data_mr174_a _audit_creation_date 2015-10-26 _audit_creation_method ; Olex2 1.2 (compiled 2015.01.26 svn.r3150 for OlexSys, GUI svn.r4998) ; _shelxl_version_number 2014/6 _publ_contact_author_address ? _publ_contact_author_email ? _publ_contact_author_name '' _publ_contact_author_phone ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2008). Acta Cryst. A64, 112-122. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'C32 H21 Ni O3 P' _chemical_formula_sum 'C32 H21 Ni O3 P' _chemical_formula_weight 543.17 _chemical_melting_point ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ni' 'Ni' 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'monoclinic' _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 11.9762(7) _cell_length_b 11.8806(6) _cell_length_c 18.6899(10) _cell_angle_alpha 90 _cell_angle_beta 92.959(4) _cell_angle_gamma 90 _cell_volume 2655.7(2) _cell_formula_units_Z 4 _cell_measurement_reflns_used 5595 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 27.53 _cell_measurement_theta_min 2.42 _shelx_estimated_absorpt_T_max 0.968 _shelx_estimated_absorpt_T_min 0.887 _exptl_absorpt_coefficient_mu 0.822 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.5811 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/5 (Bruker,2014/5) was used for absorption correction. wR2(int) was 0.1046 before and 0.0760 after correction. The Ratio of minimum to maximum transmission is 0.7793. The \l/2 correction factor is Not present. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'colourless' _exptl_crystal_density_diffrn 1.358 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description 'block' _exptl_crystal_F_000 1120 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.09 _exptl_crystal_size_min 0.04 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.1672 _diffrn_reflns_av_unetI/netI 0.1328 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 29858 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 26.000 _diffrn_reflns_theta_max 28.318 _diffrn_reflns_theta_min 2.416 _diffrn_ambient_temperature 100.0 _diffrn_detector_area_resol_mean ? _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_source ? _diffrn_standards_number 0 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3945 _reflns_number_total 6595 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'SAINT v8.34A (Bruker, 2013)' _computing_data_collection ? _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2008)' _computing_structure_solution ? _refine_diff_density_max 0.436 _refine_diff_density_min -0.513 _refine_diff_density_rms 0.101 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.015 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 334 _refine_ls_number_reflns 6595 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.1322 _refine_ls_R_factor_gt 0.0623 _refine_ls_restrained_S_all 1.015 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0264P)^2^+0.8751P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0860 _refine_ls_wR_factor_ref 0.1027 _refine_special_details ? _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C13(H13), C7(H7), C19(H19), C29(H29), C2(H2), C10(H10), C26(H26), C9(H9), C4(H4), C20(H20), C17(H17), C14(H14), C11(H11), C8(H8), C15(H15), C16(H16), C28(H28), C27(H27), C23(H23), C21(H21), C22(H22) ; _atom_sites_solution_hydrogens geom _atom_sites_solution_primary ? _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ni1 Ni 0.70140(4) 0.12231(3) 0.46565(2) 0.01316(11) Uani 1 1 d . . . . . P1 P 0.73880(7) 0.29143(6) 0.50806(4) 0.01021(19) Uani 1 1 d . . . . . O1 O 0.5898(2) -0.00224(19) 0.57765(12) 0.0264(6) Uani 1 1 d . . . . . O2 O 0.8934(2) -0.00925(19) 0.42303(15) 0.0355(7) Uani 1 1 d . . . . . O3 O 0.5540(2) 0.1609(2) 0.33672(13) 0.0394(8) Uani 1 1 d . . . . . C12 C 0.5368(3) 0.3062(2) 0.58743(17) 0.0112(7) Uani 1 1 d . . . . . C1 C 0.6385(3) 0.3635(2) 0.56480(15) 0.0113(7) Uani 1 1 d . . . . . C13 C 0.4545(3) 0.2677(2) 0.53800(18) 0.0164(8) Uani 1 1 d . . . . . H13 H 0.4629 0.2794 0.4883 0.020 Uiso 1 1 calc R . . . . C24 C 0.8606(3) 0.3198(2) 0.56844(16) 0.0117(7) Uani 1 1 d . . . . . C7 C 0.8177(3) 0.3184(2) 0.33548(16) 0.0152(7) Uani 1 1 d . . . . . H7 H 0.8664 0.2712 0.3637 0.018 Uiso 1 1 calc R . . . . C19 C 0.8808(3) 0.7000(2) 0.55512(17) 0.0163(8) Uani 1 1 d . . . . . H19 H 0.9160 0.6702 0.5148 0.020 Uiso 1 1 calc R . . . . C5 C 0.7592(3) 0.4108(2) 0.44781(16) 0.0120(7) Uani 1 1 d . . . . . C29 C 0.9372(3) 0.2389(2) 0.59094(16) 0.0136(7) Uani 1 1 d . . . . . H29 H 0.9279 0.1632 0.5754 0.016 Uiso 1 1 calc R . . . . C18 C 0.8054(3) 0.6343(2) 0.58973(16) 0.0130(7) Uani 1 1 d . . . . . C6 C 0.7514(3) 0.3975(2) 0.36863(16) 0.0113(7) Uani 1 1 d . . . . . C2 C 0.6705(3) 0.4658(2) 0.58593(16) 0.0133(7) Uani 1 1 d . . . . . H2 H 0.6244 0.5088 0.6155 0.016 Uiso 1 1 calc R . . . . C10 C 0.6736(3) 0.4541(3) 0.25229(17) 0.0191(8) Uani 1 1 d . . . . . H10 H 0.6238 0.5001 0.2239 0.023 Uiso 1 1 calc R . . . . C26 C 0.9633(3) 0.4608(3) 0.63601(16) 0.0162(8) Uani 1 1 d . . . . . H26 H 0.9724 0.5365 0.6517 0.019 Uiso 1 1 calc R . . . . C9 C 0.7407(3) 0.3763(3) 0.22013(16) 0.0190(8) Uani 1 1 d . . . . . H9 H 0.7375 0.3693 0.1694 0.023 Uiso 1 1 calc R . . . . C4 C 0.7772(3) 0.5081(2) 0.48055(15) 0.0121(7) Uani 1 1 d . . . . . H4 H 0.7876 0.5743 0.4531 0.015 Uiso 1 1 calc R . . . . C20 C 0.9064(3) 0.8083(3) 0.57769(18) 0.0191(8) Uani 1 1 d . . . . . H20 H 0.9577 0.8523 0.5525 0.023 Uiso 1 1 calc R . . . . C25 C 0.8731(3) 0.4318(2) 0.59088(16) 0.0114(7) Uani 1 1 d . . . . . C17 C 0.5225(3) 0.2889(2) 0.66019(17) 0.0149(7) Uani 1 1 d . . . . . H17 H 0.5772 0.3157 0.6947 0.018 Uiso 1 1 calc R . . . . C14 C 0.3608(3) 0.2128(3) 0.5603(2) 0.0205(8) Uani 1 1 d . . . . . H14 H 0.3048 0.1878 0.5261 0.025 Uiso 1 1 calc R . . . . C3 C 0.7814(3) 0.5149(2) 0.56279(16) 0.0115(7) Uani 1 1 d . . . . . C11 C 0.6795(3) 0.4643(2) 0.32644(16) 0.0156(7) Uani 1 1 d . . . . . H11 H 0.6336 0.5179 0.3486 0.019 Uiso 1 1 calc R . . . . C31 C 0.8210(3) 0.0455(3) 0.44074(19) 0.0208(8) Uani 1 1 d . . . . . C8 C 0.8127(3) 0.3085(3) 0.26141(17) 0.0178(8) Uani 1 1 d . . . . . H8 H 0.8586 0.2552 0.2390 0.021 Uiso 1 1 calc R . . . . C15 C 0.3484(3) 0.1943(3) 0.6330(2) 0.0245(9) Uani 1 1 d . . . . . H15 H 0.2848 0.1553 0.6485 0.029 Uiso 1 1 calc R . . . . C16 C 0.4292(3) 0.2329(3) 