data_MK02_1_a _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C27 H17 F6 P' _chemical_formula_weight 486.38 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 10.5596(2) _cell_length_b 22.6126(7) _cell_length_c 9.5917(3) _cell_angle_alpha 90 _cell_angle_beta 108.6424(9) _cell_angle_gamma 90 _cell_volume 2170.14(10) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 8903 _cell_measurement_theta_min 2.42 _cell_measurement_theta_max 26.40 _exptl_crystal_description 'block' _exptl_crystal_colour 'yellow' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.489 _exptl_crystal_F_000 992 _exptl_transmission_factor_min 0.8299 _exptl_transmission_factor_max 0.9420 _exptl_crystal_size_max 0.450 _exptl_crystal_size_mid 0.290 _exptl_crystal_size_min 0.190 _exptl_absorpt_coefficient_mu 0.192 _shelx_estimated_absorpt_T_min 0.919 _shelx_estimated_absorpt_T_max 0.964 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'sealed tube' _diffrn_measurement_device_type 'D8 Venture, Bruker Photon CMOS Detector' _diffrn_measurement_method '\f and \w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 26264 _diffrn_reflns_av_unetI/netI 0.0471 _diffrn_reflns_av_R_equivalents 0.0729 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_k_min -28 _diffrn_reflns_limit_k_max 28 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_theta_min 2.415 _diffrn_reflns_theta_max 26.437 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measured_fraction_theta_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_point_group_measured_fraction_full 0.997 _reflns_number_total 4436 _reflns_number_gt 3444 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'Diamond 2.1e' _computing_publication_material 'X-STEP32, Microsoft Word' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0417P)^2^+1.6425P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 4436 _refine_ls_number_parameters 307 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0647 _refine_ls_R_factor_gt 0.0429 _refine_ls_wR_factor_ref 0.1052 _refine_ls_wR_factor_gt 0.0944 _refine_ls_goodness_of_fit_ref 1.043 _refine_ls_restrained_S_all 1.043 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.3562(2) 0.53695(8) 0.2702(2) 0.0144(4) Uani 1 1 d . . . . . C2 C 0.47962(19) 0.55917(8) 0.3207(2) 0.0135(4) Uani 1 1 d . . . . . H2 H 0.5517 0.5392 0.3021 0.016 Uiso 1 1 calc R U . . . C3 C 0.50517(19) 0.61710(8) 0.4091(2) 0.0138(4) Uani 1 1 d . . . . . C4 C 0.4535(2) 0.60628(8) 0.5402(2) 0.0144(4) Uani 1 1 d . . . . . H4 H 0.5117 0.6121 0.6377 0.017 Uiso 1 1 calc R U . . . C5 C 0.3288(2) 0.58901(8) 0.5186(2) 0.0142(4) Uani 1 1 d . . . . . C6 C 0.26710(19) 0.57813(9) 0.6343(2) 0.0150(4) Uani 1 1 d . . . . . C7 C 0.3030(2) 0.61259(9) 0.7623(2) 0.0188(5) Uani 1 1 d . . . . . H7 H 0.3651 0.6440 0.7732 0.023 Uiso 1 1 calc R U . . . C8 C 0.2485(2) 0.60101(10) 0.8730(3) 0.0235(5) Uani 1 1 d . . . . . H8 H 0.2733 0.6247 0.9595 0.028 Uiso 1 1 calc R U . . . C9 C 0.1579(2) 0.55515(10) 0.8587(2) 0.0224(5) Uani 1 1 d . . . . . H9 H 0.1211 0.5473 0.9351 0.027 Uiso 1 1 calc R U . . . C10 C 0.1214(2) 0.52086(10) 0.7324(3) 0.0219(5) Uani 1 1 d . . . . . H10 H 0.0600 0.4892 0.7226 0.026 Uiso 1 1 calc R U . . . C11 C 0.1741(2) 0.53267(9) 0.6205(2) 0.0182(5) Uani 1 1 d . . . . . H11 H 0.1468 0.5096 0.5332 0.022 Uiso 