 C5 95.5(2) . . ? O2 P2 C34 120.2(2) . . ? O2 P2 C33 120.6(2) . . ? C34 P2 C33 97.6(2) . . ? O2 P2 C30 122.0(2) . . ? C34 P2 C30 95.2(2) . . ? C33 P2 C30 95.0(3) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C18 C1 C2 C3 -137.8(5) . . . . ? C7 C1 C2 C3 114.9(5) . . . . ? P1 C1 C2 C3 15.4(5) . . . . ? C18 C1 C2 C7 107.3(5) . . . . ? P1 C1 C2 C7 -99.5(3) . . . . ? C1 C2 C3 C4 -4.6(6) . . . . ? C7 C2 C3 C4 63.9(7) . . . . ? C2 C3 C4 C24 -178.8(5) . . . . ? C2 C3 C4 P1 -9.2(6) . . . . ? C17 C5 C6 C14 -0.6(8) . . . . ? P1 C5 C6 C14 -174.5(4) . . . . ? C17 C5 C6 C7 179.7(5) . . . . ? P1 C5 C6 C7 5.8(6) . . . . ? C5 C6 C7 C8 147.8(5) . . . . ? C14 C6 C7 C8 -31.9(7) . . . . ? C5 C6 C7 C2 -56.9(7) . . . . ? C14 C6 C7 C2 123.4(5) . . . . ? C5 C6 C7 C1 7.4(6) . . . . ? C14 C6 C7 C1 -172.3(5) . . . . ? C3 C2 C7 C6 -2.9(7) . . . . ? C1 C2 C7 C6 96.3(5) . . . . ? C3 C2 C7 C8 152.6(5) . . . . ? C1 C2 C7 C8 -108.3(5) . . . . ? C3 C2 C7 C1 -99.1(5) . . . . ? C18 C1 C7 C6 130.1(5) . . . . ? C2 C1 C7 C6 -114.0(4) . . . . ? P1 C1 C7 C6 -16.4(5) . . . . ? C18 C1 C7 C8 -10.0(7) . . . . ? C2 C1 C7 C8 105.9(5) . . . . ? P1 C1 C7 C8 -156.5(4) . . . . ? C18 C1 C7 C2 -115.9(5) . . . . ? P1 C1 C7 C2 97.5(4) . . . . ? C6 C7 C8 C13 130.3(5) . . . . ? C2 C7 C8 C13 -25.8(7) . . . . ? C1 C7 C8 C13 -92.6(6) . . . . ? C6 C7 C8 C9 -50.2(7) . . . . ? C2 C7 C8 C9 153.7(5) . . . . ? C1 C7 C8 C9 86.9(6) . . . . ? C13 C8 C9 C10 -0.5(9) . . . . ? C7 C8 C9 C10 179.9(6) . . . . ? C8 C9 C10 C11 -0.9(10) . . . . ? C9 C10 C11 C12 1.6(11) . . . . ? C10 C11 C12 C13 -0.8(10) . . . . ? C11 C12 C13 C8 -0.7(9) . . . . ? C9 C8 C13 C12 1.4(8) . . . . ? C7 C8 C13 C12 -179.1(5) . . . . ? C5 C6 C14 C15 0.4(8) . . . . ? C7 C6 C14 C15 -180.0(5) . . . . ? C6 C14 C15 C16 0.0(8) . . . . ? C14 C15 C16 C17 -0.1(9) . . . . ? C6 C5 C17 C16 0.4(8) . . . . ? P1 C5 C17 C16 173.1(4) . . . . ? C15 C16 C17 C5 -0.1(8) . . . . ? C2 C1 C18 C23 -173.6(5) . . . . ? C7 C1 C18 C23 -100.4(6) . . . . ? P1 C1 C18 C23 38.8(7) . . . . ? C2 C1 C18 C19 3.4(8) . . . . ? C7 C1 C18 C19 76.6(7) . . . . ? P1 C1 C18 C19 -144.2(5) . . . . ? C23 C18 C19 C20 4.1(10) . . . . ? C1 C18 C19 C20 -172.9(6) . . . . ? C18 C19 C20 C21 -2.9(11) . . . . ? C19 C20 C21 C22 0.4(11) . . . . ? C20 C21 C22 C23 0.7(11) . . . . ? C21 C22 C23 C18 0.5(10) . . . . ? C19 C18 C23 C22 -2.9(9) . . . . ? C1 C18 C23 C22 174.1(6) . . . . ? C3 C4 C24 C25 159.9(5) . . . . ? P1 C4 C24 C25 -8.1(7) . . . . ? C3 C4 C24 C29 -18.6(8) . . . . ? P1 C4 C24 C29 173.4(4) . . . . ? C29 C24 C25 C26 1.4(8) . . . . ? C4 C24 C25 C26 -177.2(5) . . . . ? C24 C25 C26 C27 -0.7(9) . . . . ? C25 C26 C27 C28 -0.3(9) . . . . ? C26 C27 C28 C29 0.5(10) . . . . ? C27 C28 C29 C24 0.3(10) . . . . ? C25 C24 C29 C28 -1.2(9) . . . . ? C4 C24 C29 C28 177.4(5) . . . . ? C47 C30 C31 C32 135.6(5) . . . . ? C36 C30 C31 C32 -115.3(5) . . . . ? P2 C30 C31 C32 -15.1(5) . . . . ? C47 C30 C31 C36 -109.2(6) . . . . ? P2 C30 C31 C36 100.2(4) . . . . ? C30 C31 C32 C33 4.0(7) . . . . ? C36 C31 C32 C33 -63.4(7) . . . . ? C31 C32 C33 C53 178.2(5) . . . . ? C31 C32 C33 P2 9.7(6) . . . . ? C46 C34 C35 C43 2.1(8) . . . . ? P2 C34 C35 C43 173.4(4) . . . . ? C46 C34 C35 C36 -178.9(5) . . . . ? P2 C34 C35 C36 -7.6(6) . . . . ? C43 C35 C36 C37 33.6(8) . . . . ? C34 C35 C36 C37 -145.4(5) . . . . ? C43 C35 C36 C30 173.7(5) . . . . ? C34 C35 C36 C30 -5.3(7) . . . . ? C43 C35 C36 C31 -121.7(6) . . . . ? C34 C35 C36 C31 59.3(6) . . . . ? C47 C30 C36 C37 7.9(7) . . . . ? C31 C30 C36 C37 -108.0(6) . . . . ? P2 C30 C36 C37 154.6(4) . . . . ? C47 C30 C36 C35 -131.9(5) . . . . ? C31 C30 C36 C35 112.3(5) . . . . ? P2 C30 C36 C35 14.9(5) . . . . ? C47 C30 C36 C31 115.8(6) . . . . ? P2 C30 C36 C31 -97.4(4) . . . . ? C32 C31 C36 C37 -154.6(5) . . . . ? C30 C31 C36 C37 107.0(5) . . . . ? C32 C31 C36 C35 0.4(7) . . . . ? C30 C31 C36 C35 -98.1(5) . . . . ? C32 C31 C36 C30 98.4(6) . . . . ? C35 C36 C37 C38 52.9(7) . . . . ? C30 C36 C37 C38 -84.4(7) . . . . ? C31 C36 C37 C38 -151.5(5) . . . . ? C35 C36 C37 C42 -128.0(6) . . . . ? C30 C36 C37 C42 94.7(7) . . . . ? C31 C36 C37 C42 27.6(8) . . . . ? C42 C37 C38 C39 1.5(10) . . . . ? C36 C37 C38 C39 -179.4(6) . . . . ? C37 C38 C39 C40 0.0(10) . . . . ? C38 C39 C40 C41 -1.4(11) . . . . ? C39 C40 C41 C42 1.4(11) . . . . ? C40 C41 C42 C37 0.2(10) . . . . ? C38 C37 C42 C41 -1.6(10) . . . . ? C36 C37 C42 C41 179.3(6) . . . . ? C34 C35 C43 C44 -2.0(8) . . . . ? C36 C35 C43 C44 179.1(5) . . . . ? C35 C43 C44 C45 0.7(8) . . . . ? C43 C44 C45 C46 0.6(8) . . . . ? C44 C45 C46 C34 -0.5(8) . . . . ? C35 C34 C46 C45 -0.8(8) . . . . ? P2 C34 C46 C45 -170.1(4) . . . . ? C31 C30 C47 C48 -0.7(8) . . . . ? C36 C30 C47 C48 -75.7(7) . . . . ? P2 C30 C47 C48 144.1(5) . . . . ? C31 C30 C47 C52 173.4(5) . . . . ? C36 C30 C47 C52 98.5(6) . . . . ? P2 C30 C47 C52 -41.7(7) . . . . ? C52 C47 C48 C49 -2.2(8) . . . . ? C30 C47 C48 C49 171.9(5) . . . . ? C47 C48 C49 C50 1.1(9) . . . . ? C48 C49 C50 C51 1.3(10) . . . . ? C49 C50 C51 C52 -2.4(11) . . . . ? C50 C51 C52 C47 1.2(10) . . . . ? C48 C47 C52 C51 1.1(9) . . . . ? C30 C47 C52 C51 -173.2(6) . . . . ? C32 C33 C53 C54 -159.9(6) . . . . ? P2 C33 C53 C54 7.0(7) . . . . ? C32 C33 C53 C58 19.8(9) . . . . ? P2 C33 C53 C58 -173.4(4) . . . . ? C58 C53 C54 C55 -3.0(9) . . . . ? C33 C53 C54 C55 176.7(5) . . . . ? C53 C54 C55 C56 2.8(10) . . . . ? C54 C55 C56 C57 -1.6(11) . . . . ? C55 C56 C57 C58 0.6(11) . . . . ? C56 C57 C58 C53 -0.8(10) . . . . ? C54 C53 C58 C57 2.0(9) . . . . ? C33 C53 C58 C57 -177.7(6) . . . . ? C3 C4 P1 O1 147.4(3) . . . . ? C24 C4 P1 O1 -42.6(5) . . . . ? C3 C4 P1 C1 16.2(4) . . . . ? C24 C4 P1 C1 -173.8(4) . . . . ? C3 C4 P1 C5 -80.1(4) . . . . ? C24 C4 P1 C5 89.9(5) . . . . ? C18 C1 P1 O1 4.8(5) . . . . ? C2 C1 P1 O1 -148.3(3) . . . . ? C7 C1 P1 O1 148.8(3) . . . . ? C18 C1 P1 C4 135.4(4) . . . . ? C2 C1 P1 C4 -17.7(4) . . . . ? C7 C1 P1 C4 -80.6(3) . . . . ? C18 C1 P1 C5 -126.8(4) . . . . ? C2 C1 P1 C5 80.0(3) . . . . ? C7 C1 P1 C5 17.2(4) . . . . ? C17 C5 P1 O1 40.9(6) . . . . ? C6 C5 P1 O1 -145.7(3) . . . . ? C17 C5 P1 C4 -91.0(5) . . . . ? C6 C5 P1 C4 82.4(4) . . . . ? C17 C5 P1 C1 172.5(5) . . . . ? C6 C5 P1 C1 -14.0(4) . . . . ? C46 C34 P2 O2 -43.4(6) . . . . ? C35 C34 P2 O2 146.5(3) . . . . ? C46 C34 P2 C33 88.8(5) . . . . ? C35 C34 P2 C33 -81.2(4) . . . . ? C46 C34 P2 C30 -175.4(5) . . . . ? C35 C34 P2 C30 14.6(4) . . . . ? C32 C33 P2 O2 -148.4(4) . . . . ? C53 C33 P2 O2 42.5(5) . . . . ? C32 C33 P2 C34 79.7(4) . . . . ? C53 C33 P2 C34 -89.5(5) . . . . ? C32 C33 P2 C30 -16.3(4) . . . . ? C53 C33 P2 C30 174.6(4) . . . . ? C47 C30 P2 O2 -2.2(6) . . . . ? C31 C30 P2 O2 148.7(3) . . . . ? C36 C30 P2 O2 -147.4(3) . . . . ? C47 C30 P2 C34 128.6(5) . . . . ? C31 C30 P2 C34 -80.6(4) . . . . ? C36 C30 P2 C34 -16.6(4) . . . . ? C47 C30 P2 C33 -133.3(5) . . . . ? C31 C30 P2 C33 17.5(4) . . . . ? C36 C30 P2 C33 81.5(4) . . . . ? _refine_diff_density_max 0.854 _refine_diff_density_min -0.566 _refine_diff_density_rms 0.073 _shelx_res_file ; MR280.res created by SHELXL-2014/7 TITL MR280_a.res in P2(1)2(1)2(1) REM Old TITL MR280 in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.176, Rweak 0.049, Alpha 0.013, Orientation as input REM Flack x = 0.337 ( 0.093 ) from Parsons' quotients REM Formula found by SHELXT: C58 O2 P2 CELL 0.71073 8.3195 12.1199 42.2796 90.000 90.000 90.000 ZERR 8.000 0.0001 0.0002 0.0008 0.000 0.000 0.000 LATT -1 SYMM 1/2-X, -Y, 1/2+Z SYMM -X, 1/2+Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H O P DISP $C 0.00341 0.00169 11.32113!source kissel DISP $H -0.00002 0.00000 0.66638!source kissel DISP $O 0.01140 0.00623 32.03669!source kissel DISP $P 0.10406 0.09609 404.11213!source kissel UNIT 232 168 8 8 TEMP -165.320 SIZE 0.13 0.21 0.44 L.S. 30 eadp C20 C40 eadp C19 C41 C39 BOND $H LIST 6 FMAP 2 twin acta conf PLAN 20 WGHT 0.029800 10.814200 EXTI 0.008297 BASF 0.59153 FVAR 0.41869 C1 1 0.140065 0.466007 0.632969 11.00000 0.00966 0.01551 = 0.01999 0.00052 0.00060 0.00170 C2 1 0.157092 0.370317 0.610005 11.00000 0.01398 0.01349 = 0.01895 0.00282 -0.00032 0.00237 AFIX 13 H2 2 0.227175 0.307689 0.616856 11.00000 -1.20000 AFIX 0 C3 1 0.176699 0.409033 0.576897 11.00000 0.00955 0.01441 = 0.02159 -0.00325 0.00083 -0.00105 AFIX 43 H3 2 0.196397 0.358507 0.560162 11.00000 -1.20000 AFIX 0 C4 1 0.165561 0.518509 0.571405 11.00000 0.00768 0.02104 = 0.01608 -0.00165 -0.00039 0.00049 C5 1 -0.116372 0.550674 0.602665 11.00000 0.02043 0.01492 = 0.02183 -0.00771 -0.00076 -0.00526 C6 1 -0.142619 0.444303 0.613030 11.00000 0.01632 0.01532 = 0.01715 -0.00008 0.00445 -0.00092 C7 