0.68224(19) 0.0208(8) Uani 1 1 d . . . . . H16 H 0.4206 0.2208 0.7319 0.025 Uiso 1 1 calc R . . . . C30 C 0.6316(3) 0.0472(3) 0.53452(17) 0.0166(8) Uani 1 1 d . . . . . C28 C 1.0281(3) 0.2685(3) 0.63640(17) 0.0185(8) Uani 1 1 d . . . . . H28 H 1.0810 0.2131 0.6522 0.022 Uiso 1 1 calc R . . . . C27 C 1.0409(3) 0.3792(3) 0.65851(17) 0.0195(7) Uani 1 1 d . . . . . H27 H 1.1033 0.3997 0.6893 0.023 Uiso 1 1 calc R . . . . C23 C 0.7577(3) 0.6786(3) 0.64987(19) 0.0249(9) Uani 1 1 d . . . . . H23 H 0.7069 0.6345 0.6754 0.030 Uiso 1 1 calc R . . . . C21 C 0.8575(3) 0.8524(3) 0.6366(2) 0.0254(9) Uani 1 1 d . . . . . H21 H 0.8744 0.9269 0.6521 0.031 Uiso 1 1 calc R . . . . C32 C 0.6105(3) 0.1453(3) 0.38671(18) 0.0213(8) Uani 1 1 d . . . . . C22 C 0.7838(3) 0.7873(3) 0.6728(2) 0.0346(10) Uani 1 1 d . . . . . H22 H 0.7505 0.8168 0.7139 0.042 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ni1 0.0149(3) 0.01191(19) 0.0128(2) -0.00084(18) 0.00168(17) -0.0024(2) P1 0.0107(5) 0.0101(4) 0.0100(4) 0.0001(3) 0.0019(4) -0.0010(4) O1 0.0312(17) 0.0301(14) 0.0178(13) 0.0060(11) 0.0002(12) -0.0139(12) O2 0.0230(17) 0.0196(13) 0.065(2) -0.0101(13) 0.0145(15) -0.0003(12) O3 0.040(2) 0.0582(18) 0.0186(14) 0.0155(13) -0.0113(14) -0.0205(15) C12 0.0087(18) 0.0074(15) 0.0177(17) -0.0005(12) 0.0007(14) 0.0025(13) C1 0.0117(19) 0.0126(15) 0.0095(15) 0.0023(12) -0.0008(13) -0.0004(14) C13 0.015(2) 0.0158(16) 0.0187(18) -0.0023(14) -0.0020(15) 0.0006(14) C24 0.0112(19) 0.0176(16) 0.0069(15) -0.0016(13) 0.0050(14) -0.0034(14) C7 0.018(2) 0.0166(16) 0.0114(16) 0.0041(13) 0.0014(15) 0.0000(14) C19 0.019(2) 0.0167(16) 0.0125(16) -0.0004(13) -0.0012(15) -0.0045(15) C5 0.0100(19) 0.0131(15) 0.0132(16) 0.0019(12) 0.0034(14) 0.0008(13) C29 0.013(2) 0.0141(16) 0.0144(17) -0.0003(13) 0.0059(15) -0.0014(14) C18 0.0123(19) 0.0120(15) 0.0144(16) -0.0009(13) -0.0027(14) -0.0014(14) C6 0.0112(19) 0.0114(16) 0.0114(16) 0.0024(12) 0.0009(14) -0.0061(13) C2 0.015(2) 0.0131(15) 0.0119(16) 0.0012(13) 0.0010(14) 0.0009(14) C10 0.022(2) 0.0197(17) 0.0147(17) 0.0047(14) -0.0041(16) -0.0025(15) C26 0.017(2) 0.0173(16) 0.0145(17) 0.0002(14) -0.0003(15) -0.0046(15) C9 0.025(2) 0.0252(17) 0.0074(15) 0.0010(15) 0.0024(14) -0.0047(17) C4 0.013(2) 0.0134(15) 0.0099(16) 0.0049(12) 0.0039(14) 0.0016(13) C20 0.017(2) 0.0176(17) 0.0221(19) 0.0042(14) -0.0022(16) -0.0059(15) C25 0.014(2) 0.0126(15) 0.0077(15) 0.0021(12) 0.0046(14) -0.0025(13) C17 0.014(2) 0.0151(16) 0.0161(17) -0.0014(13) 0.0038(15) -0.0001(14) C14 0.010(2) 0.0146(16) 0.036(2) -0.0069(15) -0.0023(17) -0.0020(15) C3 0.014(2) 0.0104(15) 0.0104(15) -0.0014(12) 0.0008(14) -0.0001(13) C11 0.016(2) 0.0140(16) 0.0169(17) 0.0002(13) 0.0001(15) 0.0001(14) C31 0.023(2) 0.0123(16) 0.028(2) -0.0023(15) 0.0030(17) -0.0067(16) C8 0.019(2) 0.0193(17) 0.0159(17) -0.0022(14) 0.0075(16) -0.0039(15) C15 0.010(2) 0.0148(17) 0.050(3) 0.0032(16) 0.0107(19) -0.0026(14) C16 0.016(2) 0.0239(18) 0.0231(19) 0.0034(15) 0.0080(16) 0.0002(15) C30 0.014(2) 0.0180(17) 0.0171(18) -0.0041(14) -0.0067(16) -0.0009(14) C28 0.016(2) 0.0229(18) 0.0169(18) 0.0050(14) 0.0050(16) 0.0032(15) C27 0.0099(19) 0.0312(18) 0.0173(17) 0.0026(16) -0.0021(14) -0.0049(17) C23 0.030(3) 0.0186(18) 0.027(2) -0.0091(15) 0.0133(18) -0.0093(16) C21 0.022(2) 0.0158(18) 0.038(2) -0.0097(16) -0.0038(18) -0.0063(15) C32 0.023(2) 0.0206(19) 0.0207(19) 0.0006(15) 0.0066(17) -0.0098(15) C22 0.037(3) 0.027(2) 0.041(2) -0.0222(18) 0.018(2) -0.0121(19) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ni1 P1 2.1976(8) . ? Ni1 C31 1.780(4) . ? Ni1 C30 1.806(4) . ? Ni1 C32 1.809(4) . ? P1 C1 1.853(3) . ? P1 C24 1.829(3) . ? P1 C5 1.835(3) . ? O1 C30 1.135(4) . ? O2 C31 1.147(4) . ? O3 C32 1.140(4) . ? C12 C1 1.476(4) . ? C12 C13 1.392(4) . ? C12 C17 1.395(4) . ? C1 C2 1.329(4) . ? C13 H13 0.9500 . ? C13 C14 1.381(5) . ? C24 C29 1.380(4) . ? C24 C25 1.401(4) . ? C7 H7 0.9500 . ? C7 C6 1.395(4) . ? C7 C8 1.388(4) . ? C19 H19 0.9500 . ? C19 C18 1.379(4) . ? C19 C20 1.383(4) . ? C5 C6 1.486(4) . ? C5 C4 1.320(4) . ? C29 H29 0.9500 . ? C29 C28 1.391(4) . ? C18 C3 1.528(4) . ? C18 C23 1.391(4) . ? C6 C11 1.387(4) . ? C2 H2 0.9500 . ? C2 C3 1.533(4) . ? C10 H10 0.9500 . ? C10 C9 1.383(5) . ? C10 C11 1.389(4) . ? C26 H26 0.9500 . ? C26 C25 1.380(4) . ? C26 C27 1.394(4) . ? C9 H9 0.9500 . ? C9 C8 1.385(4) . ? C4 H4 0.9500 . ? C4 C3 1.537(4) . ? C20 H20 0.9500 . ? C20 C21 1.377(5) . ? C25 C3 1.548(4) . ? C17 H17 0.9500 . ? C17 C16 1.382(5) . ? C14 H14 0.9500 . ? C14 C15 1.391(5) . ? C11 H11 0.9500 . ? C8 H8 0.9500 . ? C15 H15 0.9500 . ? C15 C16 1.379(5) . ? C16 H16 0.9500 . ? C28 H28 0.9500 . ? C28 C27 1.385(4) . ? C27 H27 0.9500 . ? C23 H23 0.9500 . ? C23 C22 1.391(4) . ? C21 H21 0.9500 . ? C21 C22 1.378(5) . ? C22 H22 0.9500 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C31 Ni1 P1 114.29(11) . . ? C31 Ni1 C30 109.98(15) . . ? C31 Ni1 C32 108.83(16) . . ? C30 Ni1 P1 106.71(10) . . ? C30 Ni1 C32 111.99(15) . . ? C32 Ni1 P1 105.01(10) . . ? C1 P1 Ni1 120.19(10) . . ? C24 P1 Ni1 122.16(10) . . ? C24 P1 C1 94.69(14) . . ? C24 P1 C5 96.25(14) . . ? C5 P1 Ni1 121.09(10) . . ? C5 P1 C1 96.03(14) . . ? C13 C12 C1 121.8(3) . . ? C13 C12 C17 118.7(3) . . ? C17 C12 C1 119.5(3) . . ? C12 C1 P1 121.3(2) . . ? C2 C1 P1 114.0(2) . . ? C2 C1 C12 124.5(3) . . ? C12 C13 H13 119.6 . . ? C14 C13 C12 120.8(3) . . ? C14 C13 H13 119.6 . . ? C29 C24 P1 123.8(2) . . ? C29 C24 C25 120.8(3) . . ? C25 C24 P1 115.4(2) . . ? C6 C7 H7 119.9 . . ? C8 C7 H7 119.9 . . ? C8 C7 C6 120.3(3) . . ? C18 C19 H19 119.2 . . ? C18 C19 C20 121.5(3) . . ? C20 C19 H19 119.2 . . ? C6 C5 P1 121.7(2) . . ? C4 C5 P1 114.6(2) . . ? C4 C5 C6 123.7(3) . . ? C24 C29 H29 120.1 . . ? C24 C29 C28 119.8(3) . . ? C28 C29 H29 120.1 . . ? C19 C18 C3 119.2(3) . . ? C19 C18 C23 118.1(3) . . ? C23 C18 C3 122.6(3) . . ? C7 C6 C5 120.4(3) . . ? C11 C6 C7 118.9(3) . . ? C11 C6 C5 120.7(3) . . ? C1 C2 H2 119.8 . . ? C1 C2 C3 120.3(3) . . ? C3 C2 H2 119.8 . . ? C9 C10 H10 120.3 . . ? C9 C10 C11 119.4(3) . . ? C11 C10 H10 120.3 . . ? C25 C26 H26 120.0 . . ? C25 C26 C27 120.0(3) . . ? C27 C26 H26 120.0 . . ? C10 C9 H9 119.8 . . ? C10 C9 C8 120.4(3) . . ? C8 C9 H9 119.8 . . ? C5 C4 H4 119.8 . . ? C5 C4 C3 120.4(3) . . ? C3 C4 H4 119.8 . . ? C19 C20 H20 120.0 . . ? C21 C20 C19 120.1(3) . . ? C21 