1 1 calc R U . . . C12 C 0.3181(2) 0.48263(9) 0.1806(2) 0.0151(4) Uani 1 1 d . . . . . C13 C 0.2013(2) 0.45126(9) 0.1705(2) 0.0214(5) Uani 1 1 d . . . . . H13 H 0.1448 0.4646 0.2237 0.026 Uiso 1 1 calc R U . . . C14 C 0.1671(2) 0.40094(10) 0.0839(3) 0.0259(5) Uani 1 1 d . . . . . H14 H 0.0869 0.3805 0.0778 0.031 Uiso 1 1 calc R U . . . C15 C 0.2479(2) 0.38021(10) 0.0066(3) 0.0266(5) Uani 1 1 d . . . . . H15 H 0.2238 0.3458 -0.0527 0.032 Uiso 1 1 calc R U . . . C16 C 0.3653(2) 0.41045(10) 0.0168(3) 0.0247(5) Uani 1 1 d . . . . . H16 H 0.4223 0.3963 -0.0349 0.030 Uiso 1 1 calc R U . . . C17 C 0.3994(2) 0.46091(9) 0.1017(2) 0.0175(4) Uani 1 1 d . . . . . H17 H 0.4794 0.4813 0.1066 0.021 Uiso 1 1 calc R U . . . C18 C 0.6522(2) 0.63605(8) 0.4635(2) 0.0154(4) Uani 1 1 d . . . . . C19 C 0.6951(2) 0.67696(9) 0.5777(2) 0.0203(5) Uani 1 1 d . . . . . H19 H 0.6324 0.6929 0.6198 0.024 Uiso 1 1 calc R U . . . C20 C 0.8275(2) 0.69486(10) 0.6309(3) 0.0291(6) Uani 1 1 d . . . . . H20 H 0.8546 0.7231 0.7081 0.035 Uiso 1 1 calc R U . . . C21 C 0.9204(2) 0.67157(10) 0.5716(3) 0.0298(6) Uani 1 1 d . . . . . H21 H 1.0117 0.6829 0.6094 0.036 Uiso 1 1 calc R U . . . C22 C 0.8789(2) 0.63164(10) 0.4569(3) 0.0270(5) Uani 1 1 d . . . . . H22 H 0.9419 0.6159 0.4149 0.032 Uiso 1 1 calc R U . . . C23 C 0.7461(2) 0.61422(9) 0.4025(3) 0.0199(5) Uani 1 1 d . . . . . H23 H 0.7190 0.5871 0.3229 0.024 Uiso 1 1 calc R U . . . C24 C 0.2777(2) 0.65272(8) 0.2716(2) 0.0148(4) Uani 1 1 d . . . . . C25 C 0.4085(2) 0.66369(8) 0.3079(2) 0.0138(4) Uani 1 1 d . . . . . C26 C 0.1658(2) 0.69591(9) 0.2044(2) 0.0197(5) Uani 1 1 d . . . . . C27 C 0.4675(2) 0.71614(9) 0.2524(2) 0.0189(5) Uani 1 1 d . . . . . F1 F 0.05673(13) 0.68081(6) 0.23878(16) 0.0313(3) Uani 1 1 d . . . . . F2 F 0.12709(13) 0.69836(6) 0.05730(14) 0.0288(3) Uani 1 1 d . . . . . F3 F 0.19620(13) 0.75102(5) 0.25548(15) 0.0271(3) Uani 1 1 d . . . . . F4 F 0.37950(13) 0.74214(6) 0.13481(15) 0.0289(3) Uani 1 1 d . . . . . F5 F 0.56954(13) 0.69951(5) 0.20673(15) 0.0276(3) Uani 1 1 d . . . . . F6 F 0.51225(13) 0.75835(5) 0.35349(15) 0.0290(3) Uani 1 1 d . . . . . P1 P 0.22712(5) 0.57896(2) 0.32246(6) 0.01384(13) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0191(10) 0.0131(9) 0.0122(11) 0.0025(8) 0.0067(8) 0.0035(8) C2 0.0130(10) 0.0138(9) 0.0149(11) 0.0019(8) 0.0062(8) 0.0026(7) C3 0.0150(10) 0.0127(9) 0.0132(11) 0.0012(8) 0.0038(8) 0.0003(8) C4 0.0193(10) 0.0119(9) 0.0119(10) 0.0002(8) 0.0049(8) 0.0011(8) C5 0.0174(10) 0.0101(9) 0.0147(11) 0.0003(8) 0.0045(8) 0.0010(7) C6 0.0147(10) 0.0157(10) 0.0152(11) 0.0040(8) 0.0057(8) 0.0050(8) C7 0.0171(10) 0.0189(11) 0.0201(12) -0.0002(9) 0.0056(9) 0.0011(8) C8 0.0246(12) 0.0309(12) 0.0160(12) -0.0028(9) 0.0077(10) 0.0039(9) C9 0.0187(11) 0.0322(12) 0.0180(12) 0.0090(10) 0.0082(9) 0.0071(9) C10 0.0191(11) 0.0230(11) 0.0255(13) 0.0070(9) 0.0098(10) 0.0003(9) C11 0.0202(11) 0.0172(10) 0.0170(12) 0.0010(8) 0.0056(9) -0.0008(8) C12 0.0179(10) 0.0136(10) 0.0124(11) 0.0021(8) 0.0029(8) 0.0015(8) C13 0.0239(11) 0.0190(11) 0.0231(12) -0.0017(9) 0.0101(10) -0.0006(9) C14 0.0242(12) 0.0202(11) 0.0299(14) -0.0050(10) 0.0040(10) -0.0049(9) C15 0.0301(13) 0.0194(11) 0.0250(13) -0.0082(9) 0.0015(10) 0.0003(9) C16 0.0285(13) 0.0247(12) 0.0195(12) -0.0063(9) 0.0058(10) 0.0037(9) C17 