1 -0.004623 0.385318 0.628173 11.00000 0.01580 0.01648 = 0.01470 0.00126 0.00130 -0.00321 C8 1 -0.041934 0.303350 0.653880 11.00000 0.01537 0.01729 = 0.02096 0.00149 -0.00215 -0.00315 C9 1 -0.142712 0.335602 0.678735 11.00000 0.03080 0.02215 = 0.02840 0.00336 0.00637 -0.00236 AFIX 43 H9 2 -0.186357 0.408009 0.679280 11.00000 -1.20000 AFIX 0 C10 1 -0.178080 0.261005 0.702481 11.00000 0.03911 0.03434 = 0.02484 0.00034 0.01719 0.00429 AFIX 43 H10 2 -0.245112 0.282929 0.719551 11.00000 -1.20000 AFIX 0 C11 1 -0.117083 0.154832 0.701696 11.00000 0.04296 0.02316 = 0.03184 0.01393 0.00390 -0.00042 AFIX 43 H11 2 -0.144414 0.103664 0.717846 11.00000 -1.20000 AFIX 0 C12 1 -0.015860 0.123415 0.677230 11.00000 0.03258 0.01703 = 0.03585 0.00739 -0.00030 0.00805 AFIX 43 H12 2 0.027599 0.050955 0.676688 11.00000 -1.20000 AFIX 0 C13 1 0.021157 0.197604 0.653811 11.00000 0.01794 0.01880 = 0.02120 0.00135 -0.00108 0.00287 AFIX 43 H13 2 0.091452 0.175989 0.637223 11.00000 -1.20000 AFIX 0 C14 1 -0.294344 0.397732 0.609104 11.00000 0.01454 0.01216 = 0.02537 0.00150 0.00405 0.00281 AFIX 43 H14 2 -0.315558 0.324755 0.616163 11.00000 -1.20000 AFIX 0 C15 1 -0.413988 0.459672 0.594716 11.00000 0.01029 0.03237 = 0.02885 -0.00208 -0.00166 -0.00719 AFIX 43 H15 2 -0.517658 0.428236 0.591971 11.00000 -1.20000 AFIX 0 C16 1 -0.385915 0.566336 0.584247 11.00000 0.01525 0.02676 = 0.03313 0.00698 -0.00016 0.00826 AFIX 43 H16 2 -0.469374 0.607405 0.574419 11.00000 -1.20000 AFIX 0 C17 1 -0.233881 0.612742 0.588290 11.00000 0.01440 0.01861 = 0.02373 0.00256 0.00231 0.00081 AFIX 43 H17 2 -0.211979 0.685661 0.581264 11.00000 -1.20000 AFIX 0 C18 1 0.219025 0.472818 0.664267 11.00000 0.01542 0.01952 = 0.01805 0.00359 0.00086 -0.00159 C19 1 0.324940 0.391751 0.674714 11.00000 0.03849 0.04702 = 0.05061 0.02187 0.01475 0.01195 AFIX 43 H19 2 0.357581 0.334428 0.660800 11.00000 -1.20000 AFIX 0 C20 1 0.383003 0.394785 0.705595 11.00000 0.04274 0.04657 = 0.05522 0.03126 0.01330 0.02107 AFIX 43 H20 2 0.451394 0.337455 0.712922 11.00000 -1.20000 AFIX 0 C21 1 0.342114 0.480608 0.725797 11.00000 0.04564 0.03855 = 0.02111 -0.00131 -0.01011 -0.00645 AFIX 43 H21 2 0.382418 0.482815 0.746811 11.00000 -1.20000 AFIX 0 C22 1 0.242234 0.562255 0.714796 11.00000 0.05258 0.03005 = 0.01939 -0.00423 -0.00217 0.00381 AFIX 43 H22 2 0.214589 0.621768 0.728370 11.00000 -1.20000 AFIX 0 C23 1 0.181003 0.559750 0.684391 11.00000 0.03785 0.02450 = 0.02047 0.00167 -0.00066 -0.00020 AFIX 43 H23 2 0.112871 0.617499 0.677244 11.00000 -1.20000 AFIX 0 C24 1 0.177809 0.575122 0.540808 11.00000 0.01489 0.02015 = 0.01940 0.00275 0.00062 -0.00655 C25 1 0.116067 0.681564 0.536749 11.00000 0.01706 0.02767 = 0.02763 0.00555 0.00228 -0.00213 AFIX 43 H25 2 0.069724 0.719259 0.554212 11.00000 -1.20000 AFIX 0 C26 1 0.122117 0.732277 0.507430 11.00000 0.02434 0.03211 = 0.03713 0.01151 -0.00005 -0.00599 AFIX 43 H26 2 0.078753 0.804261 0.504928 11.00000 -1.20000 AFIX 0 C27 1 0.189986 0.679863 0.481926 11.00000 0.02793 0.04627 = 0.02396 0.00995 -0.00081 -0.01200 AFIX 43 H27 2 0.192951 0.715348 0.461899 11.00000 -1.20000 AFIX 0 C28 1 0.253917 0.575454 0.485455 11.00000 0.03450 0.04473 = 0.02377 -0.00098 0.00365 -0.00996 AFIX 43 H28 2 0.301730 0.539206 0.467894 11.00000 -1.20000 AFIX 0 C29 1 0.248259 0.523705 0.514593 11.00000 0.02527 0.02992 = 0.02616 0.00174 0.00482 -0.00106 AFIX 43 H29 2 0.292961 0.452011 0.516858 11.00000 -1.20000 AFIX 0 C30 1 0.461221 0.962113 0.633447 11.00000 0.01459 0.01404 = 0.02410 -0.00176 0.00253 0.00009 C31 1 0.446848 0.865875 0.610884 11.00000 0.01497 0.01850 = 0.03812 -0.01315 0.01124 -0.00485 AFIX 13 H31 2 0.379806 0.802139 0.618066 11.00000 -1.20000 AFIX 0 C32 1 0.423841 0.902749 0.578014 11.00000 0.01525 0.03123 = 0.03014 -0.01030 0.00665 -0.00247 AFIX 43 H32 2 0.406229 0.850851 0.561536 11.00000 -1.20000 AFIX 0 C33 1 0.428303 1.011074 0.571872 11.00000 0.00769 0.02720 = 0.02615 -0.00818 -0.00028 -0.00112 C34 1 0.707119 1.052798 0.602473 11.00000 0.00992 0.01456 = 0.01388 0.00333 -0.00059 -0.00482 C35 1 0.743417 0.945215 0.612931 11.00000 0.01635 0.01386 = 0.02031 -0.00086 0.00134 -0.00644 C36 1 0.608041 0.886062 0.629135 11.00000 0.01657 0.00920 = 0.03475 -0.00129 0.00994 -0.00206 C37 1 0.651030 0.810410 0.655541 11.00000 0.02295 0.01762 = 0.04243 0.01149 0.01546 0.00399 C38 1 0.745377 0.851200 0.679909 11.00000 0.03229 0.04238 = 0.04832 0.01983 0.00815 0.00489 AFIX 43 H38 2 0.779512 0.925979 0.679404 11.00000 -1.20000 AFIX 0 C39 1 0.790354 0.784854 0.704848 11.00000 0.03849 0.04702 = 0.05061 0.02187 0.01475 0.01195 AFIX 43 H39 2 0.855017 0.812544 0.721581 11.00000 -1.20000 AFIX 0 C40 1 0.736747 0.673808 0.704665 11.00000 0.04274 0.04657 = 0.05522 0.03126 0.01330 0.02107 AFIX 43 H40 2 0.768422 0.626149 0.721379 11.00000 -1.20000 AFIX 0 C41 1 0.643118 0.634368 0.681693 11.00000 0.03849 0.04702 = 0.05061 0.02187 0.01475 0.01195 AFIX 43 H41 2 0.607053 0.560039 0.682407 11.00000 -1.20000 AFIX 0 C42 1 0.599053 0.701326 0.657052 11.00000 0.05200 0.01730 = 0.05732 0.01256 0.03036 0.01412 AFIX 43 H42 2 0.532102 0.672917 0.640774 11.00000 -1.20000 AFIX 0 C43 1 0.896616 0.900480 0.608543 11.00000 0.01878 0.02610 = 0.02489 -0.00085 0.00318 0.00557 AFIX 43 H43 2 0.921732 0.828842 0.616207 11.00000 -1.20000 AFIX 0 C44 1 1.011240 0.962725 0.592781 11.00000 0.00985 0.02590 = 0.03051 -0.00520 0.00168 -0.00257 AFIX 43 H44 2 1.115459 0.932862 0.589459 11.00000 -1.20000 AFIX 0 C45 1 0.976017 1.068815 0.581680 11.00000 0.01204 0.02849 = 0.02397 -0.00148 0.00723 -0.00284 AFIX 43 H45 2 1.055886 1.109898 0.570763 11.00000 -1.20000 AFIX 0 C46 1 0.825789 1.113960 0.586528 11.00000 0.02440 0.01076 = 0.02249 0.00121 0.00222 -0.00273 AFIX 43 H46 2 0.802536 1.186209 0.579112 11.00000 -1.20000 AFIX 0 C47 1 0.378699 0.969856 0.664630 11.00000 0.01589 0.01669 = 0.02699 -0.00353 0.00389 0.00430 C48 1 0.277762 0.886223 0.675276 11.00000 0.02009 0.01437 = 0.02171 -0.00548 0.00591 -0.00152 AFIX 43 H48 2 0.249465 0.827350 0.661527 11.00000 -1.20000 AFIX 0 C49 1 0.217909 0.888612 0.706142 11.00000 0.03028 0.02025 = 0.02629 0.00399 0.01475 0.00135 AFIX 43 H49 2 0.150424 0.830877 0.713534 11.00000 -1.20000 AFIX 0 C50 1 0.257036 0.974626 0.725689 11.00000 0.04707 0.03430 = 0.02096 0.00451 0.00885 -0.00334 AFIX 43 H50 2 0.218176 0.975564 0.746816 11.00000 -1.20000 AFIX 0 C51 1 0.353285 1.060723 0.714869 11.00000 0.05233 0.02802 = 0.02119 0.00148 -0.00231 -0.00747 AFIX 43 H51 2 0.376354 1.121407 0.728347 11.00000 -1.20000 AFIX 0 C52 1 0.415055 1.058032 0.684670 11.00000 0.02647 0.01892 = 0.02435 0.00202 0.00057 -0.00371 AFIX 43 H52 2 0.482391 1.116128 0.677461 11.00000 -1.20000 AFIX 0 C53 1 0.412759 1.066527 0.540854 11.00000 0.01334 0.04731 = 0.02167 -0.00410 0.00017 0.00773 C54 1 0.468015 1.173930 0.536376 11.00000 0.02452 0.03954 = 0.02878 0.00138 -0.00002 0.01300 AFIX 43 H54 2 0.511319 1.213747 0.553754 11.00000 -1.20000 AFIX 0 C55 1 0.460497 1.223224 0.506888 11.00000 0.04026 0.05406 = 0.03030 0.00926 0.00285 0.02592 AFIX 43 H55 2 0.503004 1.295278 0.504010 11.00000 -1.20000 AFIX 0 C56 1 0.392072 1.168872 0.481720 11.00000 0.05080 0.06983 = 0.03007 0.00554 -0.00124 0.03594 AFIX 43 H56 2 0.384909 1.203884 0.461666 11.00000 -1.20000 AFIX 0 C57 1 0.333629 1.062771 0.485762 11.00000 0.03901 0.09631 = 0.02334 -0.01919 -0.01756 0.02896 AFIX 43 H57 2 0.287277 1.024934 0.468325 11.00000 -1.20000 AFIX 0 C58 1 0.342156 1.010801 0.515238 11.00000 0.02327 0.05554 = 0.03775 -0.01417 -0.00777 0.01000 AFIX 43 H58 2 0.300557 0.938407 0.517923 11.00000 -1.20000 AFIX 0 O1 3 0.149573 0.696514 0.615902 11.00000 0.02030 0.01452 = 0.02294 0.00031 -0.00104 0.00003 O2 3 0.441819 1.192234 0.615244 11.00000 0.01519 0.01828 = 0.02642 0.00366 0.00152 0.00427 P1 4 0.095753 0.582889 0.607475 11.00000 0.01193 0.01287 = 0.01806 0.00178 -0.00040 0.00192 P2 4 0.497970 1.079731 0.607363 11.00000 0.01040 0.01546 = 0.01976 -0.00041 0.00220 0.00145 HKLF 4 REM MR280_a.res in P2(1)2(1)2(1) REM R1 = 0.0631 for 7445 Fo > 4sig(Fo) and 0.0685 for all 8076 data REM 543 parameters refined using 0 restraints END WGHT 0.0298 10.8145 REM Highest difference peak 0.854, deepest hole -0.566, 1-sigma level 0.073 Q1 1 0.6950 0.6449 0.6941 11.00000 0.05 0.63 Q2 1 0.7888 0.7136 0.7153 11.00000 0.05 0.56 Q3 1 0.3029 0.3364 0.6105 11.00000 0.05 0.47 Q4 1 0.2908 0.5839 0.6103 11.00000 0.05 0.40 Q5 1 0.8968 1.0150 0.6032 11.00000 0.05 0.38 Q6 1 0.2997 0.5014 0.6052 11.00000 0.05 0.35 Q7 1 -0.4816 0.3401 0.6162 11.00000 0.05 0.32 Q8 1 0.8109 0.8412 0.7132 11.00000 0.05 0.32 Q9 1 -0.4860 0.5173 0.5986 11.00000 0.05 0.31 Q10 1 0.3908 