C20 H20 120.0 . . ? C24 C25 C3 116.2(3) . . ? C26 C25 C24 119.2(3) . . ? C26 C25 C3 124.6(3) . . ? C12 C17 H17 119.9 . . ? C16 C17 C12 120.2(3) . . ? C16 C17 H17 119.9 . . ? C13 C14 H14 120.0 . . ? C13 C14 C15 120.0(3) . . ? C15 C14 H14 120.0 . . ? C18 C3 C2 114.3(3) . . ? C18 C3 C4 112.0(2) . . ? C18 C3 C25 111.2(3) . . ? C2 C3 C4 106.1(3) . . ? C2 C3 C25 105.7(2) . . ? C4 C3 C25 106.9(2) . . ? C6 C11 C10 121.0(3) . . ? C6 C11 H11 119.5 . . ? C10 C11 H11 119.5 . . ? O2 C31 Ni1 175.6(3) . . ? C7 C8 H8 120.0 . . ? C9 C8 C7 120.0(3) . . ? C9 C8 H8 120.0 . . ? C14 C15 H15 120.2 . . ? C16 C15 C14 119.5(3) . . ? C16 C15 H15 120.2 . . ? C17 C16 H16 119.6 . . ? C15 C16 C17 120.8(3) . . ? C15 C16 H16 119.6 . . ? O1 C30 Ni1 178.1(3) . . ? C29 C28 H28 120.2 . . ? C27 C28 C29 119.6(3) . . ? C27 C28 H28 120.2 . . ? C26 C27 H27 119.7 . . ? C28 C27 C26 120.6(3) . . ? C28 C27 H27 119.7 . . ? C18 C23 H23 119.8 . . ? C22 C23 C18 120.3(3) . . ? C22 C23 H23 119.8 . . ? C20 C21 H21 120.4 . . ? C20 C21 C22 119.2(3) . . ? C22 C21 H21 120.4 . . ? O3 C32 Ni1 179.1(3) . . ? C23 C22 H22 119.7 . . ? C21 C22 C23 120.6(3) . . ? C21 C22 H22 119.7 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ni1 P1 C1 C12 5.0(3) . . . . ? Ni1 P1 C1 C2 -179.01(19) . . . . ? Ni1 P1 C24 C29 0.6(3) . . . . ? Ni1 P1 C24 C25 -179.99(19) . . . . ? Ni1 P1 C5 C6 -0.1(3) . . . . ? Ni1 P1 C5 C4 177.7(2) . . . . ? P1 C1 C2 C3 0.5(4) . . . . ? P1 C24 C29 C28 179.3(2) . . . . ? P1 C24 C25 C26 -179.4(2) . . . . ? P1 C24 C25 C3 1.1(4) . . . . ? P1 C5 C6 C7 -55.5(4) . . . . ? P1 C5 C6 C11 125.5(3) . . . . ? P1 C5 C4 C3 0.8(4) . . . . ? C12 C1 C2 C3 176.3(3) . . . . ? C12 C13 C14 C15 -0.7(5) . . . . ? C12 C17 C16 C15 -0.7(5) . . . . ? C1 P1 C24 C29 131.0(3) . . . . ? C1 P1 C24 C25 -49.6(3) . . . . ? C1 P1 C5 C6 -130.9(3) . . . . ? C1 P1 C5 C4 46.9(3) . . . . ? C1 C12 C13 C14 179.1(3) . . . . ? C1 C12 C17 C16 -178.4(3) . . . . ? C1 C2 C3 C18 178.6(3) . . . . ? C1 C2 C3 C4 54.6(4) . . . . ? C1 C2 C3 C25 -58.7(4) . . . . ? C13 C12 C1 P1 -61.4(4) . . . . ? C13 C12 C1 C2 123.1(3) . . . . ? C13 C12 C17 C16 1.1(4) . . . . ? C13 C14 C15 C16 1.2(5) . . . . ? C24 P1 C1 C12 -126.7(3) . . . . ? C24 P1 C1 C2 49.3(2) . . . . ? C24 P1 C5 C6 133.7(3) . . . . ? C24 P1 C5 C4 -48.6(3) . . . . ? C24 C29 C28 C27 -0.2(5) . . . . ? C24 C25 C3 C18 -178.9(3) . . . . ? C24 C25 C3 C2 56.5(3) . . . . ? C24 C25 C3 C4 -56.4(4) . . . . ? C7 C6 C11 C10 -0.5(5) . . . . ? C19 C18 C3 C2 -159.3(3) . . . . ? C19 C18 C3 C4 -38.6(4) . . . . ? C19 C18 C3 C25 81.0(4) . . . . ? C19 C18 C23 C22 1.6(5) . . . . ? C19 C20 C21 C22 0.4(5) . . . . ? C5 P1 C1 C12 136.5(3) . . . . ? C5 P1 C1 C2 -47.5(3) . . . . ? C5 P1 C24 C29 -132.4(3) . . . . ? C5 P1 C24 C25 47.0(3) . . . . ? C5 C6 C11 C10 178.5(3) . . . . ? C5 C4 C3 C18 178.8(3) . . . . ? C5 C4 C3 C2 -55.8(4) . . . . ? C5 C4 C3 C25 56.7(4) . . . . ? C29 C24 C25 C26 0.0(5) . . . . ? C29 C24 C25 C3 -179.4(3) . . . . ? C29 C28 C27 C26 0.4(5) . . . . ? C18 C19 C20 C21 1.0(5) . . . . ? C18 C23 C22 C21 -0.2(6) . . . . ? C6 C7 C8 C9 -0.8(5) . . . . ? C6 C5 C4 C3 178.6(3) . . . . ? C10 C9 C8 C7 0.0(5) . . . . ? C26 C25 C3 C18 1.7(4) . . . . ? C26 C25 C3 C2 -122.9(3) . . . . ? C26 C25 C3 C4 124.2(3) . . . . ? C9 C10 C11 C6 -0.2(5) . . . . ? C4 C5 C6 C7 127.0(4) . . . . ? C4 C5 C6 C11 -52.1(5) . . . . ? C20 C19 C18 C3 -179.4(3) . . . . ? C20 C19 C18 C23 -2.0(5) . . . . ? C20 C21 C22 C23 -0.8(6) . . . . ? C25 C24 C29 C28 0.0(5) . . . . ? C25 C26 C27 C28 -0.5(5) . . . . ? C17 C12 C1 P1 118.1(3) . . . . ? C17 C12 C1 C2 -57.5(4) . . . . ? C17 C12 C13 C14 -0.4(4) . . . . ? C14 C15 C16 C17 -0.5(5) . . . . ? C3 C18 C23 C22 178.9(3) . . . . ? C11 C10 C9 C8 0.5(5) . . . . ? C8 C7 C6 C5 -178.0(3) . . . . ? C8 C7 C6 C11 1.0(5) . . . . ? C27 C26 C25 C24 0.3(5) . . . . ? C27 C26 C25 C3 179.7(3) . . . . ? C23 C18 C3 C2 23.4(4) . . . . ? C23 C18 C3 C4 144.1(3) . . . . ? C23 C18 C3 C25 -96.3(4) . . . . ? _iucr_refine_instructions_details ; TITL MR174_a.res in P2(1)/c REM Old TITL MR174 in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.127, Rweak 0.015, Alpha 0.068, Orientation as input REM Formula found by SHELXT: C32 O3 P Ni CELL 0.71073 11.9762 11.8806 18.6899 90 92.959 90 ZERR 4 0.0007 0.0006 0.001 0 0.004 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Ni O P UNIT 128 84 4 12 4 L.S. 50 PLAN 20 SIZE 0.04 0.09 0.15 TEMP -173.15 BOND $H LIST 6 fmap 2 MORE -1 ACTA 52 CONF REM REM REM WGHT 0.026400 0.875100 FVAR 0.45940 NI1 3 0.701402 0.122312 0.465645 11.00000 0.01486 0.01191 = 0.01282 -0.00084 0.00168 -0.00239 P1 5 0.738798 0.291435 0.508064 11.00000 0.01065 0.01007 = 0.01004 0.00010 0.00189 -0.00098 O1 4 0.589759 -0.002241 0.577647 11.00000 0.03116 0.03010 = 0.01781 0.00600 0.00023 -0.01394 O2 4 0.893432 -0.009248 0.423031 11.00000 0.02295 0.01961 = 0.06522 -0.01009 0.01453 -0.00033 O3 4 0.554018 0.160883 0.336725 11.00000 0.04017 0.05821 = 0.01856 0.01547 -0.01130 -0.02054 C12 1 0.536795 0.306152 0.587429 11.00000 0.00868 0.00738 = 0.01770 -0.00050 0.00073 0.00249 C1 1 0.638470 0.363500 0.564798 11.00000 0.01173 0.01262 = 0.00950 0.00225 -0.00082 -0.00037 C13 1 0.454521 0.267731 0.537997 11.00000 0.01462 0.01576 = 0.01867 -0.00227 -0.00202 0.00062 AFIX 43 H13 2 0.462950 0.279411 0.488281 11.00000 -1.20000 AFIX 0 C24 1 0.860595 0.319806 0.568445 11.00000 0.01120 0.01761 = 0.00688 -0.00163 0.00495 -0.00337 C7 1 0.817652 0.318440 0.335484 11.00000 0.01776 0.01664 = 0.01135 0.00413 0.00142 0.00000 AFIX 43 H7 2 0.866393 0.271218 0.363737 11.00000 -1.20000 AFIX 0 C19 1 0.880805 0.700024 0.555124 11.00000 0.01949 0.01675 = 0.01250 -0.00037 -0.00120 -0.00447 AFIX 43 H19 2 0.915989 0.670196 0.514848 11.00000 -1.20000 AFIX 0 C5 1 0.759231 0.410828 0.447806 11.00000 0.01001 0.01308 = 0.01315 0.00193 0.00336 0.00083 C29 1 0.937201 0.238877 0.590935 11.00000 0.01287 0.01408 = 0.01442 -0.00029 0.00586 -0.00135 AFIX 43 H29 2 0.927908 0.163152 0.575423 11.00000 -1.20000 AFIX 0 C18 1 0.805422 0.634343 0.589732 11.00000 0.01234 0.01200 = 0.01442 -0.00089 -0.00274 -0.00142 C6 1 0.751414 0.397462 0.368629 11.00000 0.01123 0.01136 = 0.01136 0.00241 0.00089 -0.00606 C2 1 0.670497 0.465848 0.585932 11.00000 0.01496 0.01310 = 0.01192 0.00124 0.00099 0.00088 AFIX 43 H2 2 0.624439 0.508820 0.615534 11.00000 -1.20000 AFIX 0 C10 1 0.673553 0.454064 