0.0181(10) 0.0191(10) 0.0144(11) 0.0013(8) 0.0036(9) 0.0010(8) C18 0.0142(10) 0.0136(10) 0.0174(11) 0.0037(8) 0.0038(9) 0.0005(8) C19 0.0206(11) 0.0190(11) 0.0212(12) -0.0031(9) 0.0066(9) -0.0039(8) C20 0.0289(13) 0.0240(12) 0.0299(14) -0.0056(10) 0.0030(11) -0.0098(10) C21 0.0163(11) 0.0278(13) 0.0402(15) 0.0011(11) 0.0018(11) -0.0058(9) C22 0.0182(11) 0.0254(12) 0.0386(15) -0.0012(11) 0.0108(11) -0.0019(9) C23 0.0168(11) 0.0189(11) 0.0231(12) -0.0003(9) 0.0052(9) -0.0006(8) C24 0.0213(11) 0.0133(9) 0.0100(10) -0.0009(8) 0.0053(8) 0.0016(8) C25 0.0196(11) 0.0118(9) 0.0112(10) -0.0006(8) 0.0067(8) 0.0002(8) C26 0.0206(11) 0.0188(11) 0.0193(12) 0.0014(9) 0.0056(9) 0.0022(8) C27 0.0201(11) 0.0158(10) 0.0200(12) 0.0036(9) 0.0052(9) 0.0033(8) F1 0.0197(7) 0.0303(7) 0.0471(9) 0.0106(7) 0.0153(6) 0.0091(5) F2 0.0293(7) 0.0331(7) 0.0179(7) 0.0032(6) -0.0013(6) 0.0095(6) F3 0.0289(7) 0.0162(6) 0.0326(8) -0.0021(5) 0.0046(6) 0.0074(5) F4 0.0287(7) 0.0266(7) 0.0298(8) 0.0159(6) 0.0071(6) 0.0021(5) F5 0.0282(7) 0.0249(7) 0.0372(8) 0.0110(6) 0.0210(6) 0.0044(5) F6 0.0361(8) 0.0137(6) 0.0345(8) -0.0024(6) 0.0074(7) -0.0059(5) P1 0.0126(3) 0.0148(3) 0.0143(3) -0.0001(2) 0.0045(2) 0.0004(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C2 1.335(3) . ? C1 C12 1.479(3) . ? C1 P1 1.857(2) . ? C2 C3 1.537(3) . ? C2 H2 0.9500 . ? C3 C18 1.532(3) . ? C3 C4 1.542(3) . ? C3 C25 1.568(3) . ? C4 C5 1.325(3) . ? C4 H4 0.9500 . ? C5 C6 1.476(3) . ? C5 P1 1.858(2) . ? C6 C11 1.399(3) . ? C6 C7 1.400(3) . ? C7 C8 1.386(3) . ? C7 H7 0.9500 . ? C8 C9 1.388(3) . ? C8 H8 0.9500 . ? C9 C10 1.385(3) . ? C9 H9 0.9500 . ? C10 C11 1.384(3) . ? C10 H10 0.9500 . ? C11 H11 0.9500 . ? C12 C13 1.399(3) . ? C12 C17 1.402(3) . ? C13 C14 1.387(3) . ? C13 H13 0.9500 . ? C14 C15 1.380(3) . ? C14 H14 0.9500 . ? C15 C16 1.391(3) . ? C15 H15 0.9500 . ? C16 C17 1.381(3) . ? C16 H16 0.9500 . ? C17 H17 0.9500 . ? C18 C23 1.393(3) . ? C18 C19 1.394(3) . ? C19 C20 1.387(3) . ? C19 H19 0.9500 . ? C20 C21 1.386(3) . ? C20 H20 0.9500 . ? C21 C22 1.382(3) . ? C21 H21 0.9500 . ? C22 C23 1.388(3) . ? C22 H22 0.9500 . ? C23 H23 0.9500 . ? C24 C25 1.336(3) . ? C24 C26 1.509(3) . ? C24 P1 1.863(2) . ? C25 C27 1.513(3) . ? C26 F2 1.339(3) . ? C26 F1 1.340(2) . ? C26 F3 1.340(2) . ? C27 F6 1.335(2) . ? C27 F5 1.340(2) . ? C27 F4 1.346(2) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 C1 C12 125.19(18) . . ? C2 C1 P1 115.16(15) . . ? C12 C1 P1 119.65(14) . . ? C1 C2 C3 120.01(17) . . ? C1 C2 H2 120.0 . . ? C3 C2 H2 120.0 . . ? C18 C3 C2 113.97(16) . . ? C18 C3 C4 110.55(16) . . ? C2 C3 C4 105.61(15) . . ? C18 C3 C25 114.26(16) . . ? C2 C3 C25 105.46(15) . . ? C4 C3 C25 106.34(15) . . ? C5 C4 C3 120.81(18) . . ? C5 C4 H4 119.6 . . ? C3 C4 H4 119.6 . . ? C4 C5 C6 125.92(19) . . ? C4 C5 P1 114.73(16) . . ? C6 C5 P1 119.35(14) . . ? C11 C6 C7 118.53(19) . . ? C11 C6 C5 121.09(18) . . ? C7 C6 C5 120.37(18) . . ? C8 C7 C6 120.3(2) . . ? C8 C7 H7 119.9 . . ? C6 C7 H7 119.9 . . ? C7 C8 C9 120.5(2) . . ? C7 C8 H8 119.8 . . ? C9 C8 H8 119.8 . . ? C10 C9 C8 119.7(2) . . ? C10 C9 H9 120.1 . . ? C8 C9 H9 120.1 . . ? C11 C10 C9 120.1(2) . . ? C11 C10 H10 119.9 . . ? C9 C10 H10 119.9 . . ? C10 C11 C6 120.8(2) . . ? C10 C11 H11 119.6 . . ? C6 C11 H11 119.6 . . ? C13 C12 C17 117.58(19) . . ? C13 