0.9587 0.5929 11.00000 0.05 0.31 Q11 1 1.0989 0.8278 0.6101 11.00000 0.05 0.30 Q12 1 0.4551 1.0464 0.5867 11.00000 0.05 0.30 Q13 1 0.5933 0.6265 0.6689 11.00000 0.05 0.30 Q14 1 -0.0169 0.5628 0.6074 11.00000 0.05 0.29 Q15 1 0.2255 0.4965 0.7247 11.00000 0.05 0.29 Q16 1 0.7240 1.0753 0.5861 11.00000 0.05 0.29 Q17 1 0.6493 0.9968 0.5721 11.00000 0.05 0.28 Q18 1 -0.1250 0.5122 0.6213 11.00000 0.05 0.28 Q19 1 0.6202 1.0696 0.6060 11.00000 0.05 0.27 Q20 1 0.1322 0.5613 0.5853 11.00000 0.05 0.27 ; _shelx_res_checksum 65628 _shelx_hkl_file ; -1 0 0 0.40 0.30 1 0 0 -0.20 0.30 2 0 0 949.60 49.20 -2 0 0 984.30 49.20 3 0 0 2.10 1.10 -3 0 0 3.10 1.00 4 0 0 309.57 16.70 5 0 0 1.30 1.40 6 0 0 28.50 3.90 6 0 0 27.70 2.70 7 0 0 1.70 2.40 7 0 0 0.50 1.40 8 0 0 481.35 25.00 8 0 0 466.15 26.80 9 0 0 -5.30 3.40 10 0 0 116.79 10.60 1 -1 0 901.51 47.10 -1 1 0 909.31 47.10 1 -1 0 945.61 47.20 -1 1 0 967.30 47.30 -2 1 0 9862.21 506.25 2 -1 0 9999.00 506.75 3 1 0 2191.68 111.69 3 -1 0 2230.18 111.49 -3 1 0 2209.78 111.79 -3 -1 0 2205.48 111.69 3 -1 0 2181.48 111.89 4 1 0 80.79 5.20 4 -1 0 79.79 4.60 4 -1 0 78.39 5.40 -4 -1 0 69.49 4.90 5 -1 0 438.26 22.30 5 1 0 422.96 22.80 5 -1 0 420.76 22.90 6 -1 0 259.67 13.90 6 -1 0 230.58 12.90 6 1 0 222.88 13.60 7 -1 0 5.30 1.80 7 -1 0 11.90 3.10 7 1 0 3.00 2.70 8 -1 0 83.29 7.60 8 1 0 65.99 6.80 8 -1 0 71.89 5.30 9 -1 0 -4.40 4.80 9 1 0 4.30 4.30 10 -1 0 1.90 5.30 10 1 0 -8.00 4.60 0 2 0 9992.60 486.45 0 -2 0 9107.39 486.35 1 2 0 0.70 3.20 1 -2 0 -2.20 3.80 -1 2 0 2.00 4.70 -1 -2 0 2.20 2.80 -2 2 0 760.02 38.70 2 -2 0 758.42 38.40 2 -2 0 737.83 38.60 -2 2 0 755.52 38.40 -3 2 0 701.23 35.80 -3 2 0 668.23 36.30 3 -2 0 687.33 36.30 3 -2 0 691.43 35.90 3 2 0 757.22 36.00 -4 2 0 5.00 1.10 4 2 0 4.90 1.60 4 -2 0 2.90 1.70 4 -2 0 6.30 1.40 5 -2 0 210.08 11.50 5 -2 0 207.88 12.10 6 -2 0 35.50 3.40 6 -2 0 35.60 4.00 7 -2 0 295.17 15.60 7 -2 0 271.17 17.10 7 2 0 284.87 16.40 8 2 0 125.69 9.20 8 -2 0 127.69 10.00 8 -2 0 107.49 7.70 9 -2 0 8.20 4.70 9 -2 0 9.50 2.80 9 2 0 11.50 4.10 10 -2 0 71.59 11.40 0 -3 0 0.60 0.60 0 3 0 0.20 0.60 0 -3 0 0.70 0.70 0 3 0 0.20 0.60 1 3 0 -0.40 0.60 -1 3 0 1.00 0.80 1 -3 0 1.10 0.90 -1 3 0 0.80 0.70 1 -3 0 1.20 0.90 1 3 0 2.90 0.70 2 -3 0 327.27 18.00 -2 3 0 333.57 18.00 2 -3 0 332.77 17.90 2 3 0 372.16 17.70 -2 3 0 341.67 17.80 3 3 0 618.54 30.50 3 -3 0 561.84 30.60 3 -3 0 547.95 30.80 -3 3 0 599.74 30.50 3 3 0 627.44 30.50 4 -3 0 4.60 1.40 4 3 0 6.50 1.60 -4 3 0 8.90 1.50 4 -3 0 5.00 1.90 5 -3 0 866.21 45.00 5 -3 0 902.81 45.60 5 3 0 843.22 45.20 -5 3 0 875.61 44.60 6 -3 0 391.66 20.60 6 -3 0 340.17 19.60 7 -3 0 46.90 6.30 7 -3 0 53.89 4.60 7 3 0 49.70 5.40 8 3 0 0.50 2.90 8 -3 0 1.50 3.90 8 -3 0 -3.70 2.40 9 3 0 23.50 4.50 9 -3 0 18.40 5.90 0 -4 0 2084.39 105.69 0 -4 0 2094.69 105.69 0 4 0 2082.69 105.69 1 -4 0 19.60 2.10 -1 4 0 17.30 1.90 -1 4 0 17.60 1.90 1 4 0 18.60 1.70 1 4 0 17.60 1.70 1 -4 0 21.40 2.00 -1 -4 0 22.50 1.80 -2 4 0 14.70 1.90 2 -4 0 15.00 2.30 2 -4 0 17.70 2.30 2 4 0 17.20 1.70 -2 -4 0 19.60 1.80 3 -4 0 87.09 5.60 3 -4 0 89.29 5.90 3 4 0 89.29 5.20 4 4 0 8.30 1.60 4 -4 0 9.30 1.90 4 4 0 9.80 1.80 4 -4 0 8.70 2.30 5 -4 0 306.87 16.90 5 -4 0 322.27 17.60 5 4 0 305.07 17.00 6 -4 0 -2.70 1.70 6 -4 0 0.90 2.70 6 4 0 -1.20 2.10 7 -4 0 689.33 37.70 7 4 0 655.23 36.50 7 -4 0 725.53 36.60 8 -4 0 20.10 3.50 8 4 0 22.10 3.80 8 -4 0 23.10 5.40 9 -4 0 85.89 8.10 9 -4 0 86.49 10.50 0 5 0 3.30 1.10 0 5 0 4.10 1.10 0 -5 0 3.40 1.10 0 -5 0 3.90 1.20 -1 -5 0 41.20 3.00 1 5 0 41.20 3.00 1 5 0 40.10 3.00 1 -5 0 41.50 3.70 1 -5 0 44.80 3.30 2 5 0 37.70 2.80 2 -5 0 40.70 3.30 2 5 0 33.50 2.70 -2 -5 0 36.40 2.90 2 -5 0 36.60 3.10 3 5 0 1481.95 71.99 3 -5 0 1365.96 72.29 3 -5 0 1389.76 72.49 4 5 0 23.00 2.30 5 -5 0 205.18 12.20 5 -5 0 198.88 11.70 6 -5 0 2.40 2.70 6 -5 0 -1.60 2.30 6 5 0 3.50 2.30 7 -5 0 2.90 3.00 7 5 0 4.50 2.50 8 -5 0 15.70 5.10 8 -5 0 23.10 3.90 9 -5 0 18.00 4.40 9 -5 0 19.40 6.20 0 -6 0 996.50 50.59 0 -6 0 975.20 50.99 -1 -6 0 310.27 16.30 1 6 0 300.97 16.20 1 6 0 299.07 16.30 1 -6 0 309.57 16.50 1 -6 0 309.57 16.40 -2 -6 0 72.19 4.60 2 -6 0 64.79 4.70 2 6 0 66.19 4.40 2 6 0 73.29 4.50 2 -6 0 68.19 4.70 3 6 0 44.20 3.50 3 -6 0 63.29 4.40 3 6 0 48.60 3.50 3 -6 0 55.99 4.30 4 -6 0 65.89 5.30 4 -6 0 54.29 4.70 5 -6 0 4.90 2.60 5 6 0 5.30 2.20 5 -6 0 2.00 2.20 6 -6 0 1.00 2.90 6 -6 0 0.10 2.70 6 6 0 0.20 2.10 7 -6 0 240.08 16.50 7 6 0 258.07 14.80 7 -6 0 249.48 15.00 8 -6 0 62.09 6.80 8 -6 0 59.79 8.90 9 -6 0 6.80 4.70 9 -6 0 6.20 6.30 0 -7 0 6.80 1.50 0 -7 0 3.60 1.50 1 -7 0 176.98 9.40 1 -7 0 166.98 9.50 -1 -7 0 144.59 9.90 2 -7 0 162.48 9.10 2 -7 0 161.28 9.10 -2 -7 0 137.79 8.90 3 -7 0 151.68 8.60 3 7 0 131.09 7.80 3 -7 0 136.19 8.50 -3 -7 0 127.49 8.20 4 7 0 20.70 2.40 4 -7 0 31.60 3.80 5 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347.57 20.00 7 -2 -4 365.26 19.70 7 -2 -4 371.66 20.80 7 2 4 341.67 20.30 8 -2 4 190.68 11.00 8 2 -4 164.18 11.30 8 2 4 167.18 11.80 8 -2 -4 189.08 12.10 8 -2 -4 181.18 10.60 9 2 -4 60.09 6.40 9 -2 4 65.59 6.10 9 -2 4 59.39 8.80 9 -2 -4 68.49 7.70 9 2 4 56.19 8.10 9 -2 -4 61.09 6.20 10 -2 4 255.17 17.60 10 -2 -4 222.58 17.00 10 2 4 251.87 17.00 0 3 4 6.80 1.00 0 -3 4 6.60 1.00 0 -3 4 8.20 1.20 0 3 -4 5.70 0.90 0 -3 -4 7.50 1.10 0 3 4 7.00 1.10 0 3 -4 8.30 1.10 -1 3 4 109.09 6.00 1 -3 4 101.19 6.10 1 3 -4 108.29 5.90 -1 -3 -4 118.69 6.10 1 3 -4 106.59 5.70 -1 3 4 103.69 6.10 1 -3 4 108.89 6.10 1 3 4 114.89 6.00 1 -3 -4 111.19 6.10 -1 3 -4 101.99 6.10 -1 -3 4 100.19 5.80 -1 -3 4 113.19 5.70 1 -3 -4 105.99 6.10 -1 3 -4 107.09 6.10 -2 3 4 462.85 24.20 -2 3 4 458.35 24.40 2 -3 4 467.15 24.40 2 -3 4 474.35 24.30 -2 3 -4 476.15 24.20 2 -3 -4 451.15 24.30 2 -3 -4 461.65 24.30 -2 3 -4 459.15 24.40 2 3 4 499.45 24.20 -3 3 4 346.57 18.20 3 3 -4 346.67 17.90 3 3 -4 351.66 18.00 3 -3 -4 340.97 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8 -2 -7 70.89 6.40 9 -2 7 11.80 5.50 9 -2 7 18.50 4.70 9 -2 -7 6.10 4.70 9 2 7 10.80 4.80 0 3 -7 1.50 0.70 0 -3 7 3.30 0.80 0 -3 7 1.70 0.80 0 -3 -7 1.90 0.90 0 3 -7 2.50 0.70 0 3 7 2.50 0.80 1 -3 7 118.79 6.50 -1 3 7 124.39 6.50 -1 -3 -7 114.59 6.50 1 3 -7 101.29 6.00 -1 3 7 128.39 6.50 1 3 -7 111.99 6.20 1 3 7 110.39 6.40 1 -3 -7 123.89 6.60 -1 3 -7 110.99 6.50 -1 -3 7 102.79 5.90 1 -3 -7 122.99 6.40 -1 -3 7 102.49 6.10 -2 3 7 2212.08 119.89 -2 3 7 2213.68 119.79 2 -3 7 2565.14 119.99 2 3 -7 2188.18 119.49 2 -3 7 2585.74 120.19 -2 3 -7 2624.54 120.19 2 -3 -7 2197.58 119.79 2 3 7 2177.18 119.79 -2 3 -7 2704.53 119.99 2 -3 -7 2188.38 119.89 3 3 -7 615.04 34.60 3 -3 7 676.63 35.50 3 -3 7 649.93 35.20 3 3 -7 656.83 34.60 -3 3 -7 724.63 35.40 3 -3 -7 768.82 35.90 4 -3 7 353.66 17.60 4 -3 7 358.86 18.20 -4 3 7 334.87 17.30 4 3 -7 291.17 17.00 4 -3 -7 341.27 17.40 4 3 7 290.17 17.60 5 3 -7 220.88 12.50 5 -3 7 227.18 13.70 5 -3 7 224.68 12.90 5 3 7 233.08 13.20 5 -3 -7 256.27 13.40 5 -3 -7 225.48 12.70 6 -3 7 26.50 3.10 6 -3 7 18.20 3.60 6 -3 -7 20.60 3.10 6 -3 -7 24.10 3.80 7 -3 7 45.20 4.60 7 -3 7 39.10 6.20 7 3 -7 43.50 4.10 7 3 7 49.20 5.60 7 -3 -7 45.30 4.40 7 -3 -7 53.29 5.60 8 -3 7 47.90 5.40 8 -3 7 48.10 7.60 8 3 -7 64.49 5.60 8 -3 -7 59.59 6.40 8 -3 -7 49.20 4.80 8 3 7 62.29 6.70 9 -3 7 191.38 13.10 9 -3 7 212.58 15.90 9 -3 -7 222.18 14.80 9 3 7 239.58 14.40 0 4 7 111.39 6.40 0 -4 7 111.89 6.40 0 -4 -7 110.99 6.50 0 4 7 109.59 6.40 0 4 -7 107.49 6.30 0 -4 7 109.09 6.20 0 4 -7 125.09 6.50 1 -4 7 65.19 4.20 -1 -4 -7 57.99 4.00 -1 4 7 70.29 4.10 1 -4 7 64.29 4.10 1 4 -7 60.19 3.90 -1 4 7 70.09 4.40 1 4 -7 58.79 3.60 -1 4 -7 69.09 4.20 1 4 7 59.49 4.00 1 -4 -7 69.29 4.30 -1 -4 7 57.29 3.80 -1 -4 7 57.29 3.60 -1 4 -7 62.79 4.10 1 -4 -7 66.29 4.10 2 -4 7 452.25 21.50 2 -4 7 439.76 21.60 2 4 -7 393.66 20.90 -2 -4 -7 364.46 21.30 2 -4 -7 414.16 22.00 2 4 7 368.56 21.20 2 -4 -7 410.76 21.30 3 -4 7 729.93 34.20 3 -4 7 719.23 34.00 3 -4 -7 566.94 33.70 3 -4 -7 592.94 33.90 4 -4 7 253.87 13.40 4 4 -7 232.98 12.70 4 4 -7 229.28 12.60 4 -4 7 255.07 13.90 4 -4 -7 231.18 13.20 4 -4 -7 242.18 13.60 5 -4 7 5.60 1.80 5 -4 7 3.00 2.40 5 4 -7 1.40 1.40 5 -4 -7 2.80 2.00 5 -4 -7 2.60 1.60 5 4 7 5.90 1.90 6 4 -7 9.20 2.00 6 -4 7 7.50 2.50 6 -4 7 9.10 2.90 6 -4 -7 12.50 3.00 6 4 7 7.60 2.90 6 -4 -7 7.30 2.20 7 -4 7 194.08 12.00 7 -4 7 178.68 14.60 7 4 -7 188.28 11.20 7 -4 -7 202.38 11.80 7 4 7 223.48 12.90 7 -4 -7 184.28 13.50 8 -4 7 268.17 16.50 8 -4 7 268.87 17.70 8 4 7 300.87 17.10 8 -4 -7 257.07 16.90 8 -4 -7 260.77 15.60 9 -4 7 15.00 4.20 9 -4 7 15.00 5.60 9 -4 -7 11.90 5.20 9 4 7 13.50 4.70 9 -4 -7 12.90 4.20 0 5 -7 29.70 2.60 0 -5 7 33.70 2.50 0 -5 -7 31.90 2.80 