0.252288 11.00000 0.02230 0.01971 = 0.01475 0.00471 -0.00408 -0.00246 AFIX 43 H10 2 0.623780 0.500088 0.223936 11.00000 -1.20000 AFIX 0 C26 1 0.963259 0.460831 0.636007 11.00000 0.01682 0.01728 = 0.01447 0.00022 -0.00034 -0.00460 AFIX 43 H26 2 0.972426 0.536454 0.651748 11.00000 -1.20000 AFIX 0 C9 1 0.740717 0.376302 0.220131 11.00000 0.02474 0.02519 = 0.00738 0.00104 0.00241 -0.00466 AFIX 43 H9 2 0.737495 0.369341 0.169430 11.00000 -1.20000 AFIX 0 C4 1 0.777206 0.508094 0.480552 11.00000 0.01328 0.01338 = 0.00994 0.00492 0.00388 0.00163 AFIX 43 H4 2 0.787620 0.574258 0.453141 11.00000 -1.20000 AFIX 0 C20 1 0.906357 0.808274 0.577686 11.00000 0.01739 0.01756 = 0.02208 0.00419 -0.00219 -0.00593 AFIX 43 H20 2 0.957693 0.852263 0.552504 11.00000 -1.20000 AFIX 0 C25 1 0.873056 0.431817 0.590879 11.00000 0.01420 0.01259 = 0.00774 0.00212 0.00457 -0.00247 C17 1 0.522533 0.288865 0.660194 11.00000 0.01373 0.01514 = 0.01614 -0.00142 0.00384 -0.00014 AFIX 43 H17 2 0.577160 0.315699 0.694723 11.00000 -1.20000 AFIX 0 C14 1 0.360804 0.212846 0.560350 11.00000 0.01032 0.01464 = 0.03627 -0.00690 -0.00235 -0.00197 AFIX 43 H14 2 0.304835 0.187804 0.526134 11.00000 -1.20000 AFIX 0 C3 1 0.781384 0.514917 0.562788 11.00000 0.01378 0.01040 = 0.01043 -0.00140 0.00084 -0.00014 C11 1 0.679510 0.464289 0.326439 11.00000 0.01574 0.01398 = 0.01691 0.00018 0.00013 0.00013 AFIX 43 H11 2 0.633615 0.517890 0.348588 11.00000 -1.20000 AFIX 0 C31 1 0.820960 0.045520 0.440736 11.00000 0.02282 0.01234 = 0.02753 -0.00234 0.00304 -0.00670 C8 1 0.812657 0.308506 0.261411 11.00000 0.01910 0.01926 = 0.01585 -0.00224 0.00751 -0.00395 AFIX 43 H8 2 0.858586 0.255200 0.239021 11.00000 -1.20000 AFIX 0 C15 1 0.348436 0.194274 0.632976 11.00000 0.01008 0.01479 = 0.04953 0.00322 0.01074 -0.00259 AFIX 43 H15 2 0.284810 0.155306 0.648541 11.00000 -1.20000 AFIX 0 C16 1 0.429233 0.232850 0.682236 11.00000 0.01605 0.02392 = 0.02310 0.00341 0.00801 0.00018 AFIX 43 H16 2 0.420634 0.220766 0.731895 11.00000 -1.20000 AFIX 0 C30 1 0.631554 0.047247 0.534522 11.00000 0.01393 0.01798 = 0.01706 -0.00407 -0.00670 -0.00087 C28 1 1.028106 0.268478 0.636401 11.00000 0.01617 0.02292 = 0.01690 0.00495 0.00502 0.00321 AFIX 43 H28 2 1.081038 0.213096 0.652185 11.00000 -1.20000 AFIX 0 C27 1 1.040944 0.379197 0.658505 11.00000 0.00989 0.03118 = 0.01725 0.00261 -0.00212 -0.00488 AFIX 43 H27 2 1.103251 0.399686 0.689275 11.00000 -1.20000 AFIX 0 C23 1 0.757663 0.678631 0.649870 11.00000 0.03042 0.01863 = 0.02696 -0.00907 0.01325 -0.00926 AFIX 43 H23 2 0.706924 0.634454 0.675409 11.00000 -1.20000 AFIX 0 C21 1 0.857515 0.852395 0.636585 11.00000 0.02200 0.01582 = 0.03795 -0.00973 -0.00376 -0.00634 AFIX 43 H21 2 0.874444 0.926905 0.652075 11.00000 -1.20000 AFIX 0 C32 1 0.610465 0.145323 0.386713 11.00000 0.02321 0.02059 = 0.02070 0.00065 0.00656 -0.00980 C22 1 0.783804 0.787261 0.672808 11.00000 0.03740 0.02721 = 0.04086 -0.02221 0.01763 -0.01212 AFIX 43 H22 2 0.750517 0.816849 0.713852 11.00000 -1.20000 AFIX 0 HKLF 4 REM MR174_a.res in P2(1)/c REM R1 = 0.0623 for 3945 Fo > 4sig(Fo) and 0.1322 for all 6595 data REM 334 parameters refined using 0 restraints END WGHT 0.0264 0.8749 REM Highest difference peak 0.436, deepest hole -0.513, 1-sigma level 0.101 Q1 1 0.7204 0.5037 0.5720 11.00000 0.05 0.44 Q2 1 0.6749 0.1006 0.5296 11.00000 0.05 0.42 Q3 1 0.8599 0.4585 0.5617 11.00000 0.05 0.39 Q4 1 0.5776 0.3446 0.5812 11.00000 0.05 0.39 Q5 1 0.6390 0.4154 0.5352 11.00000 0.05 0.38 Q6 1 0.6017 0.5033 0.3764 11.00000 0.05 0.37 Q7 1 0.4816 0.1637 0.5033 11.00000 0.05 0.37 Q8 1 0.8754 0.3732 0.5797 11.00000 0.05 0.36 Q9 1 0.7182 0.4397 0.4433 11.00000 0.05 0.36 Q10 1 0.7073 0.2206 0.4868 11.00000 0.05 0.35 Q11 1 0.7024 0.3000 0.4145 11.00000 0.05 0.35 Q12 1 0.6249 0.6378 0.3290 11.00000 0.05 0.35 Q13 1 0.6569 0.6072 0.6505 11.00000 0.05 0.34 Q14 1 0.7572 0.0769 0.5233 11.00000 0.05 0.34 Q15 1 0.6385 0.0997 0.4152 11.00000 0.05 0.34 Q16 1 0.4968 0.3262 0.6756 11.00000 0.05 0.34 Q17 1 0.9024 0.9769 0.7246 11.00000 0.05 0.34 Q18 1 0.7360 0.2218 0.4804 11.00000 0.05 0.34 Q19 1 0.7718 0.5317 0.5271 11.00000 0.05 0.34 Q20 1 0.4170 0.0930 0.5901 11.00000 0.05 0.34 REM The information below was added by Olex2. REM REM R1 = 0.0623 for 3945 Fo > 4sig(Fo) and 0.1322 for all 30508 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.44, deepest hole -0.51 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.1322 REM R1_gt = 0.0623 REM wR_ref = 0.1027 REM GOOF = 1.015 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 30508 REM Reflections_gt = 3945 REM Parameters = n/a REM Hole = -0.51 REM Peak = 0.44 REM Flack = n/a ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma -2 0 0 8167.88 190.78 -3 0 0 341.17 23.3 -4 0 0 135.49 20.6 -5 0 0 591.14 39.5 -6 0 0 223.08 33.9 -7 0 0 283.27 36.6 -8 0 0 78.69 26.7 -9 0 0 15.9 28.3 9 0 0 43.3 23.8 10 0 0 25.3 27.2 -10 0 0 -16.9 31.2 -11 0 0 -2.2 39.4 11 0 0 66.09 29.8 -12 0 0 417.46 74.69 -13 0 0 128.19 94.59 -14 0 0 93.19 76.29 -15 0 0 1.7 81.49 1 -1 0 4086.69 89.59 -1 -1 0 3713.93 86.39 1 -1 0 3827.12 89.99 -1 -1 0 3269.97 97.09 1 1 0 3496.05 92.29 2 -1 0 1089.49 33 -2 -1 0 1040.6 40.9 2 -1 0 1109.89 35.3 2 1 0 1059.39 40.7 3 -1 0 2287.47 61.09 -3 -1 0 2288.37 74.29 3 1 0 2300.77 73.49 -3 1 0 2191.78 63.09 -4 -1 0 178.78 25.3 4 -1 0 170.98 17.2 -4 1 0 173.58 19.2 -5 -1 0 227.18 31.8 5 -1 0 258.47 22.6 -5 1 0 224.18 25.6 -6 -1 0 1533.85 73.29 6 -1 0 1535.95 53.39 -6 1 0 1439.56 63.89 -7 -1 0 119.99 31.2 7 -1 0 28.7 18.7 -7 1 0 67.29 23.5 8 -1 0 534.05 37.3 -8 -1 0 536.75 55.89 -8 1 0 516.95 48.1 -9 -1 0 42 36.1 9 -1 0 8.8 23.5 -9 1 0 -9.2 24.5 -10 -1 0 694.03 71.99 10 -1 0 607.24 47.8 -10 1 0 680.13 61.89 11 -1 0 18.3 38.2 -11 -1 0 72.29 42.8 -11 1 0 42.2 42.1 -12 -1 0 198.78 58.39 -12 1 0 108.89 51.99 -13 -1 0 89.19 62.49 13 -1 0 14.3 53.79 -13 1 0 -72.89 52.29 -14 -1 0 20.4 70.79 -14 1 0 -69.49 62.39 -15 -1 0 199.78 92.89 -15 1 0 337.07 93.49 0 -2 0 2254.17 59.79 0 -2 0 1956.2 58.89 0 -2 0 2180.68 54.89 0 2 0 2255.77 57.79 1 -2 0 118.59 14.4 -1 -2 0 105.09 15.2 -1 -2 0 103.29 12.7 -1 -2 0 106.29 13.5 1 -2 0 103.79 9.5 1 2 0 104.69 15.4 -2 -2 0 903.61 32 2 -2 0 899.71 31.1 -2 -2 0 910.01 41.1 2 -2 0 940.11 34.1 2 2 0 817.92 39.8 3 -2 0 1175.88 42.7 -3 -2 0 1203.48 53.29 3 -2 0 1155.88 40.8 3 2 0 1162.88 52.29 