C12 C1 122.10(18) . . ? C17 C12 C1 120.32(18) . . ? C14 C13 C12 120.9(2) . . ? C14 C13 H13 119.6 . . ? C12 C13 H13 119.6 . . ? C15 C14 C13 120.9(2) . . ? C15 C14 H14 119.6 . . ? C13 C14 H14 119.6 . . ? C14 C15 C16 119.1(2) . . ? C14 C15 H15 120.5 . . ? C16 C15 H15 120.5 . . ? C17 C16 C15 120.4(2) . . ? C17 C16 H16 119.8 . . ? C15 C16 H16 119.8 . . ? C16 C17 C12 121.2(2) . . ? C16 C17 H17 119.4 . . ? C12 C17 H17 119.4 . . ? C23 C18 C19 117.94(19) . . ? C23 C18 C3 122.54(19) . . ? C19 C18 C3 119.52(18) . . ? C20 C19 C18 121.3(2) . . ? C20 C19 H19 119.3 . . ? C18 C19 H19 119.3 . . ? C21 C20 C19 120.0(2) . . ? C21 C20 H20 120.0 . . ? C19 C20 H20 120.0 . . ? C22 C21 C20 119.3(2) . . ? C22 C21 H21 120.4 . . ? C20 C21 H21 120.4 . . ? C21 C22 C23 120.7(2) . . ? C21 C22 H22 119.7 . . ? C23 C22 H22 119.7 . . ? C22 C23 C18 120.7(2) . . ? C22 C23 H23 119.6 . . ? C18 C23 H23 119.6 . . ? C25 C24 C26 126.47(18) . . ? C25 C24 P1 117.19(15) . . ? C26 C24 P1 116.14(15) . . ? C24 C25 C27 124.16(18) . . ? C24 C25 C3 116.80(17) . . ? C27 C25 C3 118.99(17) . . ? F2 C26 F1 105.84(17) . . ? F2 C26 F3 107.67(17) . . ? F1 C26 F3 105.74(17) . . ? F2 C26 C24 114.24(17) . . ? F1 C26 C24 110.32(17) . . ? F3 C26 C24 112.49(17) . . ? F6 C27 F5 107.64(17) . . ? F6 C27 F4 106.59(16) . . ? F5 C27 F4 105.07(17) . . ? F6 C27 C25 113.29(18) . . ? F5 C27 C25 111.06(16) . . ? F4 C27 C25 112.69(17) . . ? C1 P1 C5 95.71(9) . . ? C1 P1 C24 95.22(9) . . ? C5 P1 C24 91.98(9) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C12 C1 C2 C3 178.21(18) . . . . ? P1 C1 C2 C3 -2.7(2) . . . . ? C1 C2 C3 C18 178.30(18) . . . . ? C1 C2 C3 C4 56.8(2) . . . . ? C1 C2 C3 C25 -55.6(2) . . . . ? C18 C3 C4 C5 -179.42(17) . . . . ? C2 C3 C4 C5 -55.7(2) . . . . ? C25 C3 C4 C5 56.0(2) . . . . ? C3 C4 C5 C6 -179.00(17) . . . . ? C3 C4 C5 P1 0.4(2) . . . . ? C4 C5 C6 C11 -144.1(2) . . . . ? P1 C5 C6 C11 36.5(2) . . . . ? C4 C5 C6 C7 34.6(3) . . . . ? P1 C5 C6 C7 -144.86(16) . . . . ? C11 C6 C7 C8 0.9(3) . . . . ? C5 C6 C7 C8 -177.78(18) . . . . ? C6 C7 C8 C9 0.1(3) . . . . ? C7 C8 C9 C10 -0.3(3) . . . . ? C8 C9 C10 C11 -0.6(3) . . . . ? C9 C10 C11 C6 1.6(3) . . . . ? C7 C6 C11 C10 -1.8(3) . . . . ? C5 C6 C11 C10 176.90(19) . . . . ? C2 C1 C12 C13 159.0(2) . . . . ? P1 C1 C12 C13 -20.0(3) . . . . ? C2 C1 C12 C17 -21.2(3) . . . . ? P1 C1 C12 C17 159.76(16) . . . . ? C17 C12 C13 C14 -0.8(3) . . . . ? C1 C12 C13 C14 179.0(2) . . . . ? C12 C13 C14 C15 0.6(3) . . . . ? C13 C14 C15 C16 0.2(4) . . . . ? C14 C15 C16 C17 -0.8(3) . . . . ? C15 C16 C17 C12 0.7(3) . . . . ? C13 C12 C17 C16 0.1(3) . . . . ? C1 C12 C17 C16 -179.69(19) . . . . ? C2 C3 C18 C23 18.8(3) . . . . ? C4 C3 C18 C23 137.55(19) . . . . ? C25 C3 C18 C23 -102.6(2) . . . . ? C2 C3 C18 C19 -161.62(18) . . . . ? C4 C3 C18 C19 -42.9(2) . . . . ? C25 C3 C18 C19 77.0(2) . . . . ? C23 C18 C19 C20 -1.0(3) . . . . ? C3 C18 C19 C20 179.4(2) . . . . ? C18 C19 C20 C21 -0.7(3) . . . . ? C19 C20 C21 C22 1.6(4) . . . . ? C20 C21 C22 C23 -0.9(4) . . . . ? C21 C22 C23 C18 -0.8(3) . . . . ? C19 C18 C23 C22 1.7(3) . . . . ? C3 C18 C23 C22 -178.7(2) . . . . ? C26 C24 C25 C27 -16.7(3) . . . . ? P1 C24 C25 C27 168.70(16) . . . . ? C26 C24 C25 C3 166.02(18) . . . . ? P1 C24 C25 C3 -8.6(2) . . . . ? C18 C3 C25 C24 -172.27(18) . . . . ? C2 C3 C25 C24 