0 5 -7 30.80 2.70 0 -5 7 27.60 2.60 1 -5 7 33.60 2.60 -1 -5 -7 27.90 2.70 1 5 -7 21.00 2.40 1 5 -7 23.60 2.20 1 -5 7 33.80 2.80 1 -5 -7 24.50 2.50 -1 5 -7 32.80 2.80 -1 -5 7 24.30 2.10 1 5 7 24.30 2.40 2 5 -7 164.38 9.40 2 5 -7 172.28 9.20 2 -5 7 206.48 10.10 -2 -5 -7 163.38 9.90 2 -5 -7 182.88 10.10 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275.37 15.40 2 -6 7 197.78 10.80 -2 -6 -7 190.38 10.80 2 6 -7 189.68 10.10 2 -6 7 183.68 10.70 2 6 -7 188.08 10.40 -2 -6 7 185.98 10.10 2 -6 -7 189.58 10.70 2 -6 -7 182.98 10.80 3 6 -7 53.39 3.30 3 6 -7 51.89 3.70 3 -6 7 54.59 4.40 3 -6 7 58.49 4.30 3 -6 -7 48.00 4.40 3 -6 -7 45.80 4.20 4 6 -7 79.19 4.90 4 6 -7 84.79 4.80 4 -6 7 80.99 6.40 4 6 -7 77.29 4.80 4 -6 7 86.19 6.20 4 -6 -7 81.99 6.30 4 -6 -7 84.99 5.80 5 6 -7 1245.18 60.99 5 -6 7 1159.88 62.29 5 -6 7 1195.28 61.89 5 -6 -7 1200.88 61.79 5 -6 -7 1163.68 62.19 6 -6 7 66.19 7.10 6 -6 7 76.39 6.50 6 6 -7 68.29 5.00 6 6 7 63.69 5.80 6 -6 -7 70.89 6.60 6 -6 -7 63.19 6.00 7 -6 7 179.28 12.40 7 -6 7 181.98 13.30 7 -6 -7 183.68 11.60 7 6 7 185.98 11.70 7 -6 -7 176.78 13.10 8 -6 7 18.70 4.70 8 -6 7 15.30 6.10 8 -6 -7 15.50 5.50 8 6 7 10.20 4.00 8 -6 -7 11.80 4.30 9 -6 7 69.09 8.60 9 -6 7 72.49 10.30 9 -6 -7 62.09 7.50 9 -6 -7 49.90 8.70 0 -7 7 37.30 3.40 0 -7 7 34.00 3.20 0 -7 -7 34.70 3.10 -1 -7 -7 18.30 2.50 1 -7 7 20.60 2.50 1 -7 7 16.20 2.40 -1 -7 7 17.70 2.70 1 -7 -7 16.60 2.20 1 -7 -7 15.00 2.30 2 -7 7 82.29 5.60 2 7 -7 81.49 5.00 -2 -7 -7 83.29 5.70 2 -7 7 86.59 5.60 2 -7 -7 76.59 5.70 2 -7 -7 81.19 5.60 -2 -7 7 83.29 5.10 3 -7 7 181.38 11.10 3 -7 7 177.48 10.90 3 7 -7 181.08 10.20 3 7 -7 187.08 9.90 -3 -7 -7 194.08 11.00 3 -7 -7 186.18 11.00 3 -7 -7 185.68 11.20 4 7 -7 147.99 8.20 4 7 -7 143.49 8.40 4 -7 7 158.78 10.00 4 -7 7 152.48 9.60 4 -7 -7 147.29 9.30 4 -7 -7 143.29 9.70 5 -7 7 24.20 3.70 5 7 -7 30.50 2.80 5 -7 7 26.90 4.40 5 -7 -7 35.60 4.90 5 -7 -7 27.10 3.90 6 -7 7 62.69 7.40 6 -7 7 63.39 6.60 6 -7 -7 79.69 6.60 6 -7 -7 83.09 7.20 6 7 7 48.20 5.60 7 -7 7 37.20 6.20 7 -7 7 41.40 6.20 7 -7 -7 39.50 6.40 7 -7 -7 31.90 5.50 7 7 7 36.30 5.30 8 -7 7 16.20 5.00 8 -7 7 18.70 6.40 8 -7 -7 14.40 5.80 8 -7 -7 9.90 4.80 0 -8 7 682.43 36.20 0 -8 -7 745.23 36.70 0 -8 7 659.93 36.30 1 -8 7 66.79 5.20 1 -8 7 75.99 5.20 -1 -8 -7 71.39 5.30 1 -8 -7 72.49 5.40 -1 -8 7 73.49 5.20 -1 -8 7 71.69 5.10 2 -8 7 182.38 10.90 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3 0 -8 372.06 19.90 -3 0 8 370.66 19.90 3 0 8 391.56 20.40 3 0 -8 408.66 19.70 3 0 8 379.86 19.90 4 0 8 0.30 1.00 4 0 8 1.60 1.50 -4 0 8 0.20 1.30 4 0 -8 1.50 1.20 5 0 8 14.70 2.50 5 0 -8 11.50 2.70 5 0 8 16.60 2.80 5 0 -8 15.60 1.80 6 0 -8 1.30 1.40 6 0 -8 3.30 2.00 6 0 8 3.50 2.30 6 0 8 -1.20 1.40 7 0 -8 6.10 1.60 7 0 8 7.30 2.00 7 0 8 7.30 3.60 7 0 -8 11.30 2.70 8 0 8 258.17 17.30 8 0 -8 280.57 15.70 8 0 8 262.37 15.00 8 0 -8 265.17 15.30 9 0 -8 10.70 4.00 9 0 8 4.40 4.50 10 0 8 0.50 5.50 0 -1 -8 3.10 0.80 0 -1 8 4.60 0.80 0 1 8 3.50 0.80 0 1 8 3.40 0.70 0 1 -8 3.60 0.70 1 -1 8 1429.26 73.49 1 1 -8 1510.35 73.29 -1 1 8 1375.56 73.39 1 1 -8 1507.15 73.19 1 -1 8 1402.86 73.39 -1 1 8 1440.16 73.39 -1 1 -8 1476.05 73.49 -1 -1 8 1445.36 73.29 -1 -1 8 1497.65 73.19 1 -1 -8 1415.26 73.39 -1 1 -8 1450.65 73.39 1 1 8 1434.46 73.39 -2 1 8 84.89 4.80 2 1 -8 89.59 4.70 -2 1 8 93.79 4.80 2 -1 8 87.59 5.00 -2 1 8 83.69 5.00 2 -1 8 87.09 5.30 -2 1 -8 86.29 4.90 2 -1 -8 85.39 4.90 -2 1 -8 85.49 5.20 2 -1 -8 82.39 5.00 3 -1 8 186.48 10.00 3 1 -8 187.18 9.80 3 -1 8 185.18 10.50 -3 1 8 189.28 10.10 -3 1 -8 183.08 9.90 3 -1 -8 183.08 9.90 3 1 8 184.58 9.90 -3 -1 8 188.38 9.90 3 -1 -8 184.58 10.10 3 1 8 180.58 10.40 4 -1 8 1081.99 54.09 4 1 -8 1107.59 53.99 4 -1 8 1047.90 54.59 4 1 8 1038.00 53.79 -4 -1 8 1069.69 53.99 4 1 8 1028.40 54.49 -4 1 -8 1072.59 53.79 4 -1 -8 1044.70 53.89 4 -1 -8 1025.30 54.19 5 -1 8 83.39 6.30 5 1 -8 82.89 5.50 5 -1 8 82.99 5.30 5 -1 -8 84.79 5.20 5 1 8 82.99 6.10 5 1 8 86.99 5.10 5 -1 -8 87.69 5.70 6 1 -8 253.77 14.40 6 -1 8 257.47 15.10 6 -1 8 276.87 14.30 6 -1 -8 255.67 14.60 6 1 8 251.47 13.80 6 -1 -8 259.07 13.90 6 1 8 251.07 15.00 7 1 -8 768.42 41.00 7 1 -8 750.32 40.00 7 -1 8 822.72 40.80 7 -1 8 794.42 42.10 7 1 8 791.62 40.40 7 -1 -8 820.72 41.40 7 1 8 736.53 41.70 7 -1 -8 773.32 40.40 8 1 -8 22.10 3.30 8 -1 8 23.00 3.30 8 -1 8 19.60 5.20 8 1 8 19.50 2.70 8 1 8 11.90 4.20 8 -1 -8 20.40 2.80 8 -1 -8 22.10 4.10 9 -1 8 159.58 10.90 9 -1 8 184.78 13.60 9 1 8 181.28 13.40 9 -1 -8 172.18 12.50 10 -1 8 21.10 6.30 10 1 8 14.80 5.80 -1 2 8 497.95 26.90 1 -2 8 516.35 27.10 1 -2 8 511.55 27.00 1 2 -8 604.84 26.90 -1 2 8 524.15 27.00 -1 2 -8 485.05 27.00 1 -2 -8 490.25 27.00 -1 -2 8 584.14 26.80 -1 2 -8 511.85 27.00 2 -2 8 788.82 42.00 -2 2 8 854.01 41.80 2 -2 8 799.92 41.80 -2 2 8 834.22 41.70 -2 2 -8 792.02 41.90 2 -2 -8 844.72 41.80 -2 2 -8 815.22 41.70 2 -2 -8 801.32 41.70 3 2 -8 481.75 25.00 3 -2 8 465.35 26.30 -3 2 8 501.95 25.20 3 -2 8 483.75 25.50 -3 2 8 481.65 25.60 3 -2 -8 491.25 25.50 -3 2 -8 501.75 25.30 3 2 8 499.25 25.20 -3 -2 8 499.65 25.00 3 -2 -8 489.05 25.40 4 -2 8 574.34 31.40 -4 2 8 602.04 30.40 4 2 -8 579.34 30.50 4 -2 8 600.84 30.80 -4 2 8 600.24 30.40 4 2 8 605.24 30.50 4 -2 -8 606.84 31.10 4 -2 -8 541.15 31.10 4 2 8 642.94 31.30 -4 2 -8 577.94 30.60 -4 -2 8 599.84 30.50 5 2 -8 325.77 17.40 5 -2 8 319.27 18.40 5 -2 8 341.57 17.70 -5 -2 8 328.67 17.50 5 -2 -8 329.07 17.50 5 -2 -8 332.17 17.90 -5 2 -8 322.07 17.20 5 2 8 338.97 17.20 5 2 8 320.27 18.20 6 -2 8 67.49 4.70 6 -2 8 59.19 5.80 6 -2 -8 48.90 4.90 6 -2 -8 51.79 4.30 6 2 8 61.69 5.50 6 2 8 59.99 4.50 7 2 -8 181.98 11.00 7 -2 8 180.78 12.60 7 -2 8 193.38 11.10 7 2 8 178.28 12.00 7 2 8 173.58 10.10 7 -2 -8 191.18 10.70 7 -2 -8 184.88 11.70 8 -2 8 287.27 17.20 8 -2 8 302.87 19.40 8 2 -8 283.67 17.20 8 -2 -8 328.57 16.90 8 2 8 286.07 18.20 8 -2 -8 350.06 18.30 9 -2 8 -1.70 4.70 9 2 8 2.00 4.40 9 -2 -8 7.10 3.80 0 3 -8 1.70 0.80 0 3 -8 0.50 0.80 0 -3 -8 0.20 0.90 0 -3 8 0.10 0.70 0 -3 8 0.00 0.70 0 3 8 -0.20 0.70 1 -3 8 629.24 33.70 -1 3 8 662.43 33.70 1 -3 8 609.34 33.70 1 3 -8 723.13 33.30 -1 -3 -8 636.64 33.70 -1 3 8 630.34 33.70 1 -3 -8 606.74 33.70 1 3 8 647.54 33.70 -1 3 -8 642.84 33.70 -1 3 -8 609.74 33.70 -1 -3 8 719.53 33.20 -1 -3 8 743.93 33.50 2 -3 8 1423.66 71.99 -2 3 8 1368.46 72.09 2 -3 8 1390.56 72.19 -2 3 8 1416.56 71.89 -2 3 -8 1487.95 71.99 2 -3 -8 1398.96 71.99 2 3 8 1454.95 72.09 2 -3 -8 1400.36 72.09 -2 3 -8 1384.76 72.09 3 -3 8 173.68 10.00 3 -3 8 178.88 9.70 -3 3 8 173.98 9.40 3 -3 -8 160.58 9.60 4 -3 8 1664.93 86.29 4 -3 8 1677.93 85.89 -4 3 8 1674.13 85.49 4 3 -8 1703.03 85.29 4 -3 -8 1681.63 85.99 4 -3 -8 1664.43 85.69 4 3 8 1715.53 86.09 -5 3 8 475.15 23.50 5 -3 8 444.76 24.70 5 3 -8 430.16 23.60 5 -3 8 427.96 24.00 -5 3 8 454.25 23.50 5 3 8 436.66 24.40 5 -3 -8 496.65 24.40 5 -3 -8 455.25 23.90 6 3 -8 104.59 7.00 6 -3 -8 111.49 7.20 6 3 8 105.99 7.90 6 -3 -8 136.09 8.00 7 -3 8 46.60 6.10 7 -3 8 38.00 4.40 7 3 -8 48.20 4.10 7 3 8 43.20 5.20 7 -3 -8 42.30 4.30 7 -3 -8 46.40 5.50 8 -3 8 105.99 9.70 8 3 8 91.79 8.10 8 -3 -8 84.89 7.90 8 -3 -8 92.49 6.60 9 -3 8 569.44 30.70 9 -3 8 542.55 32.70 9 3 8 570.04 31.80 9 -3 -8 541.45 31.70 0 4 8 675.03 32.90 0 4 8 625.94 32.90 0 -4 8 626.34 32.80 0 -4 -8 646.24 33.00 0 -4 8 610.84 32.60 0 4 -8 646.34 32.80 0 4 -8 633.34 32.70 1 4 -8 113.99 6.70 1 -4 8 119.69 6.90 -1 -4 -8 123.79 7.00 1 4 -8 116.89 6.40 -1 4 8 118.29 6.80 1 -4 8 113.69 6.90 -1 4 -8 115.99 6.90 -1 -4 8 117.79 6.40 -1 -4 8 120.79 6.60 1 -4 -8 121.39 7.00 1 4 8 129.99 6.90 -1 4 -8 119.09 6.90 2 -4 8 506.75 26.90 -2 -4 -8 526.35 26.90 2 -4 8 508.65 26.80 2 -4 -8 511.75 26.80 3 -4 8 446.66 23.50 3 -4 8 446.26 23.30 3 -4 -8 440.36 23.30 3 -4 -8 423.66 23.10 4 -4 8 682.13 36.50 4 4 -8 691.13 35.30 4 -4 8 683.63 36.10 4 4 -8 701.33 35.30 4 -4 -8 694.93 36.20 4 -4 -8 696.83 35.90 5 4 -8 662.13 34.00 5 4 -8 653.53 33.90 5 -4 8 649.34 35.20 5 -4 8 672.03 34.60 5 -4 -8 674.33 34.90 5 4 8 638.74 34.80 5 -4 -8 670.53 34.50 6 -4 8 144.29 9.90 6 4 -8 139.59 8.50 6 -4 8 148.69 9.30 6 4 8 140.79 9.50 6 -4 -8 143.79 8.90 6 -4 -8 152.48 9.80 7 4 -8 553.84 30.10 7 -4 8 567.04 30.80 7 -4 -8 580.74 31.30 7 -4 -8 589.94 30.40 7 4 8 563.04 31.30 8 -4 8 227.68 15.50 8 -4 8 225.78 14.00 8 4 8 230.18 14.60 8 -4 -8 239.38 13.60 8 -4 -8 218.78 15.20 9 -4 8 -0.20 5.70 9 -4 8 5.10 4.20 9 4 8 1.30 4.60 9 -4 -8 4.70 4.60 9 -4 -8 -3.60 3.30 0 -5 8 3.60 1.20 0 5 -8 5.90 1.30 0 -5 8 6.20 1.30 0 5 -8 5.70 1.40 0 -5 -8 8.50 2.10 1 5 -8 530.75 26.30 1 -5 8 513.35 26.50 -1 -5 -8 503.65 26.50 1 -5 8 489.65 26.40 1 5 -8 509.35 26.00 -1 -5 8 