4 -2 0 683.43 36.5 -4 -2 0 674.13 44.3 4 -2 0 748.73 33.3 -4 2 0 673.83 29.1 4 2 0 688.33 43.6 -5 -2 0 75.99 26.5 5 -2 0 104.99 19.6 -5 2 0 70.99 16.1 6 -2 0 120.79 21.1 -6 -2 0 120.19 31 -6 2 0 120.29 21.8 7 -2 0 64.09 20.3 -7 -2 0 45.2 27.3 -7 2 0 62.19 20.7 8 -2 0 41.6 21.5 -8 -2 0 7.3 27.5 -8 2 0 4.1 20.8 9 -2 0 125.89 28.1 -9 -2 0 141.29 41.4 -9 2 0 122.69 32.5 10 -2 0 457.15 67.09 -10 -2 0 385.06 61.79 -10 2 0 456.95 55.89 11 -2 0 575.64 54.69 -11 -2 0 496.75 73.19 -11 2 0 555.94 65.19 12 -2 0 3 33.3 -12 -2 0 -32.3 58.69 -12 2 0 1.8 41.1 13 -2 0 20.9 39.8 -13 -2 0 49.5 63.09 -13 2 0 87.69 57.49 14 -2 0 59.19 42.5 -14 -2 0 71.59 77.99 -14 2 0 160.98 99.89 -15 -2 0 -54.49 86.09 -15 2 0 -38.1 73.99 0 -3 0 -4.3 6.3 0 -3 0 -11 9.1 0 -3 0 0.6 7.6 0 3 0 1.5 7.9 0 3 0 -6.2 6.8 1 -3 0 5871.41 142.09 1 -3 0 6074.49 133.19 -1 -3 0 5985.9 141.89 -1 -3 0 5537.65 143.69 -1 -3 0 5586.84 141.09 1 3 0 5569.34 145.29 -1 3 0 5241.08 128.29 -1 3 0 5209.98 127.39 2 -3 0 3640.44 89.99 -2 -3 0 3420.46 94.99 -2 -3 0 3477.35 105.49 2 -3 0 3654.23 97.99 2 3 0 3484.15 105.79 3 -3 0 19.8 11.9 -3 -3 0 31.5 18 -3 -3 0 43.6 12.8 3 -3 0 47.6 15 3 3 0 32.6 18.8 4 -3 0 1112.09 46.4 -4 -3 0 1102.59 59.39 4 -3 0 1114.69 46.6 4 3 0 1141.49 60.29 5 -3 0 179.98 26.7 -5 -3 0 105.69 26.8 5 -3 0 105.49 22.7 5 3 0 122.09 30 -5 3 0 119.39 15.9 -6 -3 0 298.87 45.6 6 -3 0 368.86 31.8 -6 3 0 284.47 25.6 7 -3 0 135.79 24.7 -7 -3 0 92.09 34.3 -7 3 0 59.79 20.1 8 -3 0 24.6 23.4 -8 -3 0 29 32.9 -8 3 0 0.3 17.9 -9 -3 0 86.99 38.3 9 -3 0 91.49 33.3 -9 3 0 135.99 31.8 -10 -3 0 280.57 57.99 10 -3 0 318.17 41.2 -10 3 0 284.07 43.9 -11 -3 0 84.49 51.69 11 -3 0 107.19 36.6 -11 3 0 126.09 41.1 -12 -3 0 98.09 55.69 12 -3 0 -21.6 35.7 -12 3 0 -14.9 42.6 13 -3 0 85.99 41.3 -13 -3 0 33.5 66.29 -13 3 0 132.99 52.09 14 -3 0 291.87 53.99 -14 -3 0 413.06 96.49 -14 3 0 482.75 91.49 14 3 0 345.57 52.39 -15 -3 0 282.87 100.19 -15 3 0 -26 73.69 0 -4 0 79.99 11.5 0 -4 0 79.99 13 0 -4 0 91.19 16.7 0 4 0 92.49 14.4 0 4 0 101.79 16 -1 -4 0 16.7 11.7 -1 -4 0 38.6 14.1 1 -4 0 -0.7 13.3 -1 -4 0 8.8 12.3 1 -4 0 8.5 9.6 1 4 0 4.9 12.8 -1 4 0 5.8 7.8 -1 4 0 7.8 8.7 -2 -4 0 2583.54 79.99 2 -4 0 2687.03 82.89 -2 -4 0 2551.64 83.59 -2 -4 0 2510.15 87.09 2 -4 0 2634.14 71.49 2 4 0 2571.84 89.59 -3 -4 0 679.13 36.4 -3 -4 0 669.13 45.2 3 -4 0 641.64 32.2 3 -4 0 739.13 39.2 3 4 0 592.04 45.4 4 -4 0 302.47 27.6 4 -4 0 260.57 27.7 -4 -4 0 199.68 35.5 -4 -4 0 257.67 26.7 4 4 0 262.37 38.5 5 -4 0 841.22 45.5 5 -4 0 908.51 46.1 -5 -4 0 870.51 60.69 5 4 0 885.31 61.59 -6 -4 0 131.89 36.7 6 -4 0 211.38 31.2 6 -4 0 187.78 29.5 -6 4 0 160.98 19.3 7 -4 0 770.92 49.4 -7 -4 0 818.72 62.59 -7 4 0 791.52 41.8 -8 -4 0 172.18 47.6 8 -4 0 201.28 33.5 -8 4 0 130.59 26.1 -9 -4 0 404.26 61.99 9 -4 0 428.36 46.3 -9 4 0 435.76 43 -10 -4 0 213.48 59.39 10 -4 0 229.18 42.5 11 -4 0 -0.7 32.8 -11 4 0 70.79 35.7 12 -4 0 291.47 47.6 -12 -4 0 377.56 81.99 -12 4 0 351.66 58.59 -13 -4 0 128.09 83.39 13 -4 0 185.48 47.6 -13 4 0 230.38 57.89 -14 -4 0 125.49 85.99 14 -4 0 91.99 50.69 -14 4 0 55.89 61.99 -15 -4 0 220.08 111.89 -15 4 0 181.28 84.59 0 -5 0 1 14.3 0 -5 0 -12.6 9.5 0 -5 0 15.5 9.6 0 5 0 -5.2 11.7 0 5 0 -1.6 11.4 -1 -5 0 48.6 18.9 -1 -5 0 33.5 15.3 1 -5 0 34.9 13.1 1 -5 0 37.7 18.7 -1 -5 0 35.4 16.6 1 5 0 36.9 18.1 -1 5 0 41.8 13.2 -1 5 0 27.1 11 -2 -5 0 1227.58 54.69 -2 -5 0 1180.78 57.79 -2 -5 0 1252.17 54.59 2 -5 0 1240.08 44.1 2 -5 0 1161.28 54.79 -2 5 0 1177.28 38 2 5 0 1212.18 60.59 3 -5 0 -6 12.3 -3 -5 0 6.2 16.7 -3 -5 0 32.3 18.6 -3 -5 0 11.6 20.6 3 5 0 23.5 21.8 -4 -5 0 159.78 34.2 4 -5 0 218.58 32.1 4 -5 0 145.79 22.7 4 5 0 167.68 35.4 5 -5 0 261.17 32.6 -5 -5 0 304.07 42.4 5 -5 0 225.38 29.6 5 5 0 259.57 43.2 -5 5 0 205.58 11.9 6 -5 0 401.66 39.4 -6 -5 0 337.27 48.9 6 -5 0 381.26 37 -6 5 0 361.76 22.8 -7 -5 0 8.1 29.9 -7 5 0 0.3 12.7 -8 -5 0 49.6 40.5 8 -5 0 42.5 28.6 -8 5 0 64.39 20.7 9 -5 0 250.27 39.4 -9 -5 0 287.97 58.99 -9 5 0 252.47 35.5 -10 -5 0 -36.7 49 10 -5 0 -14.2 31.9 -10 5 0 26.7 25.1 11 -5 0 261.27 48 -11 -5 0 357.46 76.89 -11 5 0 304.37 49.1 12 -5 0 18.7 39.5 -12 -5 0 -18.2 61.39 -12 5 0 -16.5 38.4 13 -5 0 99.49 47.8 -13 -5 0 229.78 84.19 -13 5 0 165.18 53.99 -14 -5 0 453.95 105.29 14 -5 0 279.97 61.19 -14 5 0 300.07 74.39 -15 -5 0 37.7 111.49 15 -5 0 126.89 55.39 -15 5 0 133.79 82.29 0 -6 0 1163.08 42.7 0 -6 0 1238.28 59.09 0 -6 0 1250.17 45.1 0 6 0 1266.67 56.39 0 6 0 1244.78 52.79 1 -6 0 54.59 23.1 -1 -6 0 22.1 15.9 -1 -6 0 13.7 15.9 -1 -6 0 13.9 19.9 1 -6 0 15.6 14.4 -1 6 0 25.6 14.8 -1 6 0 31.8 13.1 1 6 0 62.89 22.8 -2 -6 0 57.89 20.6 2 -6 0 86.09 17.5 -2 -6 0 55.19 21.9 -2 -6 0 78.09 23.3 2 -6 0 57.49 23.1 -2 6 0 66.19 12.9 -2 6 0 68.99 14.2 2 6 0 59.69 24.6 3 -6 0 326.07 35.9 -3 -6 0 272.87 35.6 -3 -6 0 268.57 32.6 -3 -6 0 253.57 38.7 3 -6 0 253.77 26.9 3 6 0 308.27 40.7 -3 6 0 268.47 16.6 -4 -6 0 498.85 40 -4 -6 0 493.65 44.8 -4 -6 0 444.66 46.1 4 -6 0 399.76 40 4 -6 0 427.66 33.8 4 6 0 456.95 49.3 -4 6 0 416.26 14.7 -4 6 0 402.26 14.5 5 -6 0 138.59 29.8 5 -6 0 102.09 25 -5 -6 0 85.59 29.8 -5 -6 0 122.29 27.8 -5 -6 0 134.39 35.6 5 6 0 90.19 35.6 -5 6 0 84.79 8 6 -6 0 12.5 22.6 6 -6 0 2.5 24.5 -6 -6 0 23.3 31.4 -7 -6 0 26.9 39.7 7 -6 0 -7.5 25.3 -7 6 0 34.1 13.4 8 -6 0 48 28.6 -8 -6 0 49.4 44.1 -8 6 0 17 17.1 9 -6 0 47.5 32.8 -9 -6 0 37.6 47.9 -9 6 0 62.99 23.5 -10 -6 0 91.19 76.79 10 -6 0 63.39 37.9 -10 6 0 84.79 28.4 -11 -6 0 -31.3 61.29 11 -6 0 23.1 37.7 -11 6 0 -9.3 31.3 -12 -6 0 -4.8 68.39 12 -6 0 -6.1 42 -12 6 0 17.4 38.7 -13 -6 0 -96.39 81.89 13 -6 0 18.1 45.6 -13 6 0 -23.6 48.5 -14 -6 0 -32.7 100.69 14 -6 0 -34 47.7 -14 6 0 21.1 61.09 0 -7 0 22.7 23.4 0 -7 0 -0.3 9.2 0 -7 0 4.2 12.1 0 7 0 6.1 14.6 0 7 0 -0.1 17.3 1 -7 0 249.78 27.8 1 -7 0 290.47 36.5 -1 -7 0 248.18 36.5 -1 -7 0 290.17 30 -1 -7 0 199.68 27.9 -1 7 0 275.17 26.4 -1 7 0 238.08 28.6 1 7 0 266.37 37.3 -2 -7 0 33.9 20.1 2 -7 0 -11 15.9 -2 -7 0 -14 18.9 2 -7 0 11.1 19.3 -2 -7 0 22.3 19 -2 7 0 -7.8 11.1 2 7 0 -12 21.8 -2 7 0 2.7 13.3 -3 -7 0 907.31 55.49 3 -7 0 747.13 53.19 3 -7 0 922.51 44 -3 -7 0 814.02 53.09 -3 -7 0 781.92 58.79 -3 7 0 902.21 36.4 -3 7 0 907.61 35.3 3 7 0 842.22 63.39 -4 -7 0 1136.59 71.69 4 -7 0 1094.09 52.19 -4 -7 0 1063.19 58.99 -4 -7 0 1108.69 65.39 4 -7 0 1050.39 63.09 4 7 0 1167.78 74.69 5 -7 0 121.09 28.3 -5 -7 0 85.59 39.6 -5 -7 0 