61.8(2) . . . . ? C4 C3 C25 C24 -50.0(2) . . . . ? C18 C3 C25 C27 10.3(3) . . . . ? C2 C3 C25 C27 -115.63(19) . . . . ? C4 C3 C25 C27 132.54(18) . . . . ? C25 C24 C26 F2 87.3(3) . . . . ? P1 C24 C26 F2 -98.11(18) . . . . ? C25 C24 C26 F1 -153.7(2) . . . . ? P1 C24 C26 F1 21.0(2) . . . . ? C25 C24 C26 F3 -35.9(3) . . . . ? P1 C24 C26 F3 138.75(15) . . . . ? C24 C25 C27 F6 105.0(2) . . . . ? C3 C25 C27 F6 -77.8(2) . . . . ? C24 C25 C27 F5 -133.7(2) . . . . ? C3 C25 C27 F5 43.5(2) . . . . ? C24 C25 C27 F4 -16.1(3) . . . . ? C3 C25 C27 F4 161.08(17) . . . . ? C2 C1 P1 C5 -44.99(17) . . . . ? C12 C1 P1 C5 134.16(16) . . . . ? C2 C1 P1 C24 47.53(17) . . . . ? C12 C1 P1 C24 -133.32(16) . . . . ? C4 C5 P1 C1 46.07(16) . . . . ? C6 C5 P1 C1 -134.45(15) . . . . ? C4 C5 P1 C24 -49.37(16) . . . . ? C6 C5 P1 C24 130.11(15) . . . . ? C25 C24 P1 C1 -41.47(17) . . . . ? C26 C24 P1 C1 143.37(16) . . . . ? C25 C24 P1 C5 54.44(17) . . . . ? C26 C24 P1 C5 -120.71(16) . . . . ? _refine_diff_density_max 0.484 _refine_diff_density_min -0.431 _refine_diff_density_rms 0.074 _shelx_res_file ; MK02_1_a.res created by SHELXL-2014/7 TITL MK02_1_a.res in P2(1)/c REM Old TITL MK02_1 in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.113, Rweak 0.007, Alpha 0.027, Orientation as input REM Formula found by SHELXT: C27 F6 P CELL 0.71073 10.5596 22.6126 9.5917 90.000 108.6424 90.000 ZERR 4.000 0.0002 0.0007 0.0003 0.000 0.0009 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H F P UNIT 108 68 24 4 TEMP -100. SIZE 0.190 0.290 0.450 L.S. 30 BOND $H LIST 6 acta conf FMAP 2 PLAN 20 WGHT 0.041700 1.642500 FVAR 0.54194 C1 1 0.356212 0.536951 0.270210 11.00000 0.01913 0.01308 = 0.01223 0.00253 0.00673 0.00347 C2 1 0.479621 0.559170 0.320748 11.00000 0.01300 0.01383 = 0.01491 0.00193 0.00620 0.00258 AFIX 43 H2 2 0.551665 0.539163 0.302087 11.00000 -1.20000 AFIX 0 C3 1 0.505167 0.617103 0.409103 11.00000 0.01505 0.01271 = 0.01315 0.00121 0.00380 0.00032 C4 1 0.453453 0.606284 0.540223 11.00000 0.01929 0.01189 = 0.01194 0.00021 0.00493 0.00112 AFIX 43 H4 2 0.511746 0.612084 0.637713 11.00000 -1.20000 AFIX 0 C5 1 0.328771 0.589007 0.518578 11.00000 0.01740 0.01015 = 0.01470 0.00028 0.00447 0.00103 C6 1 0.267102 0.578133 0.634322 11.00000 0.01471 0.01570 = 0.01519 0.00400 0.00570 0.00498 C7 1 0.303046 0.612586 0.762291 11.00000 0.01709 0.01889 = 0.02006 -0.00023 0.00559 0.00107 AFIX 43 H7 2 0.365115 0.644041 0.773249 11.00000 -1.20000 AFIX 0 C8 1 0.248492 0.601013 0.873046 11.00000 0.02462 0.03091 = 0.01597 -0.00280 0.00769 0.00385 AFIX 43 H8 2 0.273304 0.624651 0.959459 11.00000 -1.20000 AFIX 0 C9 1 0.157892 0.555152 0.858670 11.00000 0.01867 0.03222 = 0.01802 0.00898 0.00824 0.00712 AFIX 43 H9 2 0.121069 0.547307 0.935111 11.00000 -1.20000 AFIX 0 C10 1 0.121373 0.520860 0.732390 11.00000 0.01914 0.02304 = 0.02547 0.00697 0.00979 0.00027 AFIX 43 H10 2 0.060035 0.489183 0.722578 11.00000 -1.20000 AFIX 0 C11 1 0.174091 0.532667 0.620487 11.00000 0.02020 0.01720 = 0.01698 0.00102 0.00562 -0.00077 AFIX 43 H11 2 0.146752 0.509595 0.533163 11.00000 -1.20000 AFIX 0 C12 1 0.318097 0.482633 0.180597 11.00000 0.01787 0.01357 = 0.01241 0.00206 0.00288 0.00153 C13 1 0.201329 0.451257 0.170523 11.00000 0.02386 0.01901 = 0.02307 -0.00169 0.01006 -0.00062 AFIX 43 H13 2 0.144761 