502.85 26.20 1 -5 -8 493.45 26.50 -1 5 -8 499.45 26.50 -1 -5 8 510.55 26.00 2 5 -8 99.79 5.40 2 -5 8 96.49 6.20 2 5 -8 99.89 5.80 2 -5 8 102.59 6.20 -2 -5 8 99.49 5.50 2 -5 -8 101.39 6.40 2 -5 -8 99.49 6.20 3 5 -8 223.78 11.00 3 -5 8 198.88 11.60 3 -5 8 196.58 11.70 3 -5 -8 201.78 11.80 3 -5 -8 204.38 11.60 4 -5 8 43.20 3.80 4 -5 -8 32.50 3.90 4 -5 -8 31.70 3.40 5 5 -8 239.28 12.30 5 5 -8 229.78 12.20 5 -5 8 243.08 14.10 5 -5 8 240.38 13.40 5 5 8 227.08 13.30 5 -5 -8 219.88 13.50 5 -5 -8 216.48 13.10 6 -5 8 968.90 52.59 6 5 -8 1026.80 51.99 6 -5 8 960.10 53.39 6 5 8 993.00 52.79 6 -5 -8 1050.69 52.49 6 -5 -8 1056.89 53.09 7 -5 8 168.48 11.90 7 -5 8 178.08 12.10 7 5 8 147.99 10.70 7 -5 -8 165.08 10.20 7 -5 -8 142.49 12.40 8 -5 8 14.60 5.30 8 -5 8 14.60 3.90 8 -5 -8 5.60 3.40 8 -5 -8 13.30 5.30 8 5 8 13.70 4.00 9 -5 8 69.79 10.30 9 -5 8 60.79 8.10 9 5 8 57.49 7.90 9 -5 -8 70.19 6.90 9 -5 -8 63.29 9.50 0 -6 -8 70.99 4.50 0 -6 8 63.49 4.30 0 -6 8 64.59 4.60 0 6 -8 62.49 4.40 1 6 -8 83.99 5.20 1 -6 8 76.19 6.40 1 -6 8 90.79 5.50 -1 -6 -8 97.49 5.70 -1 -6 8 86.99 5.20 -1 -6 8 83.29 5.40 1 -6 -8 89.99 5.70 2 -6 8 106.29 6.60 2 6 -8 101.09 5.90 -2 -6 -8 105.29 6.60 2 -6 8 108.39 6.60 2 6 -8 103.99 6.30 2 -6 -8 103.59 6.80 2 -6 -8 114.09 6.70 -2 -6 8 108.19 6.00 3 -6 8 17.60 2.70 3 6 -8 20.70 1.70 3 6 -8 16.20 2.30 3 -6 8 20.50 2.90 3 -6 -8 13.80 2.40 3 -6 -8 20.20 3.00 4 -6 8 1221.28 64.29 4 6 -8 1258.27 62.99 4 6 -8 1226.88 63.09 4 -6 8 1191.38 64.09 4 -6 -8 1256.87 64.29 4 -6 -8 1283.27 63.89 5 6 -8 41.00 3.20 5 -6 -8 55.89 5.30 5 -6 -8 45.20 4.40 6 -6 8 18.50 3.90 6 -6 8 17.10 4.50 6 6 8 14.90 3.30 6 -6 -8 13.60 3.20 6 -6 -8 16.10 3.80 7 -6 8 122.09 11.10 7 -6 8 157.48 10.00 7 -6 -8 117.09 10.70 7 6 8 117.19 9.20 7 -6 -8 135.59 9.20 8 -6 8 194.88 14.00 8 -6 8 204.08 15.80 8 6 8 219.78 13.70 8 -6 -8 206.48 12.90 8 -6 -8 189.08 15.00 9 -6 8 20.10 6.40 9 -6 8 27.40 5.70 9 -6 -8 20.70 6.80 9 -6 -8 21.80 5.00 0 -7 -8 3.40 1.30 0 -7 8 1.70 1.50 0 -7 8 3.00 1.70 -1 -7 -8 321.37 17.70 1 -7 8 325.47 17.60 1 7 -8 327.87 17.30 1 -7 8 334.37 17.70 1 -7 -8 325.87 17.80 -1 -7 8 313.57 17.30 -1 -7 8 332.87 17.40 2 7 -8 56.19 3.80 2 -7 8 54.69 4.40 2 -7 8 57.49 4.40 -2 -7 -8 59.39 4.40 -2 -7 8 58.69 3.90 2 -7 -8 57.39 4.50 2 -7 -8 59.89 4.80 3 7 -8 162.98 9.30 3 7 -8 158.38 9.60 3 -7 8 171.98 10.50 -3 -7 -8 166.18 10.50 3 -7 8 177.48 10.60 3 -7 -8 181.98 10.60 3 -7 -8 194.88 10.50 4 -7 8 403.96 20.50 4 7 -8 364.36 19.30 4 7 -8 346.37 19.00 4 -7 8 413.06 20.80 4 -7 -8 337.97 20.10 4 -7 -8 335.27 20.30 5 7 -8 26.80 2.60 5 -7 8 28.40 4.30 5 -7 8 24.00 4.50 5 -7 -8 33.70 4.20 5 -7 -8 36.90 4.90 6 -7 8 356.76 20.20 6 -7 8 346.47 20.70 6 -7 -8 344.57 20.00 6 -7 -8 318.37 20.60 6 7 8 372.96 19.90 7 -7 8 153.68 11.20 7 -7 8 143.29 12.20 7 -7 -8 148.89 12.30 7 7 8 164.88 10.70 7 -7 -8 163.68 11.10 8 -7 8 8.00 4.90 8 -7 8 20.20 6.10 8 -7 -8 17.90 6.10 8 -7 -8 14.80 4.50 0 -8 8 405.26 21.80 0 -8 -8 407.76 22.10 0 -8 8 405.76 21.70 1 -8 8 55.79 4.30 1 -8 8 54.69 4.30 -1 -8 -8 46.10 4.20 1 -8 -8 49.40 4.40 -1 -8 8 49.50 4.20 -1 -8 8 47.90 4.10 -2 -8 -8 98.29 6.80 2 -8 8 105.49 6.90 2 8 -8 92.89 6.00 2 -8 8 109.79 6.90 -2 -8 8 96.89 6.10 2 -8 -8 97.99 7.00 2 -8 -8 105.39 6.90 3 -8 8 420.96 23.90 3 -8 8 423.26 23.90 -3 -8 -8 424.86 23.70 3 8 -8 418.16 22.70 3 -8 -8 480.75 23.90 -3 -8 8 419.96 22.80 3 -8 -8 465.35 24.10 4 -8 8 383.16 22.40 4 -8 8 383.46 22.20 4 -8 -8 406.96 22.40 4 -8 -8 407.76 22.00 5 -8 8 143.09 9.80 5 -8 -8 126.09 9.40 6 -8 8 243.68 16.70 6 -8 8 287.57 16.70 6 -8 -8 275.77 16.00 6 8 8 266.67 15.40 6 -8 -8 239.08 16.40 7 -8 8 8.40 5.00 7 -8 8 4.60 4.30 7 -8 -8 4.60 4.00 7 8 8 10.40 3.90 7 -8 -8 5.80 5.00 8 -8 8 65.79 10.60 8 -8 8 82.99 9.10 8 -8 -8 86.29 8.60 8 -8 -8 68.59 10.40 0 -9 8 0.10 2.00 0 -9 8 2.30 2.10 0 -9 -8 0.60 2.10 1 -9 8 253.87 14.30 1 -9 8 243.18 14.20 -1 -9 -8 237.58 14.30 1 -9 -8 248.28 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29.60 3.20 -1 -5 14 30.30 2.90 2 -5 14 135.29 8.40 -2 -5 -14 136.59 8.40 2 -5 14 134.99 8.30 2 5 -14 152.58 8.10 2 -5 -14 129.69 8.50 -2 -5 14 149.59 7.80 3 -5 14 147.29 9.40 3 -5 14 150.78 9.40 3 5 -14 182.18 8.90 3 -5 -14 144.99 9.40 4 -5 14 73.09 5.80 4 -5 14 71.69 6.00 4 5 -14 76.09 4.70 4 -5 -14 81.19 5.80 4 -5 -14 80.69 5.60 5 -5 14 82.19 6.10 5 -5 14 70.29 6.70 5 5 14 79.99 5.30 5 -5 -14 73.79 5.90 5 -5 -14 78.59 6.40 -6 5 14 50.09 5.10 6 -5 14 50.49 6.60 6 -5 14 56.89 5.90 6 5 14 60.19 4.50 6 -5 -14 52.19 6.00 6 -5 -14 54.99 5.40 6 5 14 56.09 6.00 7 -5 14 33.10 5.70 7 -5 14 41.30 5.40 7 5 14 24.00 3.50 7 5 14 26.90 4.80 8 -5 14 41.00 6.70 8 -5 14 48.20 6.70 8 5 14 34.60 6.00 8 -5 -14 46.30 6.30 8 -5 -14 49.50 7.00 9 -5 14 31.60 8.10 9 -5 14 42.10 6.90 9 -5 -14 37.90 5.70 9 5 14 49.30 7.10 9 -5 -14 52.79 7.70 0 -6 14 543.35 27.80 0 -6 14 504.35 27.40 0 6 -14 523.45 27.50 0 -6 -14 538.85 27.90 1 -6 14 93.49 6.00 -1 -6 -14 90.29 6.00 1 -6 14 89.59 6.20 1 6 -14 92.09 5.40 -1 -6 14 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38.20 4.00 7 0 22 30.00 5.50 8 0 22 -1.70 4.40 8 0 22 1.60 3.10 9 0 22 15.90 4.10 9 0 22 7.50 6.10 0 1 22 12.10 1.80 0 -1 22 8.80 1.40 1 -1 22 201.28 11.20 -1 1 22 193.98 11.00 1 -1 -22 181.98 11.10 -1 -1 22 202.98 10.80 -1 -1 22 196.48 11.00 1 1 22 210.18 11.20 -2 1 22 134.29 8.00 2 1 -22 145.29 7.90 2 -1 22 132.09 8.20 2 1 22 146.89 8.30 2 -1 -22 128.89 8.00 -2 -1 22 137.79 7.90 -2 -1 22 135.59 7.70 3 1 -22 59.99 4.10 3 -1 22 56.09 4.90 -3 1 22 61.19 4.40 3 -1 22 59.19 4.60 3 1 22 72.49 5.10 3 1 22 66.99 4.70 -3 -1 22 61.49 4.10 -3 -1 22 62.49 4.00 4 -1 22 220.18 13.40 4 -1 22 222.08 12.80 -4 1 22 226.28 12.10 4 1 -22 225.58 12.10 4 1 22 223.08 13.40 4 -1 -22 225.08 12.60 -4 -1 22 226.08 12.10 4 1 22 218.08 12.60 5 -1 22 113.69 9.00 5 1 -22 123.79 7.30 5 -1 22 122.29 8.00 5 -1 -22 127.49 7.80 5 1 22 120.99 7.80 5 1 22 110.69 8.60 6 1 -22 336.47 17.50 6 -1 22 320.57 18.00 6 -1 22 301.57 19.00 6 1 22 316.67 17.80 6 1 22 308.07 19.00 6 -1 -22 329.27 17.70 7 -1 22 240.18 16.00 7 1 22 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3.30 1.20 2 2 23 4.90 1.70 -2 -2 23 3.90 1.60 3 -2 23 12.40 2.30 -3 2 23 14.00 2.30 3 -2 23 13.10 2.40 3 2 23 18.50 2.60 3 -2 -23 12.10 2.30 -3 -2 23 14.60 2.20 -3 -2 23 15.20 1.80 4 2 -23 51.59 3.30 4 -2 23 52.69 4.60 4 -2 23 49.30 5.30 4 2 23 45.60 4.30 4 -2 -23 50.19 4.50 4 2 23 40.40 5.00 -4 -2 23 57.19 3.60 -5 2 23 90.19 5.50 5 2 -23 90.39 5.20 5 -2 -23 73.79 6.30 5 2 23 91.99 7.20 5 2 23 84.59 6.20 6 -2 23 18.60 4.70 6 -2 23 28.70 4.40 6 2 23 29.90 3.90 6 -2 -23 25.50 4.10 7 -2 23 8.80 4.40 7 -2 23 11.30 3.80 7 2 23 11.10 2.60 7 2 23 21.50 5.00 7 -2 -23 5.90 3.00 8 -2 23 39.70 7.70 8 -2 23 52.39 6.20 8 2 23 48.90 5.40 8 2 23 57.49 8.40 0 -3 -23 10.30 2.20 0 -3 23 7.90 1.70 0 3 23 5.30 1.50 0 -3 23 8.00 1.80 -1 3 23 23.20 2.50 1 3 23 25.60 2.90 -2 3 23 125.79 7.90 2 -3 23 132.69 8.20 2 -3 23 138.09 8.40 2 -3 -23 152.58 8.30 -2 -3 23 121.19 7.70 -2 -3 23 124.59 7.30 2 3 23 131.79 8.10 -2 -3 23 134.09 7.20 -3 3 23 30.60 3.30 3 -3 -23 20.70 3.20 -3 -3 23 18.90 2.50 3 3 23 20.40 2.80 4 -3 23 307.47 16.70 -4 3 23 297.17 16.20 4 -3 23 302.87 17.30 4 -3 -23 287.87 16.40 4 3 23 278.57 16.30 5 -3 23 55.69 5.20 5 -3 23 62.39 6.50 5 -3 -23 45.20 5.20 5 3 23 41.00 4.60 5 3 23 54.49 5.40 6 -3 23 195.18 13.10 6 -3 23 188.88 13.40 6 3 23 215.88 12.00 6 -3 -23 194.28 12.70 7 -3 23 21.40 4.50 7 -3 23 20.60 5.30 7 3 23 13.70 5.00 7 3 23 22.00 3.30 7 -3 -23 22.70 4.30 8 -3 23 42.40 6.40 8 -3 23 44.60 7.90 8 3 23 49.60 7.90 8 3 23 52.99 5.40 0 4 23 565.44 30.20 0 -4 23 574.24 29.90 0 -4 23 548.85 30.00 0 -4 -23 600.84 30.50 1 -4 23 188.08 9.80 -1 -4 -23 157.88 10.10 1 -4 -23 164.28 9.80 -1 -4 23 148.29 8.90 -1 -4 23 143.19 8.70 1 4 23 161.18 9.60 -1 -4 23 159.78 9.40 2 -4 23 128.19 8.30 -2 4 23 134.59 8.10 2 -4 23 131.69 8.40 2 4 23 123.29 8.20 2 -4 -23 155.28 8.50 -2 -4 23 125.29 7.80 3 -4 23 64.19 5.30 -3 4 23 66.09 5.20 3 -4 23 62.29 5.40 3 -4 -23 68.39 5.20 3 4 23 70.99 5.10 4 -4 23 219.58 12.30 4 -4 23 237.98 13.00 -4 4 23 192.38 11.60 4 -4 -23 184.48 11.90 4 4 23 177.88 11.70 -5 4 23 26.30 3.80 5 -4 23 24.40 4.60 5 -4 -23 18.80 3.40 6 -4 23 79.69 8.50 6 -4 23 77.89 7.20 6 -4 -23 74.29 7.70 6 4 23 81.89 8.10 6 4 23 84.19 6.10 7 -4 23 125.79 11.10 7 -4 23 119.29 9.80 7 -4 -23 123.09 8.80 7 4 23 126.79 10.80 7 4 23 114.69 8.20 8 -4 23 20.40 6.40 8 -4 23 26.80 5.40 8 4 23 26.20 5.70 8 4 23 16.50 3.70 0 -5 -23 -0.30 1.90 0 -5 23 0.70 1.80 0 -5 23 0.30 1.60 0 5 23 2.40 1.90 -1 -5 -23 216.08 13.30 1 -5 23 269.27 13.10 -1 5 23 246.68 12.90 -1 -5 23 201.28 12.50 1 -5 -23 218.18 13.10 1 5 23 213.58 