89.49 27.4 -5 -7 0 101.49 33.9 5 -7 0 74.59 29.1 -5 7 0 76.29 14.7 5 7 0 126.09 40 6 -7 0 239.18 37.2 6 -7 0 184.68 41.2 -6 -7 0 248.78 45.7 -6 -7 0 210.88 51.89 7 -7 0 802.52 58.59 7 -7 0 766.22 59.69 -7 -7 0 958.9 85.09 -7 -7 0 991.6 76.59 -7 7 0 782.12 35.6 -8 -7 0 12.1 47.3 8 -7 0 26.4 32.2 -8 -7 0 2.4 42.1 -8 7 0 20.2 15.7 9 -7 0 145.89 40 -9 -7 0 210.98 67.59 -9 7 0 114.89 26.8 10 -7 0 -2.7 37.6 -10 -7 0 -35.1 51.69 -10 -7 0 -12.7 63.39 -10 7 0 -4 25.5 -11 -7 0 -94.09 65.49 11 -7 0 53.89 38.8 -11 -7 0 171.08 72.49 -11 7 0 168.28 36.1 -12 -7 0 92.39 83.19 12 -7 0 94.79 48.8 -12 -7 0 48.6 79.49 -12 7 0 220.68 47 -13 -7 0 89.39 101.99 13 -7 0 84.79 50.19 -13 7 0 120.09 52.09 -14 -7 0 2.1 113.59 14 -7 0 178.78 59.79 -14 7 0 112.19 63.79 0 -8 0 332.57 42.5 0 -8 0 422.06 25.8 0 -8 0 404.36 24 0 8 0 441.16 42.5 -1 -8 0 69.39 27.4 -1 -8 0 92.89 22 -1 -8 0 59.69 21.8 1 -8 0 65.79 29.2 1 -8 0 51.39 22.1 1 8 0 132.49 30.5 -1 8 0 54.29 23.2 -1 8 0 85.39 21.4 -2 -8 0 94.39 28.2 -2 -8 0 127.89 30.5 2 -8 0 161.88 36.7 2 -8 0 175.88 25.4 -2 -8 0 116.79 30.5 -2 8 0 131.79 22.3 2 8 0 163.88 36.8 -2 8 0 106.49 23.1 -3 -8 0 859.21 63.39 3 -8 0 995 64.09 -3 -8 0 909.51 59.49 -3 -8 0 871.91 58.09 3 8 0 886.21 67.39 -3 8 0 857.91 39.8 4 -8 0 116.19 26.4 -4 -8 0 65.69 36.1 -4 -8 0 114.09 30.5 -4 -8 0 192.28 37.5 4 -8 0 137.99 36.3 -4 8 0 134.59 18.5 4 8 0 155.38 43.9 -5 -8 0 132.69 39.1 5 -8 0 94.69 30.4 -5 -8 0 101.39 33 5 -8 0 148.19 38.1 -5 -8 0 159.38 45.7 -5 8 0 100.29 14.6 -6 -8 0 75.59 45.6 6 -8 0 21.9 29.9 6 -8 0 43.4 31.8 -6 8 0 49.3 16 -7 -8 0 190.68 59.69 7 -8 0 236.28 42.1 -7 -8 0 243.18 53.99 7 -8 0 189.38 43 -7 8 0 256.57 22.8 -8 -8 0 460.05 81.59 8 -8 0 478.65 59.09 -8 -8 0 504.05 72.79 -8 8 0 467.95 32.4 9 -8 0 66.69 39.1 -9 -8 0 101.29 65.59 -9 8 0 131.29 24.6 -10 -8 0 548.85 85.79 -10 -8 0 485.45 96.29 10 -8 0 387.66 59.59 -10 8 0 489.95 45 -11 -8 0 226.08 85.39 11 -8 0 165.28 50.69 -11 -8 0 283.87 79.39 -11 8 0 178.78 38.1 -12 -8 0 189.58 100.89 12 -8 0 265.37 58.29 -12 8 0 266.37 46.4 13 -8 0 182.68 59.59 -13 -8 0 -40.7 103.59 -13 8 0 101.79 53.89 0 -9 0 36.2 30.5 0 -9 0 0 12.5 0 -9 0 -6 23.6 0 9 0 22.7 24.4 -1 -9 0 74.99 24.6 -1 -9 0 64.79 28.6 -1 -9 0 114.19 24.5 1 -9 0 37.1 32 1 -9 0 38.5 24.5 -1 9 0 102.29 25 1 9 0 81.69 32.2 -1 9 0 56.39 25.9 -2 -9 0 789.12 60.19 -2 -9 0 720.23 55.29 -2 -9 0 707.43 52.19 2 -9 0 747.13 60.49 2 -9 0 674.63 45.2 -2 9 0 712.93 44.6 2 9 0 930.81 70.39 -3 -9 0 81.49 34.4 3 -9 0 69.69 24.9 3 -9 0 139.49 39.7 -3 -9 0 77.99 35.4 -3 -9 0 50.79 31.1 3 9 0 77.89 38.5 -3 9 0 46.7 18.4 4 -9 0 1518.05 85.89 -4 -9 0 1598.04 90.59 -4 -9 0 1419.06 84.79 4 -9 0 1711.33 69.69 -4 -9 0 1509.55 82.79 -4 9 0 1526.45 57.39 -5 -9 0 408.86 63.09 5 -9 0 404.76 46.1 5 -9 0 352.66 56.49 -5 -9 0 453.95 61.29 -5 -9 0 379.96 48.9 -5 9 0 356.36 25.9 6 -9 0 -6.1 33 -6 -9 0 6.9 38 -6 -9 0 41.5 49.9 -6 -9 0 52.99 33.7 6 -9 0 -12 30.3 -6 9 0 5.1 12.6 -7 -9 0 47.9 47.9 7 -9 0 101.49 39.3 -7 -9 0 20.4 57.09 7 -9 0 10.5 38.1 8 -9 0 -12 34.3 -8 9 0 17.3 16.3 9 -9 0 289.17 56.69 -9 -9 0 315.37 88.79 -9 -9 0 110.29 61.39 -9 9 0 241.08 34.3 -10 -9 0 96.59 78.79 -10 -9 0 -21.8 73.89 10 -9 0 67.39 45.7 -10 9 0 7 25.8 11 -9 0 -54.49 42.2 -11 -9 0 11.9 81.99 -11 -9 0 175.18 98.49 -11 9 0 -64.79 31 12 -9 0 56.89 53.29 -12 -9 0 -44.5 99.19 -12 9 0 -16.5 39.7 -13 -9 0 192.38 123.39 13 -9 0 157.68 60.89 0 -10 0 490.95 57.99 0 -10 0 498.55 48.1 1 -10 0 -23.1 28.5 1 -10 0 12.5 25.9 -1 -10 0 6 19 -1 -10 0 12.6 22 -1 -10 0 -34.8 28.5 -2 -10 0 420.36 48.2 -2 -10 0 422.46 48.7 -2 -10 0 338.57 51.39 2 -10 0 486.55 57.59 2 -10 0 467.35 44.7 -2 10 0 371.76 40 -3 -10 0 96.99 37.5 -3 -10 0 93.09 38.6 3 -10 0 72.59 29.3 3 -10 0 128.39 42.4 -3 -10 0 110.99 37.7 -3 10 0 59.89 23 -4 -10 0 425.46 62.99 -4 -10 0 403.86 57.79 -4 -10 0 320.47 54.59 4 -10 0 500.65 47.8 4 -10 0 383.26 57.19 -4 10 0 419.26 35.4 -5 -10 0 114.89 39.3 5 -10 0 123.99 34.5 -5 -10 0 79.29 52.99 5 -10 0 133.99 44.8 -5 -10 0 119.89 51.59 -5 10 0 98.39 21.8 -6 -10 0 490.35 70.99 -6 -10 0 520.75 62.79 -6 -10 0 496.85 77.89 6 -10 0 437.66 63.19 6 -10 0 406.56 55.89 -6 10 0 468.75 32 7 -10 0 31.5 39.2 -7 -10 0 113.09 54.89 -7 -10 0 58.49 62.19 7 -10 0 -11.1 46.5 -7 10 0 29.9 15.9 8 -10 0 231.78 55.29 -8 -10 0 378.86 89.99 -8 10 0 209.98 26.6 -9 -10 0 92.19 81.89 -9 -10 0 64.69 66.29 9 -10 0 21 43.6 -9 10 0 22.9 21.6 -10 -10 0 -84.09 81.99 -10 -10 0 -49.4 77.59 10 -10 0 -70.29 42.3 -10 10 0 2.9 26.9 11 -10 0 47 53.19 -11 -10 0 115.19 103.79 -11 10 0 73.29 33.8 12 -10 0 120.09 55.59 -12 -10 0 -89.49 111.39 -12 10 0 -0.6 40 0 -11 0 -58.49 30.1 0 -11 0 62.39 36.7 1 -11 0 447.26 64.39 -1 -11 0 455.45 37 1 -11 0 467.95 50.39 -1 -11 0 384.56 34.9 -1 -11 0 391.26 58.69 2 -11 0 354.06 48.5 -2 -11 0 420.96 50.69 2 -11 0 341.37 58.19 -2 -11 0 344.97 47 -2 -11 0 371.16 57.99 -3 -11 0 863.01 73.19 -3 -11 0 910.51 75.89 3 -11 0 908.91 78.19 3 -11 0 810.32 57.89 -3 -11 0 859.11 71.69 -3 11 0 861.91 54.99 -4 -11 0 310.17 56.89 -4 -11 0 239.68 54.99 4 -11 0 246.08 40.8 4 -11 0 207.98 54.29 -4 -11 0 207.98 49.4 -4 11 0 255.57 37.3 -5 -11 0 271.17 53.99 -5 -11 0 224.08 62.59 5 -11 0 126.29 47.5 -5 -11 0 287.37 64.59 5 -11 0 248.88 42.5 -5 11 0 237.98 32.8 6 -11 0 775.12 74.69 -6 -11 0 750.12 91.09 -6 -11 0 828.32 92.89 -6 -11 0 594.74 70.89 -6 11 0 662.73 43.2 -7 -11 0 112.19 73.79 7 -11 0 138.19 49.8 -7 11 0 127.79 24.6 -8 -11 0 355.76 90.89 -8 -11 0 291.07 78.79 8 -11 0 299.17 60.59 -8 11 0 310.37 32.9 -9 -11 0 83.39 79.49 9 -11 0 64.59 50.49 -9 -11 0 -99.39 81.29 -9 11 0 -14.7 22.2 10 -11 0 57.69 54.79 -10 -11 0 54.09 98.89 -10 11 0 85.79 28.9 -11 -11 0 343.47 117.99 11 -11 0 28.4 51.69 -11 11 0 94.19 34.3 0 -12 0 1568.34 96.39 0 -12 0 1570.84 82.89 -1 -12 0 84.19 42.8 1 -12 0 97.29 57.49 1 -12 0 149.39 47.2 -1 -12 0 114.19 44 -2 -12 0 590.24 70.19 2 -12 0 709.53 73.69 -2 -12 0 708.53 60.49 2 -12 0 689.53 60.79 3 -12 0 795.02 78.39 3 -12 0 767.72 61.69 -3 -12 0 642.14 71.49 -3 -12 0 625.84 72.09 -4 -12 0 166.58 57.69 -4 -12 0 284.37 61.59 4 -12 0 85.49 45.9 4 -12 0 166.28 43.3 -4 -12 0 79.19 41.3 -4 12 0 161.78 34.5 -5 -12 0 402.16 66.49 -5 -12 0 511.25 79.09 -5 -12 0 416.16 80.99 5 -12 0 490.65 62.49 5 -12 0 415.46 67.89 -5 12 0 454.85 45 -6 -12 0 210.78 57.49 -6 -12 0 133.49 66.09 6 -12 0 209.68 54.89 -6 -12 0 134.49 78.79 6 -12 0 