0.464592 0.223686 11.00000 -1.20000 AFIX 0 C14 1 0.167079 0.400944 0.083943 11.00000 0.02424 0.02017 = 0.02989 -0.00497 0.00396 -0.00485 AFIX 43 H14 2 0.086892 0.380485 0.077786 11.00000 -1.20000 AFIX 0 C15 1 0.247917 0.380206 0.006630 11.00000 0.03007 0.01944 = 0.02496 -0.00819 0.00152 0.00031 AFIX 43 H15 2 0.223789 0.345770 -0.052707 11.00000 -1.20000 AFIX 0 C16 1 0.365295 0.410446 0.016797 11.00000 0.02847 0.02475 = 0.01947 -0.00625 0.00579 0.00375 AFIX 43 H16 2 0.422329 0.396292 -0.034941 11.00000 -1.20000 AFIX 0 C17 1 0.399362 0.460909 0.101652 11.00000 0.01805 0.01905 = 0.01437 0.00128 0.00361 0.00099 AFIX 43 H17 2 0.479360 0.481294 0.106643 11.00000 -1.20000 AFIX 0 C18 1 0.652193 0.636054 0.463494 11.00000 0.01425 0.01363 = 0.01745 0.00366 0.00378 0.00052 C19 1 0.695135 0.676964 0.577662 11.00000 0.02060 0.01899 = 0.02116 -0.00306 0.00656 -0.00392 AFIX 43 H19 2 0.632449 0.692900 0.619806 11.00000 -1.20000 AFIX 0 C20 1 0.827529 0.694859 0.630933 11.00000 0.02893 0.02400 = 0.02993 -0.00557 0.00302 -0.00978 AFIX 43 H20 2 0.854560 0.723101 0.708133 11.00000 -1.20000 AFIX 0 C21 1 0.920440 0.671567 0.571616 11.00000 0.01626 0.02780 = 0.04019 0.00108 0.00177 -0.00584 AFIX 43 H21 2 1.011691 0.682925 0.609388 11.00000 -1.20000 AFIX 0 C22 1 0.878880 0.631638 0.456919 11.00000 0.01820 0.02538 = 0.03863 -0.00117 0.01084 -0.00186 AFIX 43 H22 2 0.941864 0.615950 0.414857 11.00000 -1.20000 AFIX 0 C23 1 0.746113 0.614220 0.402546 11.00000 0.01682 0.01886 = 0.02314 -0.00030 0.00523 -0.00064 AFIX 43 H23 2 0.718970 0.587098 0.322853 11.00000 -1.20000 AFIX 0 C24 1 0.277658 0.652723 0.271617 11.00000 0.02128 0.01328 = 0.01004 -0.00086 0.00534 0.00160 C25 1 0.408527 0.663686 0.307908 11.00000 0.01959 0.01183 = 0.01116 -0.00063 0.00668 0.00023 C26 1 0.165811 0.695905 0.204417 11.00000 0.02056 0.01879 = 0.01929 0.00137 0.00562 0.00217 C27 1 0.467494 0.716136 0.252441 11.00000 0.02007 0.01581 = 0.02004 0.00357 0.00521 0.00329 F1 3 0.056726 0.680812 0.238776 11.00000 0.01972 0.03027 = 0.04713 0.01060 0.01531 0.00910 F2 3 0.127089 0.698356 0.057295 11.00000 0.02927 0.03305 = 0.01790 0.00323 -0.00131 0.00946 F3 3 0.196201 0.751023 0.255475 11.00000 0.02892 0.01619 = 0.03262 -0.00212 0.00463 0.00739 F4 3 0.379505 0.742138 0.134806 11.00000 0.02873 0.02663 = 0.02976 0.01595 0.00706 0.00212 F5 3 0.569542 0.699509 0.206734 11.00000 0.02823 0.02490 = 0.03724 0.01099 0.02096 0.00444 F6 3 0.512250 0.758353 0.353488 11.00000 0.03614 0.01366 = 0.03451 -0.00241 0.00741 -0.00593 P1 4 0.227117 0.578964 0.322461 11.00000 0.01257 0.01485 = 0.01426 -0.00014 0.00450 0.00037 HKLF 4 REM MK02_1_a.res in P2(1)/c REM R1 = 0.0429 for 3444 Fo > 4sig(Fo) and 0.0647 for all 4436 data REM 307 parameters refined using 0 restraints END WGHT 0.0417 1.6425 REM Highest difference peak 0.484, deepest hole -0.431, 1-sigma level 0.074 Q1 1 0.2973 0.5526 0.2914 11.00000 0.05 0.48 Q2 1 0.1341 0.5856 0.3116 11.00000 0.05 0.35 Q3 1 0.3519 0.6562 0.2465 11.00000 0.05 0.31 Q4 1 0.4600 0.7899 0.1009 11.00000 0.05 0.31 Q5 1 0.5833 0.6262 0.4343 11.00000 0.05 0.30 Q6 1 0.3781 0.4663 0.1752 11.00000 0.05 0.29 Q7 1 0.4459 0.6860 0.2738 11.00000 0.05 0.28 Q8 1 0.4012 0.5413 0.3311 11.00000 0.05 0.28 Q9 1 0.0012 0.7004 0.3377 11.00000 0.05 0.28 Q10 1 0.3072 0.5785 0.5782 11.00000 0.05 