12.90 -1 -5 23 206.18 12.10 -2 5 23 265.47 14.80 2 -5 23 255.57 15.10 2 -5 23 253.77 15.00 2 -5 -23 267.87 15.20 -2 -5 23 265.77 14.50 2 5 23 270.67 14.90 3 -5 23 230.18 13.90 -3 5 23 249.58 13.90 3 -5 23 228.38 14.20 3 5 23 246.28 13.80 3 -5 -23 243.88 14.10 4 -5 23 205.48 12.70 -4 5 23 212.18 12.20 4 -5 23 195.48 12.90 4 -5 -23 206.68 12.80 4 5 23 202.68 12.20 -5 5 23 46.90 4.80 5 -5 23 42.70 5.60 5 -5 23 42.40 6.60 5 5 23 43.10 5.20 5 -5 -23 54.69 5.80 6 -5 23 310.87 19.50 6 -5 23 298.77 18.60 6 -5 -23 338.87 18.80 6 5 23 310.67 19.30 6 5 23 316.97 17.80 7 -5 23 118.79 9.60 7 -5 23 101.89 10.80 7 5 23 110.89 9.00 7 5 23 123.89 10.50 7 -5 -23 116.19 9.40 8 -5 23 35.70 7.50 8 -5 23 35.40 6.30 8 5 23 30.50 4.30 8 5 23 32.00 6.90 8 -5 -23 38.10 5.70 0 -6 23 114.29 8.00 0 -6 23 120.99 7.80 0 -6 -23 140.39 8.60 1 -6 23 9.10 2.80 1 -6 23 7.40 2.60 -1 -6 -23 7.00 2.80 -1 -6 23 8.40 2.30 -1 -6 23 9.70 1.80 1 6 23 7.60 2.50 1 -6 -23 9.70 2.90 2 -6 23 140.59 9.50 -2 6 23 152.78 9.50 2 -6 23 132.99 9.30 -2 -6 -23 154.18 10.30 2 6 23 139.89 9.10 -2 -6 23 144.69 9.50 2 -6 -23 162.38 9.60 -3 6 23 237.68 13.90 3 -6 23 248.18 14.50 3 -6 23 232.58 14.20 3 6 23 243.28 13.90 3 -6 -23 223.98 14.30 -4 6 23 162.48 10.10 4 -6 23 157.28 10.90 4 -6 -23 149.99 10.80 4 6 23 155.68 10.20 -5 6 23 72.89 7.00 5 -6 23 86.09 8.00 5 -6 23 74.49 7.70 5 6 23 87.49 6.50 5 -6 -23 72.99 7.60 6 -6 23 14.00 4.40 6 -6 23 24.20 5.10 6 6 23 18.70 4.90 6 -6 -23 27.80 4.70 6 6 23 24.40 4.20 7 -6 23 35.50 5.60 7 -6 23 23.90 6.30 7 -6 -23 43.00 6.50 7 6 23 34.70 6.20 7 6 23 35.20 4.70 8 -6 23 102.19 10.30 8 -6 23 106.09 11.80 8 6 23 92.99 10.20 8 -6 -23 101.89 9.30 0 -7 23 -1.30 2.10 0 -7 23 0.90 2.20 0 -7 -23 -0.10 2.50 1 -7 23 218.78 12.80 1 -7 23 212.78 12.70 -1 -7 -23 229.38 13.40 1 -7 -23 199.38 13.10 -1 -7 23 211.18 11.70 -1 -7 23 215.28 12.50 2 -7 23 226.48 13.60 2 -7 23 234.18 13.70 -2 -7 -23 234.68 14.50 -2 -7 23 231.18 13.10 2 -7 -23 215.48 13.90 3 -7 23 195.98 12.00 3 -7 23 187.08 11.90 3 7 23 182.58 11.80 3 -7 -23 175.78 11.90 4 -7 23 23.60 4.60 4 -7 23 21.70 4.10 -4 7 23 26.00 4.40 4 -7 -23 23.40 5.60 4 7 23 26.50 4.00 5 -7 23 367.46 21.30 5 -7 23 353.86 20.40 -5 7 23 347.47 20.30 5 -7 -23 314.97 20.70 6 -7 23 8.00 4.60 6 -7 23 6.90 4.20 6 -7 -23 10.20 5.60 6 7 23 10.80 3.40 7 -7 23 47.60 7.50 7 -7 23 38.70 6.10 7 7 23 44.60 6.70 7 7 23 40.00 5.70 7 -7 -23 35.90 7.10 0 -8 23 204.28 12.60 0 -8 -23 210.78 13.30 0 -8 23 207.48 11.90 -1 -8 -23 166.78 10.80 1 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6.40 3 -10 27 86.29 9.20 3 -10 27 98.89 9.30 3 -10 -27 106.69 10.30 -4 10 27 18.00 5.20 4 -10 27 12.50 5.30 4 -10 27 12.80 5.30 4 10 27 9.10 4.40 4 -10 -27 21.70 6.70 5 -10 27 48.40 7.80 5 -10 27 64.89 9.80 -5 10 27 72.19 8.20 5 10 27 52.99 7.90 5 -10 -27 69.39 9.20 0 -11 -27 7.30 5.60 1 -11 27 85.29 8.50 -1 -11 -27 71.49 9.90 1 -11 -27 76.19 9.40 2 -11 27 40.20 7.60 2 -11 27 24.70 5.30 -2 -11 -27 21.80 6.40 2 -11 -27 32.30 6.90 3 -11 27 20.60 5.50 3 -11 27 9.50 4.70 3 -11 -27 14.80 5.70 4 -11 27 7.30 5.90 4 -11 27 2.40 5.40 4 -11 -27 1.30 6.00 4 11 27 11.70 5.40 0 -12 -27 26.20 6.50 -1 -12 -27 8.50 5.80 1 -12 27 6.60 4.80 1 -12 -27 20.90 6.00 -2 -12 -27 70.19 10.70 2 -12 27 67.79 9.10 2 -12 -27 101.29 11.50 0 0 28 1580.14 80.99 -1 0 28 114.99 7.30 1 0 28 120.59 7.50 2 0 -28 220.88 12.60 2 0 28 218.58 12.90 -2 0 28 226.18 12.60 3 0 28 123.39 8.60 3 0 -28 137.39 8.00 -3 0 28 128.99 7.90 3 0 28 124.69 8.30 4 0 28 32.60 3.90 4 0 28 35.80 5.10 4 0 -28 24.80 3.50 -4 0 28 36.00 3.50 5 0 -28 1.30 2.00 5 0 28 3.00 3.50 5 0 28 9.20 2.90 6 0 28 6.20 4.10 6 0 28 0.20 2.90 7 0 28 1.70 4.60 7 0 28 0.90 3.40 8 0 28 2.60 5.70 8 0 28 -6.00 3.70 0 1 28 -1.00 1.60 0 -1 28 -0.30 1.30 1 -1 28 182.78 9.80 -1 1 28 158.48 9.50 -1 -1 28 156.68 9.50 1 1 28 166.68 9.80 1 -1 -28 146.79 9.80 -2 1 28 101.29 7.00 2 -1 28 106.59 7.30 2 -1 28 107.39 7.40 2 -1 -28 108.19 7.20 -2 -1 28 115.59 7.10 2 1 28 120.99 7.40 3 -1 28 17.50 3.20 3 1 -28 23.30 3.20 -3 1 28 22.20 3.00 3 -1 28 24.40 3.50 3 1 28 19.20 2.80 3 -1 -28 25.10 3.10 3 1 28 26.20 3.70 -3 -1 28 21.00 3.20 -4 1 28 98.09 6.50 4 -1 28 102.99 7.10 4 1 -28 93.59 6.10 4 -1 28 103.89 8.00 4 1 28 97.69 7.00 4 -1 -28 91.09 6.60 4 1 28 92.69 7.60 5 1 -28 51.69 4.10 5 -1 28 54.79 6.60 5 -1 28 61.59 5.70 5 -1 -28 50.39 4.60 5 1 28 55.39 5.50 5 1 28 52.99 7.40 6 -1 28 142.29 9.90 6 -1 28 153.08 11.20 6 1 28 132.89 10.80 6 -1 -28 145.59 9.10 6 1 28 133.19 9.50 7 -1 28 9.40 4.90 7 -1 28 12.90 3.90 7 1 28 17.00 5.20 7 1 28 11.80 3.50 8 -1 28 14.60 5.90 8 -1 28 7.80 4.10 8 1 28 13.70 5.90 8 1 28 11.70 4.00 0 2 28 334.17 19.70 0 -2 28 383.86 19.70 0 -2 28 371.86 19.70 -1 2 28 82.79 5.20 -1 -2 28 61.79 5.00 1 2 28 67.29 5.30 1 -2 -28 67.49 5.40 2 -2 28 66.39 5.50 2 -2 28 57.79 5.40 -2 2 28 66.69 5.20 2 2 28 70.39 5.40 -2 -2 28 78.79 5.30 -2 -2 28 81.69 4.70 2 -2 -28 59.99 5.30 3 -2 28 25.70 3.70 3 -2 28 20.10 3.20 -3 2 28 18.90 2.90 -3 -2 28 19.20 2.60 3 2 28 24.10 3.40 3 -2 -28 22.10 3.50 -3 -2 28 20.80 2.80 -4 2 28 27.90 3.80 4 -2 28 27.20 4.50 4 -2 28 33.70 4.20 4 2 28 33.40 4.60 4 -2 -28 26.50 3.50 4 2 28 26.50 4.00 5 -2 28 86.99 9.90 5 -2 28 85.99 8.70 5 -2 -28 97.79 7.10 5 2 28 93.89 7.20 6 -2 28 35.20 5.60 6 -2 28 42.70 6.30 6 2 28 38.20 5.00 6 -2 -28 46.50 5.00 6 2 28 48.30 6.40 7 -2 28 140.99 12.20 7 -2 28 141.39 10.90 7 2 28 150.88 12.10 7 -2 -28 159.78 10.40 7 2 28 148.09 10.10 8 -2 28 21.00 4.80 8 -2 28 28.20 6.40 8 2 28 22.30 4.40 8 2 28 19.00 6.30 0 -3 28 2.40 2.10 0 3 28 2.20 1.90 0 -3 28 4.80 1.80 0 -3 -28 4.40 2.10 1 -3 28 52.49 4.60 1 -3 28 53.09 4.90 -1 3 28 61.79 4.70 1 3 28 54.39 4.80 -1 -3 28 57.09 4.50 -1 -3 28 62.79 4.70 1 -3 -28 59.69 4.80 2 -3 28 135.69 8.80 -2 3 28 130.29 8.60 2 -3 28 135.69 9.00 -2 -3 28 133.59 7.90 2 3 28 143.29 8.80 -2 -3 28 143.09 8.50 -2 -3 28 136.59 7.80 2 -3 -28 136.09 8.70 -3 3 28 48.50 4.50 3 -3 28 38.20 5.20 3 -3 28 47.30 4.90 3 -3 -28 49.50 4.60 3 3 28 54.79 4.60 -3 -3 28 42.10 3.30 -3 -3 28 47.20 4.00 4 -3 28 57.69 6.10 -4 3 28 59.29 5.00 4 -3 28 61.89 5.80 4 3 28 53.89 5.40 4 -3 -28 54.49 5.20 -5 3 28 21.20 3.40 5 -3 28 20.30 4.00 5 -3 -28 23.20 3.80 5 3 28 19.70 3.70 5 3 28 28.90 4.70 6 -3 28 38.90 6.10 6 -3 28 44.70 5.90 6 3 28 31.00 5.80 6 -3 -28 32.50 4.70 6 3 28 32.80 4.80 7 -3 28 66.09 7.80 7 -3 28 74.39 9.30 7 3 28 58.19 8.60 7 3 28 83.79 6.90 7 -3 -28 65.29 7.40 8 -3 28 37.20 6.30 8 -3 28 34.20 8.00 8 3 28 37.40 5.50 8 3 28 29.50 6.50 0 -4 -28 638.04 34.60 0 -4 28 657.23 34.20 0 -4 28 654.43 33.90 0 4 28 637.04 34.40 1 -4 28 128.49 8.30 -1 -4 -28 136.39 8.90 -1 4 28 123.29 8.20 1 -4 28 126.39 8.40 -1 -4 28 128.29 8.20 -1 -4 28 130.09 7.80 1 -4 -28 131.29 8.60 1 4 28 130.49 8.50 -1 -4 28 126.89 7.50 2 -4 28 20.20 3.40 -2 4 28 17.80 3.10 2 -4 28 26.20 3.90 2 -4 -28 15.50 3.10 -2 -4 28 26.60 2.60 2 4 28 21.10 3.30 -2 -4 28 24.40 3.50 3 -4 28 202.28 12.70 3 -4 28 197.48 12.40 -3 4 28 195.18 12.10 3 -4 -28 180.08 12.20 -3 -4 28 223.18 11.40 3 4 28 207.28 12.20 -4 4 28 27.20 4.10 4 -4 28 25.70 4.30 4 4 28 34.30 4.70 4 -4 -28 32.00 4.40 5 -4 28 22.70 4.60 -5 4 28 22.10 3.60 5 -4 28 22.30 4.60 5 4 28 20.40 4.50 5 -4 -28 21.50 3.80 6 -4 28 0.60 4.40 6 -4 28 8.30 4.00 6 4 28 12.50 4.80 6 4 28 16.20 3.40 6 -4 -28 6.80 4.10 7 -4 28 41.20 7.40 7 -4 28 36.40 5.70 7 -4 -28 33.40 6.00 7 4 28 40.60 5.40 7 4 28 40.20 6.80 8 -4 28 16.60 5.30 8 -4 28 23.40 7.00 8 4 28 14.60 6.50 8 4 28 11.60 3.80 0 -5 28 1.30 2.40 0 -5 28 0.30 2.30 0 5 28 2.40 2.70 0 -5 -28 3.40 2.40 -1 -5 -28 40.60 5.10 1 -5 28 39.00 4.60 -1 5 28 41.90 4.70 1 -5 28 36.80 4.40 1 5 28 46.40 4.80 -1 -5 28 42.70 4.40 1 -5 -28 44.30 4.70 -1 -5 28 50.39 4.00 2 -5 28 210.28 13.10 2 -5 28 217.98 13.20 -2 5 28 217.48 12.90 2 5 28 234.38 13.20 2 -5 -28 213.18 13.20 3 -5 28 21.30 3.70 3 -5 28 30.20 4.50 -3 5 28 17.70 3.60 -3 -5 28 24.20 3.10 3 5 28 20.50 3.40 3 -5 -28 29.80 4.30 4 -5 28 20.80 3.90 -4 5 28 24.10 3.80 4 -5 28 20.30 4.30 4 5 28 21.20 3.90 4 -5 -28 27.10 4.40 -5 5 28 6.60 3.20 5 -5 28 9.70 4.50 5 -5 28 7.60 3.90 5 -5 -28 13.20 3.80 5 5 28 17.70 3.60 6 -5 28 1.50 4.50 6 -5 28 0.20 4.20 6 -5 -28 6.60 3.70 6 5 28 4.00 2.70 6 5 28 1.40 4.40 7 -5 28 7.50 5.60 7 -5 28 5.20 4.50 7 -5 -28 13.70 4.10 7 5 28 2.40 5.30 7 5 28 6.70 3.30 0 6 28 772.22 42.20 0 -6 28 799.42 41.70 0 -6 28 822.82 42.20 0 -6 -28 802.32 42.70 1 -6 28 25.70 3.60 1 -6 28 18.50 3.50 -1 -6 -28 13.90 3.80 -1 6 28 17.10 3.20 1 -6 -28 24.00 3.70 -1 -6 28 14.50 2.90 -1 -6 28 15.40 2.40 1 6 28 18.70 3.70 2 -6 28 110.79 7.70 -2 6 28 90.49 7.30 2 -6 28 94.39 7.30 -2 -6 28 85.69 6.70 2 6 28 81.19 7.00 2 -6 -28 102.99 8.00 -3 6 