157.98 46.3 -6 12 0 184.28 31.5 7 -12 0 89.29 47.6 -7 -12 0 98.09 80.09 -7 12 0 27.3 25.1 -8 -12 0 116.19 93.29 8 -12 0 78.89 50.79 -8 -12 0 -69.39 80.79 -8 12 0 102.89 25.9 -9 -12 0 62.89 97.79 -9 -12 0 260.67 110.99 9 -12 0 180.38 63.09 -9 12 0 170.88 29 10 -12 0 -4.1 48.5 -10 -12 0 -127.79 109.69 0 -13 0 -33 33.1 0 -13 0 -65.69 36.2 -1 -13 0 263.87 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69.39 -1 1 4 2380.56 60.59 0 -1 4 25.1 10.7 0 -1 -4 28.1 12.8 0 -1 4 11.9 10.4 0 1 4 17.7 12.1 0 1 4 20.6 8.8 0 1 -4 -5.4 9.3 1 -1 4 4601.64 116.99 -1 -1 -4 4719.73 114.29 -1 -1 -4 4542.85 123.69 1 -1 4 5046.29 123.69 1 1 4 4749.02 118.99 -1 1 -4 4442.16 117.69 1 1 4 4723.33 124.69 2 -1 4 5.1 8.1 -2 -1 -4 24.5 7.5 2 -1 4 12.2 12.1 -2 -1 -4 21.2 13.2 2 1 4 13.7 11.7 2 1 4 -3.2 9.9 -2 1 -4 8.5 9 3 -1 4 891.71 44.7 -3 -1 -4 917.61 44.6 -3 -1 -4 967.2 26.9 3 1 4 981 45.7 -3 1 -4 911.91 38.1 -4 -1 -4 2146.69 78.49 4 -1 4 2272.07 80.89 4 1 4 2112.99 79.59 -4 1 -4 2148.09 69.99 -5 -1 -4 417.46 36.8 5 -1 4 457.25 40.3 5 1 4 377.26 38.9 6 -1 4 66.19 27.1 7 -1 4 185.68 38.5 -8 -1 -4 106.69 37.2 -9 -1 -4 26.7 36.3 -9 1 -4 88.89 33.1 -10 -1 -4 618.04 76.29 -10 1 -4 608.14 67.59 -11 -1 -4 59.29 47.8 -11 1 -4 113.59 47 -12 -1 -4 21.4 55.99 -12 1 -4 102.49 53.89 -13 -1 -4 29.9 66.39 -13 1 -4 -44.4 55.99 -14 -1 -4 -26.1 76.39 -14 1 -4 44.1 72.89 -15 -1 -4 185.18 99.59 -15 1 -4 169.08 94.69 15 -2 -4 60.39 56.29 -15 -2 4 108.59 92.29 15 2 -4 121.19 57.39 -15 2 4 90.59 87.49 -14 -2 4 151.98 78.79 14 -2 -4 103.19 51.19 -14 2 4 58.69 66.49 -13 -2 4 319.07 75.49 13 -2 -4 120.59 49.8 -13 2 4 279.17 71.09 -12 -2 4 64.79 57.39 12 -2 -4 19.4 38.8 -12 2 4 29.9 48.2 -11 -2 4 149.09 54.69 11 -2 -4 36.4 36.8 -11 2 4 93.59 44.8 -10 -2 4 -24.5 35.1 10 -2 -4 24.6 32.9 10 2 -4 -15.4 42.2 -10 2 4 34.3 32.6 -9 -2 4 -26.4 31.2 9 -2 -4 -5.7 27 9 2 -4 57.39 38.4 -9 2 4 -8.2 25.1 -8 -2 4 -20.9 28.6 8 -2 -4 -11.9 23.9 -8 2 4 8 24.6 8 2 -4 1 29.3 7 -2 -4 531.15 43.3 -7 -2 4 467.25 51.69 7 -2 -4 521.75 38.2 -7 2 4 486.85 44.7 7 2 -4 438.76 50.39 -6 -2 4 4.7 19 6 -2 -4 0.8 16 6 -2 -4 -11.9 20.7 6 2 -4 12.4 23.1 -6 2 4 15.6 19.7 5 -2 -4 360.06 30.2 -5 -2 4 366.26 41.5 5 -2 -4 314.27 34.9 5 2 -4 321.77 39.6 -5 2 4 376.36 32.9 4 -2 -4 -1.8 11.7 -4 -2 4 -14.1 17.1 4 -2 -4 0.6 17.9 -4 2 4 28.5 16.3 4 2 -4 -18 16.1 3 -2 -4 434.46 31.6 -3 -2 4 378.06 33.1 3 -2 -4 346.27 26.7 -3 2 4 403.36 28.7 3 2 -4 367.86 33.8 2 -2 -4 4788.42 128.59 -2 -2 4 4746.43 132.39 2 -2 -4 4597.74 124.69 -2 2 4 4757.22 126.99 2 2 -4 4847.21 134.79 1 -2 -4 -6.7 10.4 1 -2 -4 0.3 9.9 -1 -2 4 11 10.7 -1 2 4 -4.5 10.4 1 2 -4 -0.7 10.7 -1 2 4 9.3 6 0 -2 4 21.2 9.9 0 -2 -4 44.2 13 0 -2 4 26.6 13 0 -2 -4 27.1 12.2 0 2 -4 26.5 11.5 0 2 4 35.8 13 0 2 4 32.9 8.1 1 -2 4 47.1 9.3 -1 -2 -4 58.19 13.4 -1 -2 -4 43.8 13 1 -2 4 32.5 12.9 1 2 4 34.4 14.5 -1 2 -4 53.09 10.9 1 2 4 56.69 13.6 -2 -2 -4 2105.89 72.39 -2 -2 -4 1969.7 58.29 2 -2 4 2175.38 69.79 2 -2 4 2023.1 58.59 2 2 4 2006.2 65.99 -2 2 -4 1982.4 57.79 2 2 4 1998 70.19 3 -2 4 279.37 27.4 -3 -2 -4 265.37 29.4 -3 -2 -4 285.27 17.5 3 -2 4 297.37 18.8 3 2 4 290.37 28 -3 2 -4 282.07 18.9 -4 -2 -4 38.8 9.5 4 -2 4 46.7 19.4 -4 -2 -4 54.79 19.4 4 -2 4 35.1 11.1 -5 -2 -4 13.1 20.6 5 -2 4 13.5 10.9 5 -2 4 31.8 20.2 -6 -2 -4 709.53 51.69 6 -2 4 747.73 52.29 6 -2 4 783.22 30.7 7 -2 4 271.37 41.9 -7 -2 -4 205.18 41.4 7 -2 4 222.18 20.4 -7 -2 -4 249.97 40.6 8 -2 4 221.78 22.2 -8 -2 -4 147.29 41.6 8 -2 4 197.38 42 9 -2 4 101.39 17.4 -9 -2 -4 76.19 41.7 10 -2 4 91.99 16.7 -10 -2 -4 75.29 43.6 -10 2 -4 30.5 29.4 -11 -2 -4 14.3 51.29 -11 2 -4 28.8 41.8 -12 -2 -4 281.27 109.09 -12 2 -4 188.58 56.29 -13 -2 -4 168.48 74.19 -13 -2 -4 48.2 66.49 -13 2 -4 84.19 58.49 -14 -2 -4 75.99 77.19 -14 -2 -4 115.69 89.59 -14 2 -4 52.09 76.39 -15 -2 -4 195.58 99.09 -15 2 -4 28.6 85.09 -15 -3 4 -36.7 97.39 15 -3 -4 53.99 55.19 -15 3 4 -33.9 78.19 14 -3 -4 89.09 51.89 -14 -3 4 26.5 76.09 -14 3 4 114.19 70.69 13 -3 -4 534.15 67.59 -13 -3 4 396.16 94.19 -13 3 4 587.14 84.49 12 -3 -4 31.9 41.6 -12 -3 4 67.79 57.99 -12 3 4 23.8 47.8 -11 -3 4 103.39 58.29 11 -3 -4 152.38 43.4 -11 3 4 100.49 48.7 -10 -3 4 94.29 44 10 -3 -4 120.29 39.8 10 3 -4 67.79 49.3 -10 3 4 173.38 43.3 -9 -3 4 -28.3 32.2 9 -3 -4 -36.6 29.3 9 3 -4 42.2 39.8 -9 3 4 -9.5 27.1 8 -3 -4 190.48 36.5 -8 -3 4 223.48 48.9 -8 3 4 207.88 34.9 8 3 -4 237.88 48.3 -7 -3 4 337.77 52.89 7 -3 -4 342.47 42.8 7 3 -4 371.36 51.29 -7 3 4 307.57 36.2 6 -3 -4 317.47 25 6 -3 -4 284.27 36.6 -6 -3 4 293.67 44.2 6 3 -4 293.27 45.9 -6 3 4 275.37 32.4 -5 -3 4 43.9 25.4 5 -3 -4 48.3 14.7 5 -3 -4 17.4 21.8 -5 3 4 41.1 18.6 5 3 -4 49.9 28.4 4 -3 -4 748.33 35 4 -3 -4 819.52 46.8 -4 -3 4 769.42 51.99 -4 3 4 788.72 41.3 4 3 -4 721.23 51.19 3 -3 -4 1.9 10.9 -3 -3 4 16.4 15.8 3 -3 -4 13.1 15.3 -3 3 4 0.6 11.8 3 3 -4 0.8 20 2 -3 -4 488.15 33.6 2 -3 -4 508.05 28.5 -2 -3 4 504.85 34.5 2 3 -4 482.45 36.2 -2 3 4 494.25 30.4 1 -3 -4 17 11.9 -1 -3 4 14.7 12.2 1 -3 -4 25.7 14.1 -1 3 4 14.3 12.1 1 3 -4 -4.2 12.1 0 -3 4 1205.58 42.9 0 -3 -4 1338.57 50.09 0 -3 -4 1272.07 50.29 0 -3 4 1331.97 51.39 0 3 -4 1220.18 46.8 0 3 4 1242.88 51.39 0 3 4 1321.17 39 -1 -3 -4 68.39 17.9 1 -3 4 95.59 16.8 -1 -3 -4 81.19 17 1 -3 4 84.29 17.6 -1 3 -4 82.89 12.8 1 3 4 67.89 17.5 2 -3 4 2651.53 77.59 2 -3 4 2573.34 83.79 -2 -3 -4 2677.63 89.29 -2 -3 -4 2754.02 77.69 2 3 4 2698.73 90.19 -2 3 -4 2565.84 69.19 3 -3 4 215.78 26.6 -3 -3 -4 163.08 28.4 3 -3 4 189.68 20.6 -3 -3 -4 220.78 20.6 -3 3 -4 206.38 14.6 3 3 4 222.98 30.1 4 -3 4 1897.61 74.59 -4 -3 -4 1811.42 78.79 4 -3 4 1970.9 60.79 -4 -3 -4 1838.42 57.89 -5 -3 -4 144.39 18.5 5 -3 4 140.89 29 5 -3 4 101.19 18.4 -5 -3 -4 119.19 30.2 6 -3 4 333.07 27.4 -6 -3 -4 352.76 43.3 6 -3 4 346.17 42 -6 -3 -4 399.46 47.8 7 -3 4 718.13 56.89 7 -3 4 739.73 37.4 -7 -3 -4 729.43 63.49 -7 -3 -4 703.83 58.69 -8 -3 -4 267.47 49.99 8 -3 4 282.47 29.1 -8 -3 -4 256.67 46.7 8 -3 4 294.07 48.5 -9 -3 -4 1060.09 78.09 9 -3 4 1061.59 47.1 -9 -3 -4 976.2 83.29 9 -3 4 1017.6 77.39 -10 -3 -4 -14.4 37.8 10 -3 4 43.2 22.3 -10 -3 -4 -11.2 40.1 -10 3 -4 -23.3 28.2 11 -3 4 280.97 35.3 -11 -3 -4 248.08 68.99 -11 -3 -4 283.97 64.09 -11 3 -4 211.38 51.19 -12 -3 -4 582.64 92.89 -12 -3 -4 491.95 83.49 -12 3 -4 550.84 75.09 -13 -3 -4 -132.89 66.19 -13 -3 -4 143.19 68.79 -13 3 -4 121.49 56.39 -14 -3 -4 -77.69 86.49 -14 