0.27 Q11 1 0.3959 0.6669 0.5631 11.00000 0.05 0.26 Q12 1 0.3653 0.6150 0.5385 11.00000 0.05 0.25 Q13 1 -0.0253 0.6767 0.2367 11.00000 0.05 0.25 Q14 1 0.4736 0.6057 0.4715 11.00000 0.05 0.25 Q15 1 0.3176 0.3897 0.0379 11.00000 0.05 0.25 Q16 1 0.0342 0.7522 0.0085 11.00000 0.05 0.24 Q17 1 0.3373 0.5055 0.2400 11.00000 0.05 0.24 Q18 1 0.9967 0.5997 0.6825 11.00000 0.05 0.24 Q19 1 0.4013 0.5867 0.5331 11.00000 0.05 0.24 Q20 1 0.0018 0.5570 0.6233 11.00000 0.05 0.24 ; _shelx_res_checksum 69394 _shelx_hkl_file ; 0 0 -1 -0.20 0.60 0 0 1 0.30 0.80 0 0 2 3657.93 157.38 0 0 2 3856.31 158.98 0 0 2 4241.18 159.78 0 0 -2 4003.70 159.18 0 0 -2 3569.34 159.08 0 0 -3 1.10 2.70 0 0 3 0.70 3.20 0 0 -3 -2.00 3.80 0 0 3 1.20 1.40 0 0 4 53.79 8.10 0 0 4 48.20 4.30 0 0 -4 67.39 9.00 0 0 -4 45.80 7.20 0 0 -5 -5.80 7.10 0 0 5 3.00 2.00 0 0 -5 0.50 4.70 0 0 5 -5.10 5.30 0 0 -6 42.20 10.30 0 0 6 38.70 8.50 0 0 -6 43.10 8.90 0 0 -7 -0.30 6.80 0 0 -7 6.70 10.90 0 0 7 5.10 8.70 0 0 -8 1.10 13.00 0 0 8 12.20 12.50 0 0 -8 10.40 8.80 0 0 9 -4.90 12.60 0 0 -9 0.30 10.20 0 0 -9 -19.40 14.90 0 0 10 29.90 24.30 0 0 -10 35.70 26.40 0 0 -10 4.60 13.30 0 0 -11 -2.10 23.90 0 0 11 15.50 21.80 0 1 1 707.63 31.10 0 1 1 686.33 31.10 0 1 -1 750.92 31.20 0 -1 1 724.23 31.50 0 -1 -1 758.02 31.10 0 -1 -1 738.83 31.00 0 1 2 8.80 3.00 0 1 2 8.60 2.80 0 1 -2 12.50 3.50 0 -1 -2 8.70 2.60 0 -1 -2 11.70 3.30 0 -1 -2 8.20 1.80 0 -1 2 8.50 3.50 0 1 3 221.28 9.40 0 1 -3 194.68 12.50 0 1 3 204.78 12.50 0 1 3 196.98 11.80 0 1 -3 213.28 12.60 0 -1 3 186.88 12.10 0 -1 3 171.88 9.20 0 -1 -3 186.58 11.50 0 -1 -3 203.08 12.40 0 -1 -3 186.98 9.50 0 1 4 356.86 20.00 0 1 -4 374.56 20.60 0 1 4 412.96 21.80 0 1 -4 363.56 21.10 0 -1 4 356.66 16.60 0 -1 -4 366.96 19.90 0 -1 -4 361.06 21.00 0 -1 -4 344.77 16.90 0 -1 4 374.06 20.70 0 1 5 88.19 11.10 0 1 -5 94.49 11.90 0 1 -5 77.09 9.70 0 -1 -5 79.39 9.50 0 -1 5 81.69 10.60 0 -1 -5 96.79 11.60 0 -1 5 77.79 5.80 0 1 6 -5.70 6.40 0 1 -6 4.20 5.90 0 1 -6 -4.50 8.30 0 -1 6 7.10 7.40 0 -1 -6 1.20 5.80 0 -1 -6 3.90 9.00 0 -1 6 2.50 2.50 0 1 -7 67.09 11.70 0 1 -7 69.59 13.40 0 1 7 56.59 11.40 0 -1 -7 62.29 11.30 0 -1 -7 64.99 14.00 0 -1 7 65.19 11.60 0 1 8 20.70 13.40 0 1 -8 14.20 13.00 0 1 -8 2.30 8.30 0 -1 -8 15.90 14.10 0 -1 8 14.60 13.50 0 -1 -8 7.20 8.60 0 1 -9 22.60 11.60 0 1 -9 21.00 15.20 0 1 9 31.40 12.70 0 -1 9 26.30 14.10 0 -1 -9 35.50 12.50 0 -1 -9 19.90 17.00 0 1 -10 25.30 22.00 0 1 -10 27.20 14.10 0 1 10 25.60 34.10 0 -1 10 -15.20 25.60 0 -1 -10 22.60 22.50 0 1 -11 11.10 24.00 0 1 11 18.60 21.50 0 -1 -11 41.10 24.20 0 -1 11 32.20 22.30 0 2 1 1153.28 49.70 0 2 -1 1217.38 50.09 0 -2 -1 1193.68 49.90 0 -2 1 1231.88 50.09 0 2 2 343.87 17.00 0 2 2 350.76 17.60 0 2 -2 360.26 17.60 0 -2 -2 365.66 17.40 0 -2 -2 358.86 17.30 0 -2 -2 386.16 15.90 0 -2 2 366.96 17.80 0 2 3 2619.74 111.09 0 2 3 2518.85 111.79 0 2 -3 2786.22 111.79 0 -2 -3 2706.43 111.49 0 -2 -3 2604.64 109.29 0 -2 -3 2639.84 111.49 0 -2 3 2734.83 111.79 0 2 -4 320.57 18.50 0 2 4 274.77 16.90 0 2 -4 319.47 18.80 0 2 4 304.27 18.30 0 -2 -4 297.47 16.90 0 -2 4 301.17 18.10 0 -2 -4 268.97 17.90 0 -2 4 259.77 13.60 0 -2 -4 283.97 14.20 0 2 5 206.48 16.70 0 2 -5 196.98 15.40 0 2 -5 212.78 16.50 0 2 5 196.68 14.80 0 -2 5 221.08 16.30 0 -2 -5 186.08 14.00 0 -2 5 198.98 10.40 0 -2 -5 172.18 16.00 