28 114.69 8.50 3 -6 28 117.79 9.00 3 -6 28 108.69 9.00 3 -6 -28 103.29 9.00 3 6 28 145.09 9.60 4 -6 28 69.89 7.60 -4 6 28 69.09 6.70 4 -6 28 61.79 7.00 4 6 28 65.19 6.60 4 -6 -28 70.59 7.50 5 -6 28 56.39 7.80 -5 6 28 51.99 6.20 5 -6 28 56.79 6.90 5 -6 -28 49.80 7.10 5 6 28 60.39 6.20 6 -6 28 83.19 8.30 6 -6 28 81.99 9.30 6 -6 -28 59.99 8.00 6 6 28 70.79 6.70 6 6 28 75.29 8.50 7 -6 28 14.00 4.90 7 -6 28 7.30 5.70 7 6 28 25.40 5.90 7 6 28 19.50 4.30 7 -6 -28 19.20 5.90 0 -7 -28 5.30 3.40 0 -7 28 -0.70 2.80 0 -7 28 3.80 2.40 1 -7 28 82.09 6.40 -1 7 28 76.29 6.90 -1 -7 -28 62.19 7.30 1 -7 28 74.69 6.70 -1 -7 28 74.49 6.30 1 -7 -28 92.89 7.40 2 -7 28 101.79 8.20 2 -7 28 109.09 8.60 -2 7 28 102.49 8.30 -2 -7 28 117.59 7.40 2 -7 -28 105.69 8.50 2 7 28 108.09 8.30 -3 7 28 168.18 10.60 3 -7 28 148.19 10.80 3 -7 28 147.59 10.70 3 -7 -28 158.48 11.30 3 7 28 143.89 10.50 4 -7 28 10.70 4.00 -4 7 28 7.90 3.80 4 -7 28 9.00 4.50 4 -7 -28 13.00 4.50 4 7 28 14.20 3.80 -5 7 28 11.40 4.30 5 -7 28 14.90 5.00 5 -7 28 16.00 4.60 5 7 28 14.00 4.20 5 -7 -28 14.10 5.40 6 -7 28 30.40 6.20 6 -7 28 50.49 7.00 6 7 28 32.40 5.00 6 -7 -28 26.50 5.90 7 -7 28 34.70 7.60 7 -7 28 36.20 7.00 7 7 28 30.10 6.90 7 -7 -28 40.00 6.50 7 7 28 32.50 4.90 0 -8 -28 222.98 14.70 0 8 28 215.58 14.50 0 -8 28 246.08 13.30 0 -8 28 224.28 13.80 1 -8 28 23.40 4.20 -1 -8 -28 19.50 4.80 1 -8 28 21.60 3.70 -1 8 28 27.20 4.70 1 8 28 21.90 4.10 -1 -8 28 24.60 4.00 1 -8 -28 25.30 4.80 -2 -8 -28 21.30 5.20 2 -8 28 17.00 4.40 2 -8 28 20.10 3.90 -2 8 28 10.60 4.20 2 -8 -28 26.70 5.10 2 8 28 20.50 4.20 3 -8 28 112.49 9.50 3 -8 28 123.99 9.80 -3 8 28 135.09 9.60 3 8 28 125.49 9.30 3 -8 -28 113.99 10.50 -4 8 28 56.49 7.00 4 -8 28 56.29 7.10 4 -8 28 48.30 7.60 4 -8 -28 47.30 7.40 4 8 28 55.59 6.80 -5 8 28 179.38 13.40 5 -8 28 215.38 14.20 5 -8 28 223.38 13.80 5 -8 -28 165.28 13.70 5 8 28 180.18 12.50 6 -8 28 3.00 5.00 6 -8 28 1.00 5.20 6 8 28 7.90 4.40 6 -8 -28 -1.90 5.10 0 -9 -28 -0.60 3.70 0 -9 28 1.30 3.40 1 -9 28 45.40 5.80 -1 -9 -28 41.50 6.60 1 9 28 45.90 6.60 1 -9 -28 51.09 7.30 -1 -9 28 45.40 5.90 2 -9 28 23.50 4.80 -2 9 28 26.80 4.70 -2 -9 -28 20.90 5.50 2 -9 28 27.80 4.80 2 -9 -28 23.50 5.70 2 9 28 26.90 5.00 -3 9 28 36.30 5.90 3 -9 28 45.70 6.20 3 -9 -28 34.60 6.20 3 9 28 44.30 6.60 4 -9 28 51.59 7.70 4 -9 28 47.50 6.80 -4 9 28 55.89 7.10 4 9 28 35.80 6.10 4 -9 -28 48.70 7.50 5 -9 28 57.19 8.30 -5 9 28 63.69 7.70 5 -9 28 69.89 9.00 5 -9 -28 63.89 8.80 5 9 28 54.19 7.80 0 -10 -28 11.40 5.20 0 -10 28 11.70 4.10 -1 -10 -28 26.70 6.00 1 -10 28 28.20 5.00 1 -10 -28 28.10 5.60 2 -10 28 28.80 5.10 -2 -10 -28 19.50 5.70 2 -10 28 28.00 5.30 2 -10 -28 25.70 5.70 3 -10 28 179.18 12.30 3 -10 28 171.98 12.40 -3 10 28 151.48 11.90 3 10 28 161.28 11.80 3 -10 -28 135.89 13.40 4 -10 28 10.20 5.30 4 -10 28 17.50 5.40 -4 10 28 7.00 5.70 4 -10 -28 12.40 6.10 4 10 28 20.70 4.80 5 -10 28 401.06 25.20 -5 10 28 418.46 25.40 5 -10 28 437.66 25.80 5 10 28 417.36 25.10 0 -11 28 9.70 4.40 0 -11 -28 -1.70 4.90 1 -11 28 5.30 4.60 -1 -11 -28 14.50 5.70 1 -11 -28 4.20 5.10 -2 -11 -28 53.99 8.10 2 -11 28 54.29 7.70 2 -11 -28 35.20 7.30 3 -11 28 129.69 10.50 3 -11 28 134.39 11.10 3 11 28 118.79 11.10 3 -11 -28 122.29 12.40 0 -12 -28 240.08 17.00 -1 -12 -28 28.10 7.20 1 -12 28 37.70 5.60 1 -12 -28 22.20 6.20 2 -12 28 170.98 12.70 -2 -12 -28 161.78 14.40 2 -12 -28 132.79 12.90 0 0 29 77.39 5.50 -1 0 29 8.30 1.90 1 0 29 4.90 1.80 2 0 -29 26.20 3.50 -2 0 29 27.10 3.40 2 0 29 29.80 3.60 3 0 -29 749.73 37.70 3 0 29 673.53 38.30 -3 0 29 742.53 37.60 3 0 29 714.53 38.10 4 0 29 24.20 3.70 -4 0 29 28.00 3.50 4 0 29 32.40 4.80 4 0 -29 27.30 3.50 5 0 29 165.78 12.10 5 0 -29 186.18 10.50 6 0 29 -4.00 3.10 6 0 29 2.50 3.80 7 0 29 14.70 4.00 7 0 29 19.90 5.40 8 0 29 9.80 5.70 8 0 29 21.60 4.70 0 1 29 3.80 1.60 0 -1 29 5.80 1.90 1 -1 29 402.66 22.30 1 -1 29 423.86 22.30 -1 1 29 402.56 22.10 1 1 29 406.46 22.30 -1 -1 29 430.66 22.20 1 -1 -29 396.46 22.30 -2 1 29 446.36 24.40 2 -1 29 456.75 24.80 2 -1 29 460.65 24.80 2 1 29 451.75 24.70 -2 -1 29 480.05 24.40 2 -1 -29 444.16 24.60 -3 1 29 52.29 4.60 3 -1 29 47.10 4.80 3 -1 29 50.19 5.30 3 1 29 47.10 4.70 3 1 29 61.79 5.60 3 -1 -29 58.19 4.70 4 -1 29 66.89 6.90 4 1 -29 84.89 5.20 4 -1 29 60.99 5.80 -4 1 29 60.29 5.10 4 1 29 65.39 6.50 4 1 29 50.99 5.50 -4 -1 29 78.39 4.90 4 -1 -29 78.09 5.60 5 1 -29 41.60 3.50 5 -1 29 33.10 5.80 5 1 29 35.40 4.90 5 -1 -29 31.60 4.10 5 1 29 36.20 7.00 6 -1 29 123.39 8.80 6 -1 29 121.79 10.30 6 1 29 114.09 8.50 6 -1 -29 109.39 7.60 6 1 29 111.19 10.00 7 -1 29 35.00 5.10 7 -1 29 32.60 6.50 7 1 29 36.70 5.60 7 1 29 46.70 7.00 8 -1 29 12.90 4.30 8 -1 29 5.60 5.20 8 1 29 7.30 4.10 8 1 29 3.70 5.40 0 -2 29 397.16 22.00 0 2 29 419.56 22.20 0 -2 29 414.26 22.10 -1 2 29 51.29 4.30 1 -2 29 48.30 4.30 1 -2 29 53.79 4.70 1 -2 -29 56.39 4.70 1 2 29 47.70 4.50 -1 -2 29 49.60 4.40 2 -2 29 733.93 38.10 2 -2 29 700.83 38.20 -2 2 29 732.23 37.90 2 -2 -29 742.73 38.10 -2 -2 29 715.23 37.50 -2 -2 29 733.93 37.70 2 2 29 697.73 38.10 3 -2 29 42.00 4.50 -3 2 29 40.00 4.30 3 -2 29 39.90 4.80 3 -2 -29 50.69 4.70 3 2 29 44.90 4.30 -4 2 29 240.28 13.60 4 -2 29 233.28 14.80 4 -2 29 243.18 14.30 4 2 29 242.58 14.20 4 -2 -29 246.68 13.90 4 2 29 231.18 14.80 5 -2 29 59.89 8.30 5 -2 29 56.89 5.70 5 2 29 55.99 6.80 5 2 29 38.20 5.70 6 -2 29 15.80 4.40 6 -2 29 21.20 5.00 6 -2 -29 24.00 3.80 6 2 29 16.10 4.90 6 2 29 25.10 4.00 7 -2 29 63.29 7.90 7 -2 29 72.89 9.00 7 2 29 75.89 6.70 7 2 29 88.49 9.30 8 -2 29 65.59 8.00 8 -2 29 66.99 10.00 8 2 29 63.59 6.80 8 2 29 65.09 9.90 0 -3 -29 9.00 2.60 0 -3 29 10.30 2.40 0 3 29 8.60 2.60 0 -3 29 10.40 2.20 1 -3 29 178.68 10.40 1 -3 29 171.58 10.40 -1 3 29 167.38 10.20 1 3 29 169.48 10.40 -1 -3 29 169.68 9.90 1 -3 -29 166.78 10.40 -1 -3 29 166.78 10.10 -2 3 29 144.29 8.80 2 -3 29 132.79 9.00 2 -3 29 129.39 8.90 2 3 29 124.69 8.70 -2 -3 29 133.39 7.90 -2 -3 29 130.99 7.80 2 -3 -29 153.08 8.90 -2 -3 29 139.29 8.50 3 -3 29 54.59 5.60 3 -3 29 57.09 5.30 -3 -3 29 45.00 3.50 3 3 29 54.59 4.70 3 -3 -29 52.79 4.70 -3 -3 29 43.40 4.30 -4 3 29 484.85 26.10 4 -3 29 516.45 27.10 4 -3 29 512.05 27.40 4 3 29 459.75 26.60 4 -3 -29 467.25 26.40 5 -3 29 40.20 5.40 5 -3 29 36.20 5.80 -5 3 29 32.70 4.90 5 3 29 36.20 5.50 5 -3 -29 35.40 4.70 6 -3 29 31.80 5.40 6 -3 29 22.00 5.40 6 3 29 31.00 4.40 6 3 29 28.50 5.90 6 -3 -29 23.70 4.00 7 -3 29 16.70 5.50 7 -3 29 9.60 4.30 7 3 29 14.00 5.20 7 3 29 17.80 3.70 7 -3 -29 13.70 4.40 8 -3 29 35.90 6.20 8 -3 29 27.30 7.30 8 3 29 43.10 5.60 8 3 29 44.30 7.40 0 -4 29 615.64 32.30 0 4 29 610.84 32.60 0 -4 -29 662.43 33.20 0 -4 29 565.74 32.40 -1 4 29 3.90 2.20 1 -4 29 1.60 2.20 1 -4 29 5.50 2.60 -1 -4 29 4.30 2.10 1 4 29 3.50 2.20 1 -4 -29 2.10 2.20 -1 -4 29 4.80 2.10 -2 4 29 153.38 9.70 2 -4 29 155.68 10.10 2 -4 29 151.88 10.00 -2 -4 29 151.88 9.40 -2 -4 29 145.09 8.60 2 4 29 154.68 9.80 2 -4 -29 162.08 10.00 -3 4 29 131.99 9.40 3 -4 29 163.48 10.20 3 -4 29 171.18 10.00 3 4 29 132.99 9.30 -3 -4 29 143.59 8.70 3 -4 -29 133.59 9.50 4 -4 29 30.10 4.60 -4 4 29 26.00 3.80 4 -4 29 23.90 4.50 4 4 29 20.10 3.80 4 -4 -29 24.80 3.90 -5 4 29 24.90 3.90 5 -4 29 19.70 3.90 5 -4 29 13.70 4.30 5 4 29 18.50 3.80 5 4 29 21.00 4.80 5 -4 -29 17.10 3.70 6 -4 29 6.50 4.30 6 -4 29 3.40 4.40 6 -4 -29 5.10 3.80 6 4 29 3.80 4.50 6 4 29 3.90 3.00 7 -4 29 4.00 4.50 7 -4 29 0.30 5.10 7 4 29 6.50 3.40 7 -4 -29 -2.60 4.10 7 4 29 -0.80 5.00 0 -5 -29 5.80 2.70 0 -5 29 3.60 2.30 0 -5 29 0.10 2.30 0 5 29 1.10 2.30 1 -5 29 49.50 5.00 1 -5 29 54.69 5.30 -1 -5 -29 68.29 6.20 -1 5 29 51.39 5.20 -1 -5 29 54.69 4.40 -1 -5 29 54.69 5.00 1 -5 -29 68.59 5.70 1 5 29 52.39 5.20 2 -5 29 290.57 16.40 2 -5 29 271.77 16.40 -2 5 29 261.27 16.10 2 5 29 292.57 16.30 -2 -5 29 279.87 15.70 2 -5 -29 288.07 16.70 3 -5 29 36.30 5.10 3 -5 29 44.20 5.30 -3 5 29 32.60 4.40 3 5 29 23.40 3.80 -3 -5 29 26.10 3.40 3 -5 -29 30.90 4.60 -4 5 29 125.29 8.80 4 -5 29 139.39 10.20 4 -5 29 123.89 9.30 4 -5 -29 123.49 9.40 -5 5 29 49.20 5.90 5 -5 29 43.00 5.90 5 -5 29 44.40 7.20 5 5 29 51.79 5.80 5 -5 -29 53.69 7.30 6 -5 29 2.50 4.80 6 -5 29 -2.50 3.70 6 5 29 -4.20 4.20 6 5 29 -1.10 3.20 6 -5 -29 1.30 4.60 7 -5 29 8.10 5.10 7 -5 29 5.30 5.70 7 -5 -29 10.80 4.40 7 5 29 2.70 3.50 7 5 29 0.30 5.20 0 6 29 979.60 51.79 0 -6 -29 1014.80 52.29 0 -6 29 979.10 51.79 0 -6 29 981.90 51.29 -1 -6 -29 26.70 4.40 1 -6 29 24.40 3.80 -1 6 29 15.60 3.80 1 -6 29 24.70 3.50 -1 -6 29 22.00 3.10 1 -6 -29 22.80 3.90 1 6 29 16.80 3.50 -2 6 29 17.60 3.60 2 -6 29 30.00 4.20 2 -6 29 20.00 3.80 2 -6 -29 17.00 3.80 2 6 29 21.90 4.00 -2 -6 29 11.70 3.00 -3 6 29 30.00 4.70 3 -6 