3 -4 128.19 75.69 -15 -3 -4 76.59 105.09 -15 3 -4 36 81.99 -15 -4 4 14.2 101.59 15 -4 -4 75.69 59.29 -15 4 4 94.29 80.59 14 -4 -4 56.09 51.19 -14 -4 4 203.78 92.89 -14 4 4 235.58 87.09 13 -4 -4 88.49 49 -13 -4 4 101.69 75.59 -13 4 4 7.9 56.19 -12 -4 4 785.02 98.99 12 -4 -4 663.73 69.79 -12 4 4 509.65 73.39 11 -4 -4 73.99 39 -11 -4 4 32.6 56.49 -11 4 4 59.29 39.7 10 -4 -4 694.73 63.99 -10 -4 4 686.83 80.89 10 4 -4 645.34 85.29 -10 4 4 667.13 61.09 9 -4 -4 618.94 57.49 -9 -4 4 678.73 76.29 -9 4 4 716.03 58.29 9 4 -4 769.82 83.19 8 -4 -4 3.4 25.1 -8 -4 4 -9.1 36.5 -8 4 4 7.5 20.7 8 4 -4 -29.6 32.9 7 -4 -4 190.28 36.7 -7 -4 4 201.18 44.6 7 4 -4 258.87 46.3 -7 4 4 196.18 32.2 6 -4 -4 109.89 29.3 -6 -4 4 160.78 38.9 6 4 -4 137.09 39.4 -6 4 4 160.38 26 5 -4 -4 324.77 37.5 -5 -4 4 336.07 43.7 -5 4 4 283.77 28.8 5 4 -4 303.57 43.9 -4 -4 4 913.81 58.79 4 -4 -4 950.2 54.29 4 -4 -4 962 32.8 -4 4 4 995.8 46.1 4 4 -4 1007.9 62.59 3 -4 -4 28.1 11.9 -3 -4 4 47.4 22.5 3 -4 -4 9.9 22.7 3 4 -4 47.9 21.6 -3 4 4 24.5 14.6 2 -4 -4 812.22 36.9 -2 -4 4 916.51 48.4 2 -4 -4 892.71 46.3 -2 4 4 858.21 41.9 2 4 -4 865.71 49.7 1 -4 -4 1302.67 51.09 1 -4 -4 1386.06 57.09 -1 -4 4 1394.76 53.99 1 4 -4 1440.26 59.29 -1 4 4 1332.97 54.19 0 -4 -4 53.19 18.4 0 -4 -4 55.29 17.7 0 -4 4 52.39 17.5 0 -4 4 56.39 12.6 0 -4 4 64.49 18.1 0 4 4 56.19 18.4 0 4 -4 57.49 14.7 -1 -4 -4 955.1 47.7 -1 -4 -4 986.6 45.1 1 -4 4 1009.8 45.5 1 -4 4 1058.59 47.7 -1 4 -4 966.1 37.9 1 4 4 992.3 50.39 2 -4 4 1565.34 61.79 -2 -4 -4 1541.95 58.19 -2 -4 -4 1542.45 66.49 2 -4 4 1612.84 59.49 2 4 4 1552.84 67.39 -2 4 -4 1513.05 45.2 3 -4 4 3640.44 111.79 3 -4 4 3582.44 104.19 -3 -4 -4 3778.92 120.59 -3 -4 -4 3640.24 103.19 -3 4 -4 3392.76 85.39 3 4 4 3624.94 119.99 -4 -4 -4 713.33 50.89 -4 -4 -4 727.83 54.59 4 -4 4 724.33 45.5 4 -4 4 713.93 39.3 -4 -4 -4 721.13 37.3 5 -4 4 1491.95 56.69 5 -4 4 1495.65 71.29 -5 -4 -4 1436.76 79.69 -5 -4 -4 1379.46 73.39 -5 -4 -4 1477.65 54.09 -6 -4 -4 1194.58 70.49 6 -4 4 1147.69 50.89 -6 -4 -4 1157.28 75.39 6 -4 4 1088.29 64.39 7 -4 4 80.69 32.4 7 -4 4 138.39 25 -7 -4 -4 139.99 41.8 -7 -4 -4 124.59 38.7 -8 -4 -4 1595.74 100.09 -8 -4 -4 1563.04 92.59 8 -4 4 1639.24 64.29 8 -4 4 1592.44 87.29 9 -4 4 290.97 55.19 -9 -4 -4 247.28 52.09 9 -4 4 301.77 34.6 -9 -4 -4 300.17 59.69 10 -4 4 154.18 31.7 -10 -4 -4 200.88 58.49 -10 -4 -4 69.19 47 -10 4 -4 152.88 39.2 11 -4 4 82.69 31.9 -11 -4 -4 153.28 57.79 -11 -4 -4 175.38 64.99 -11 4 -4 108.19 40.3 -12 -4 -4 33.2 66.69 -12 -4 -4 2.3 69.59 12 -4 4 47.8 31.5 -12 4 -4 0.1 44.7 -13 -4 -4 -2.1 76.69 -13 -4 -4 -38.5 76.49 -13 4 -4 80.09 55.99 -14 -4 -4 4.7 87.49 -14 4 -4 -31.9 65.59 -15 -4 -4 182.18 112.19 -15 4 -4 361.16 91.39 -15 -5 4 -7.7 107.79 15 -5 -4 77.79 61.29 14 -5 -4 34.8 56.59 -14 -5 4 8.1 95.59 -13 -5 4 274.27 86.99 13 -5 -4 216.98 56.39 -13 5 4 280.67 60.09 -12 -5 4 122.59 69.79 12 -5 -4 0.3 41.9 -12 5 4 28.9 45 -11 -5 4 220.58 63.29 11 -5 -4 49.9 39 -11 5 4 85.89 39.9 10 -5 -4 81.99 40 -10 -5 4 121.39 57.09 10 5 -4 49.6 55.59 -10 5 4 101.19 35.1 -9 -5 4 95.79 49.7 9 -5 -4 7.3 30.8 -9 5 4 56.49 27.5 9 5 -4 20.1 46.4 8 -5 -4 187.68 42.5 -8 -5 4 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115.69 41.3 -7 3 7 142.69 33.3 6 -3 -7 295.47 38 6 -3 -7 342.27 47.3 -6 -3 7 306.57 48.3 6 3 -7 335.27 52.99 -6 3 7 276.57 39.8 5 -3 -7 146.79 28.9 5 -3 -7 188.68 34.5 -5 -3 7 175.88 37.1 -5 3 7 151.08 30.4 5 3 -7 182.28 39.4 4 -3 -7 59.39 26.1 -4 -3 7 34 24.9 4 -3 -7 42.3 20.9 -4 3 7 51.49 21.4 4 3 -7 41.6 21.3 3 -3 -7 682.83 45.8 3 -3 -7 681.83 48.7 -3 -3 7 638.64 48.3 -3 3 7 697.13 30.4 3 3 -7 664.63 48.1 -3 3 7 714.83 46.5 2 -3 -7 43.7 23.8 -2 -3 7 33.3 18.4 2 -3 -7 31.4 19.7 -2 3 7 59.69 12.7 -2 3 7 49.5 20.9 2 3 -7 48.7 23.4 1 -3 -7 941.41 51.49 -1 -3 7 956.5 49.8 1 -3 -7 973.5 51.39 -1 -3 7 1015.4 52.39 -1 3 7 886.11 35.9 -1 3 7 967.1 52.99 1 3 -7 906.21 51.39 0 -3 -7 332.57 31.6 0 -3 7 351.46 29.7 0 -3 7 328.57 33.6 0 -3 -7 289.37 34.2 0 3 7 370.06 36 0 3 7 349.57 25.3 0 3 -7 343.77 33.4 1 -3 7 2015.8 66.19 -1 -3 -7 2092.19 72.09 -1 -3 -7 1861.81 76.89 1 -3 7 2100.19 78.39 -1 3 -7 1946.51 71.39 1 3 7 2026.6 82.39 1 3 7 1964.5 68.29 2 -3 7 1248.08 60.89 2 -3 7 1231.78 43.5 -2 -3 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67.09 -5 2 13 761.02 70.89 -5 2 13 779.02 50.89 5 2 -13 685.13 74.29 -4 -2 13 1476.55 81.89 4 -2 -13 1526.15 92.39 -4 -2 13 1619.94 93.99 -4 2 13 1525.55 91.99 -4 2 13 1663.43 73.19 4 2 -13 1237.18 107.59 3 -2 -13 -37.3 27.3 -3 -2 13 17.7 31.6 -3 -2 13 29.4 25.6 -3 2 13 13.3 28.2 3 2 -13 12.1 33.7 -3 2 13 5 21.7 2 -2 -13 799.62 68.49 -2 -2 13 696.03 56.29 -2 -2 13 778.52 64.09 -2 2 13 688.53 47.4 2 2 -13 752.52 67.39 -2 2 13 837.52 66.49 -1 -2 13 589.54 53.79 -1 -2 13 587.14 52.79 1 -2 -13 550.34 58.29 1 2 -13 553.94 56.69 -1 2 13 572.84 46 -1 2 13 591.34 57.59 0 -2 13 223.78 42.1 0 -2 13 241.88 41.2 0 -2 -13 292.47 42.5 0 2 -13 296.17 47.8 0 2 13 243.98 45.6 0 2 13 246.38 36.3 -1 -2 -13 1941.11 98.89 1 -2 13 1973.4 91.09 1 -2 13 1734.63 89.99 -1 -2 -13 1939.71 85.19 -1 2 -13 1963 94.39 1 2 13 1853.41 85.89 1 2 13 1943.01 98.69 -2 -2 -13 50.49 25.9 2 -2 13 40.8 31.7 2 -2 13 -2.9 26.2 -2 -2 -13 97.99 36.6 2 2 13 29.3 31.5 2 2 13 53.29 28.5 -2 2 -13 49.1 31.2 3 -2 13 283.27 41.9 3 -2 13 263.77 50.09 -3 -2 -13 263.27 36.6 3 2 13 218.18 42.4 -3 2 -13 196.68 42.1 3 2 13 223.58 47.8 -4 -2 -13 31.1 39.4 4 -2 13 -6.7 31.7 -4 -2 -13 -2.8 31.6 4 -2 13 12.3 25 4 2 13 38.4 32.9 -4 2 -13 42.8 31.6 4 2 13 81.59 36.3 -5 -2 -13 79.49 37 -5 -2 -13 20.4 23.1 5 -2 13 27.7 36.4 5 2 13 -4.7 32.7 -5 2 -13 42.2 32.9 5 2 13 -19.6 35.3 -6 -2 -13 -14.2 38.5 6 -2 13 38 40.5 -6 -2 -13 89.69 21.9 6 2 13 53.59 37.7 -7 -2 -13 -1.2 11 7 -2 13 9.5 38.2 -7 -2 -13 27.3 42.8 7 2 13 -1 39.3 -7 2 -13 45.8 34.9 8 -2 13 -61.09 41.9 -8 -2 -13 -3.3 47.4 -8 2 -13 -14.2 37.4 8 2 13 -34.6 42.4 -9 -2 -13 290.77 71.49 9 -2 13 244.58 64.29 9 2 13 239.58 64.39 -9 2 -13 263.97 58.29 10 -2 13 43.1 51.69 -10 -2 -13 155.88 67.99 -10 2 -13 75.49 57.29 -11 -2 -13 333.77 86.19 11 -2 13 267.27 74.19 -11 2 -13 240.48 68.29 12 -2 13 85.79 61.39 -12 2 -13 -54.19 75.09 -13 -2 -13 46.4 107.39 -13 2 -13 -77.79 122.69 -13 -3 13 240.08 99.19 13 -3 -13 55.09 52.99 -13 3 13 105.39 87.09 13 3 -13 138.49 123.89 12 -3 -13 35.4 54.09 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