29 33.50 5.00 3 -6 29 31.00 4.90 3 6 29 37.90 5.20 3 -6 -29 37.50 5.60 4 -6 29 17.90 4.80 -4 6 29 18.30 4.00 4 6 29 23.10 4.20 -5 6 29 146.99 9.90 5 -6 29 128.09 10.40 5 -6 29 118.59 10.90 5 -6 -29 121.59 10.00 5 6 29 133.59 9.60 6 -6 29 16.80 4.70 6 -6 29 13.20 5.60 6 6 29 30.60 4.50 6 6 29 28.50 5.70 6 -6 -29 23.50 5.30 7 -6 29 40.20 6.70 7 -6 29 47.50 8.10 7 -6 -29 40.40 6.40 7 6 29 43.40 6.10 7 6 29 42.50 7.40 0 -7 -29 2.30 3.50 0 -7 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29 10.00 4.70 2 -10 29 32.30 5.40 -2 -10 -29 25.60 5.90 -2 10 29 28.60 6.00 2 -10 29 23.00 5.40 2 10 29 46.70 6.40 2 -10 -29 24.70 6.30 3 -10 29 75.79 9.00 -3 10 29 71.09 8.80 3 -10 29 72.99 8.30 3 -10 -29 66.99 9.70 3 10 29 85.19 8.40 4 -10 29 2.30 5.40 -4 10 29 7.50 5.10 4 -10 29 7.30 5.30 4 -10 -29 1.80 5.40 4 10 29 6.40 4.90 0 -11 -29 2.70 5.40 0 -11 29 18.50 4.70 -1 -11 -29 10.60 6.00 1 -11 29 3.40 4.40 1 -11 -29 8.60 5.10 -2 -11 -29 92.79 11.40 2 -11 29 85.79 9.40 2 -11 -29 111.39 11.10 -3 11 29 91.89 9.60 3 -11 29 84.19 9.30 3 -11 29 78.19 8.40 3 -11 -29 78.09 11.00 3 11 29 83.29 9.70 0 -12 -29 12.20 6.50 1 -12 29 13.30 4.90 -1 -12 -29 1.40 6.40 1 -12 -29 -6.90 5.50 0 0 30 595.64 31.60 1 0 30 281.17 15.90 -1 0 30 283.87 15.80 -2 0 30 139.69 8.70 2 0 30 141.69 9.10 3 0 -30 733.63 38.90 3 0 30 749.62 39.50 3 0 30 752.42 39.80 -3 0 30 748.43 38.90 4 0 30 14.20 3.00 4 0 30 8.60 3.50 4 0 -30 12.30 2.30 5 0 -30 1.90 2.20 5 0 30 4.60 3.60 6 0 30 10.10 4.40 6 0 30 0.40 3.40 7 0 30 4.50 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54.69 4.70 0 2 30 50.59 4.50 1 -2 30 33.90 3.60 1 -2 30 36.00 4.00 -1 2 30 28.10 3.50 1 -2 -30 24.30 3.70 1 2 30 24.40 3.60 -1 -2 30 28.10 3.60 2 -2 30 528.05 26.80 -2 2 30 474.75 26.20 2 -2 30 520.75 26.60 2 2 30 473.85 26.40 2 -2 -30 433.76 26.30 -2 -2 30 506.55 26.10 3 -2 30 82.99 6.80 3 -2 30 84.09 6.50 -3 2 30 82.59 6.10 -3 -2 30 79.09 5.80 3 2 30 78.19 6.10 3 -2 -30 77.79 6.20 4 -2 30 19.40 3.80 4 -2 30 19.90 4.10 -4 2 30 26.90 3.80 4 -2 -30 19.30 3.30 4 2 30 32.70 5.10 4 2 30 32.20 4.30 5 -2 30 488.45 29.00 5 -2 30 500.35 28.20 5 -2 -30 549.74 27.80 5 2 30 509.15 28.20 5 2 30 525.25 29.10 6 -2 30 61.79 6.90 6 -2 30 61.79 7.90 6 -2 -30 58.39 5.70 6 2 30 60.89 8.10 6 2 30 62.79 6.30 7 -2 30 14.90 5.30 7 -2 30 18.80 5.70 7 2 30 8.00 3.40 7 2 30 13.40 5.40 8 -2 30 90.39 9.30 8 -2 30 101.89 11.40 8 2 30 86.69 10.60 8 2 30 91.09 8.10 0 3 30 2.90 2.30 0 -3 30 3.50 2.10 0 -3 30 4.40 2.30 0 -3 -30 8.20 2.50 -1 3 30 169.88 11.00 1 -3 30 186.58 11.20 1 -3 30 179.98 11.20 1 3 30 185.78 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-4 30 266.77 14.70 2 -4 30 147.89 10.30 2 -4 30 154.98 10.50 -2 4 30 164.38 10.20 -2 -4 30 180.38 9.30 2 -4 -30 152.98 10.50 2 4 30 159.88 10.30 -2 -4 30 178.78 10.00 3 -4 30 93.79 7.70 3 -4 30 102.19 7.70 -3 4 30 96.39 7.30 3 4 30 95.49 7.30 3 -4 -30 103.29 7.80 -3 -4 30 96.99 6.60 -4 4 30 132.99 8.70 4 -4 30 116.89 9.20 4 -4 30 127.59 9.70 4 -4 -30 117.79 9.30 -5 4 30 34.90 5.70 5 -4 30 33.30 5.00 5 -4 30 26.20 5.40 5 4 30 25.70 4.50 5 4 30 31.10 5.20 5 -4 -30 25.10 4.50 6 -4 30 -2.00 3.60 6 -4 30 5.10 4.80 6 4 30 2.60 3.30 6 4 30 9.50 4.60 6 -4 -30 10.80 3.60 7 -4 30 40.00 7.50 7 -4 30 32.10 5.70 7 4 30 44.90 7.10 7 -4 -30 40.00 5.90 7 4 30 44.50 6.00 0 -5 30 4.20 2.70 0 -5 30 2.40 2.30 0 -5 -30 1.90 2.50 0 5 30 -0.90 2.50 1 -5 30 108.29 7.90 -1 -5 -30 109.79 8.70 -1 5 30 111.49 8.00 1 -5 30 111.39 8.00 -1 -5 30 117.89 7.80 1 -5 -30 122.09 8.50 -1 -5 30 114.49 7.30 1 5 30 119.89 8.40 2 -5 30 276.87 17.50 -2 5 30 305.27 17.40 2 -5 30 300.77 17.60 2 -5 -30 331.67 18.20 -2 -5 30 312.37 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8.70 5 -6 30 70.79 7.50 5 -6 30 61.09 8.10 -5 6 30 48.40 6.80 5 -6 -30 60.39 7.40 5 6 30 50.49 6.70 6 -6 30 6.70 4.90 6 -6 30 4.40 5.20 6 -6 -30 -0.90 4.10 6 6 30 6.90 4.80 6 6 30 3.60 3.60 7 -6 30 65.49 8.80 7 -6 30 69.39 10.20 7 6 30 72.19 7.00 7 6 30 65.39 9.80 7 -6 -30 59.59 9.10 0 7 30 -0.50 3.00 0 -7 30 5.50 2.70 0 -7 30 8.10 3.40 -1 -7 -30 47.80 6.80 1 -7 30 55.19 5.60 -1 7 30 45.10 5.80 1 -7 30 52.79 5.90 1 7 30 54.89 6.30 -1 -7 30 45.70 5.30 2 -7 30 423.86 25.00 -2 7 30 467.75 25.10 2 -7 30 420.26 24.80 2 7 30 420.66 25.00 -2 -7 30 451.15 24.20 2 -7 -30 485.35 25.60 -3 7 30 17.00 5.10 3 -7 30 28.30 5.00 3 -7 30 22.10 4.70 3 -7 -30 26.80 5.20 3 7 30 27.20 4.60 4 -7 30 137.09 10.70 4 -7 30 146.49 10.40 4 7 30 110.99 10.00 4 -7 -30 120.29 10.70 5 -7 30 64.59 8.30 -5 7 30 48.10 7.00 5 -7 30 67.89 7.50 5 7 30 45.90 7.00 5 -7 -30 56.99 7.80 6 -7 30 76.09 9.20 6 -7 30 52.99 8.10 6 -7 -30 53.79 7.70 6 7 30 54.19 6.90 0 -8 -30 262.67 17.60 0 -8 30 284.67 16.50 0 8 30 271.47 16.40 -1 8 30 73.49 7.20 1 -8 30 65.19 6.50 -1 -8 -30 74.89 8.00 1 -8 30 66.29 7.60 1 8 30 73.69 6.90 -1 -8 30 70.29 6.70 1 -8 -30 62.29 7.30 2 -8 30 134.69 9.60 -2 -8 -30 121.39 10.90 2 -8 30 124.79 9.80 -2 8 30 123.79 9.90 2 -8 -30 129.19 10.80 2 8 30 123.79 9.90 3 -8 30 90.39 8.40 -3 8 30 109.69 8.60 3 -8 30 95.09 8.70 3 8 30 88.69 8.40 3 -8 -30 79.09 9.00 -4 8 30 13.30 4.60 4 -8 30 23.10 4.70 4 -8 30 12.20 4.90 4 8 30 24.50 4.70 4 -8 -30 24.10 5.20 -5 8 30 6.40 4.20 5 -8 30 20.50 5.60 5 -8 30 10.90 5.40 5 -8 -30 8.00 5.90 5 8 30 10.10 4.10 6 -8 30 118.39 11.40 6 -8 30 108.99 10.50 6 -8 -30 77.79 11.20 6 8 30 111.79 9.30 0 -9 -30 1.00 4.20 0 -9 30 1.30 3.80 0 9 30 2.20 3.80 1 -9 30 558.14 30.50 1 -9 30 555.14 30.70 -1 9 30 572.74 30.80 -1 -9 -30 571.14 31.30 -1 -9 30 557.24 29.90 1 9 30 486.05 30.60 1 -9 -30 526.85 31.90 2 -9 30 10.00 4.20 2 -9 30 11.70 4.40 -2 9 30 9.30 4.30 -2 -9 -30 16.90 5.40 2 9 30 9.50 4.20 2 -9 -30 12.90 4.90 3 -9 30 68.89 8.00 3 -9 30 70.29 7.80 -3 9 30 61.79 7.60 3 -9 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31 140.19 9.60 5 -1 31 14.80 4.50 5 -1 31 9.60 3.30 5 -1 -31 9.30 2.30 5 1 31 4.30 3.70 5 1 31 4.70 3.10 6 -1 31 91.09 8.00 6 -1 31 85.59 9.20 6 1 31 97.09 7.90 6 1 31 108.79 9.60 7 -1 31 31.10 5.30 7 -1 31 33.30 6.40 7 1 31 47.30 7.30 7 1 31 34.70 5.10 8 -1 31 4.00 5.70 8 -1 31 4.50 4.50 8 1 31 4.40 4.10 8 1 31 13.20 6.20 0 -2 31 20.40 3.10 0 2 31 21.00 3.20 0 -2 31 21.30 3.10 1 -2 31 86.79 6.40 1 -2 31 86.89 6.30 -1 2 31 83.09 6.20 -1 -2 31 84.19 6.20 1 -2 -31 85.49 6.60 1 2 31 88.39 6.80 2 -2 31 364.16 20.50 2 -2 31 354.86 20.40 -2 2 31 359.26 20.10 -2 -2 31 374.16 19.90 2 2 31 368.26 20.40 2 -2 -31 375.16 20.30 3 -2 31 39.90 5.00 -3 2 31 38.50 4.20 3 -2 31 40.20 4.80 -3 -2 31 38.50 4.10 3 -2 -31 41.90 4.60 3 2 31 44.10 4.50 4 -2 31 35.40 5.60 -4 2 31 32.90 4.20 4 -2 31 41.30 5.60 4 -2 -31 31.00 4.40 4 2 31 31.60 4.50 4 2 31 34.80 5.50 5 -2 31 49.00 5.80 5 -2 31 38.70 5.80 5 2 31 44.60 5.50 5 2 31 43.40 6.60 5 -2 -31 40.00 4.80 6 -2 31 3.80 4.60 6 -2 31 9.70 4.00 6 -2 -31 3.30 3.10 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7 5 32 25.70 6.60 7 -5 -32 19.70 5.10 7 5 32 29.30 5.00 0 -6 -32 571.74 31.80 0 6 32 567.74 30.80 0 -6 32 580.54 30.30 0 -6 32 551.34 30.70 1 -6 32 111.19 7.60 1 -6 32 89.89 7.80 1 6 32 88.59 7.40 1 -6 -32 84.29 8.40 -1 -6 32 98.39 7.40 -2 6 32 101.89 9.60 2 -6 32 96.49 8.30 2 -6 32 110.59 8.40 -2 -6 32 125.99 7.90 2 -6 -32 113.59 9.20 2 6 32 102.49 8.60 -3 6 32 44.20 5.70 3 -6 32 40.50 6.20 3 -6 32 40.10 5.80 3 6 32 44.10 6.00 3 -6 -32 35.30 6.70 -4 6 32 3.90 3.50 4 -6 32 2.10 3.80 4 -6 32 3.90 4.30 4 6 32 4.90 3.50 4 -6 -32 13.60 4.30 5 -6 32 11.90 5.20 -5 6 32 10.30 4.80 5 -6 32 9.70 4.50 5 6 32 14.50 4.00 5 -6 -32 5.40 4.00 6 -6 32 6.10 5.50 6 -6 32 6.20 5.30 6 6 32 9.80 4.00 6 6 32 9.70 5.40 0 7 32 13.20 4.20 0 -7 -32 12.20 4.60 0 -7 32 13.40 3.10 1 -7 32 49.99 5.80 -1 -7 -32 35.20 6.00 -1 7 32 44.10 6.10 1 -7 32 56.29 6.10 1 -7 -32 61.39 6.80 -1 -7 32 37.00 5.60 1 7 32 49.60 6.10 2 -7 32 12.30 4.20 -2 7 32 10.20 4.00 2 -7 32 16.50 4.10 2 7 32 8.40 3.90 2 -7 -32 7.30 4.00 3 -7 32 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Christian' ; Freie Universit\"at Berlin Institut f\"ur Chemie und Biochemie Anorganische Chemie Fabeckstr. 34-36 14195 Berlin Germany ; 'Rigo, Massimo' ; Freie Universit\"at Berlin Institut f\"ur Chemie und Biochemie Anorganische Chemie Fabeckstr. 34-36 14195 Berlin Germany ; 'Weber, Manuela' ; Freie Universit\"at Berlin Institut f\"ur Chemie und Biochemie Anorganische Chemie Fabeckstr. 34-36 14195 Berlin Germany ; _publ_section_title ; ... see the published paper. ; _publ_section_abstract ; ... and following paragraphs: see the published paper. ; _publ_section_experimental ; ; _publ_section_comment ; ; _publ_section_references ; ; _publ_section_figure_captions ; ; #END===============================================