0 -2 -5 189.78 10.90 0 2 6 646.04 33.70 0 2 -6 634.34 33.80 0 2 -6 629.14 34.70 0 -2 6 647.64 28.20 0 -2 -6 641.84 33.20 0 -2 6 637.74 34.50 0 -2 -6 644.84 35.40 0 2 -7 261.17 23.00 0 2 7 241.88 20.40 0 2 -7 236.38 19.30 0 -2 7 284.87 22.80 0 -2 -7 266.07 24.10 0 -2 -7 261.67 19.00 0 2 -8 45.00 15.00 0 2 8 50.69 15.00 0 2 -8 33.00 10.70 0 -2 -8 32.20 15.50 0 -2 -8 38.50 10.60 0 -2 8 60.89 13.70 0 2 9 416.16 31.10 0 2 -9 374.26 28.30 0 2 -9 406.46 34.50 0 -2 9 467.75 33.60 0 -2 -9 367.76 36.00 0 2 10 101.69 22.20 0 2 -10 116.09 19.20 0 2 -10 89.89 23.10 0 -2 10 118.59 24.80 0 -2 -10 35.90 27.10 0 2 11 35.70 21.10 0 2 -11 -26.50 23.40 0 2 -11 2.00 15.70 0 -2 -11 22.50 25.40 0 -2 11 -24.30 22.10 0 3 0 0.90 0.80 0 3 0 0.90 0.80 0 -3 0 -0.20 0.70 0 -3 0 -0.30 0.70 0 3 -1 1036.00 42.70 0 3 1 971.70 42.30 0 -3 1 1047.50 42.80 0 -3 -1 997.90 42.50 0 3 -2 9918.71 401.76 0 -3 2 9999.00 401.96 0 -3 -2 9613.94 401.46 0 3 3 5.80 3.20 0 3 -3 4.40 4.00 0 3 3 5.80 3.60 0 -3 3 0.00 4.10 0 -3 -3 4.80 2.00 0 -3 -3 2.30 3.60 0 3 -4 344.37 20.10 0 3 4 314.97 18.40 0 3 4 316.27 19.40 0 -3 -4 345.47 18.70 0 -3 -4 341.67 20.10 0 -3 -4 326.77 16.10 0 -3 4 357.56 20.20 0 3 -5 511.65 27.80 0 3 5 473.45 25.40 0 3 5 463.05 27.20 0 -3 5 503.65 27.00 0 -3 -5 484.05 27.10 0 -3 -5 460.15 22.20 0 -3 -5 478.85 25.40 0 -3 5 447.66 21.60 0 3 -6 236.18 19.40 0 3 6 234.98 17.70 0 3 6 274.17 20.70 0 3 -6 261.07 19.10 0 -3 -6 240.68 20.40 0 -3 -6 253.87 17.20 0 -3 6 244.28 12.70 0 -3 6 222.98 19.50 0 -3 -6 223.18 13.40 0 3 -7 13.80 10.20 0 3 7 14.80 8.10 0 3 -7 19.90 9.20 0 -3 -7 9.70 11.40 0 -3 7 4.30 9.60 0 3 -8 21.60 10.80 0 3 -8 34.70 14.40 0 3 8 55.29 13.30 0 -3 8 31.80 12.40 0 -3 -8 36.60 14.50 0 3 9 81.09 16.60 0 3 -9 96.19 19.80 0 3 -9 87.19 15.80 0 -3 9 96.39 18.20 0 -3 -9 76.89 21.10 0 3 10 172.38 23.50 0 3 -10 133.29 23.10 0 3 -10 156.58 23.00 0 -3 -10 138.29 26.00 0 -3 10 191.38 24.10 0 3 -11 75.59 26.30 0 3 11 69.49 22.30 0 -3 11 67.59 24.10 0 -3 -11 69.79 27.70 0 4 0 856.41 35.90 0 4 0 838.12 35.90 0 -4 0 872.61 36.00 0 -4 0 866.31 35.90 0 4 -1 4143.89 167.48 0 4 1 4062.79 167.18 0 -4 1 4116.29 167.58 0 -4 -1 4036.20 167.28 0 4 -2 7127.99 285.47 0 4 2 6707.63 284.87 0 -4 -2 6850.51 285.27 0 -4 2 7206.78 285.77 0 4 -3 66.59 7.80 0 4 3 59.29 7.00 0 4 3 53.89 6.20 0 -4 -3 63.69 4.90 0 -4 -3 58.19 7.40 0 -4 3 64.79 7.90 0 4 4 298.47 17.40 0 4 4 302.57 18.70 0 4 -4 316.77 19.00 0 -4 -4 313.17 18.90 0 -4 4 316.07 19.60 0 -4 -4 315.67 15.40 0 4 -5 837.22 39.50 0 4 5 750.32 37.60 0 4 5 752.02 39.40 0 -4 5 797.82 39.40 0 -4 -5 802.82 35.10 0 -4 -5 791.42 39.30 0 4 -6 1.90 8.70 0 4 6 -6.60 8.00 0 4 -6 14.50 8.70 0 4 6 0.80 6.20 0 -4 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39.10 0 -5 4 852.41 40.90 0 -5 -4 851.51 40.30 0 -5 -4 895.61 37.50 0 5 5 469.05 27.00 0 5 5 475.25 25.10 0 5 -5 463.05 26.70 0 -5 -5 486.55 22.80 0 -5 5 479.95 27.30 0 -5 -5 465.85 27.00 0 5 -6 15.00 10.70 0 5 -6 15.30 8.70 0 5 6 10.30 8.30 0 5 6 18.60 6.60 0 -5 -6 19.60 5.20 0 -5 6 34.00 10.00 0 -5 -6 13.70 9.60 0 5 -7 137.19 17.80 0 5 7 122.99 18.90 0 5 -7 109.09 16.20 0 5 7 114.19 15.60 0 -5 7 167.38 18.80 0 -5 -7 106.29 10.40 0 -5 -7 130.49 18.20 0 -5 7 112.99 8.90 0 5 8 40.60 16.60 0 5 -8 31.50 13.20 0 5 8 9.70 9.70 0 5 -8 16.20 10.70 0 -5 -8 32.90 15.20 0 -5 8 16.40 21.40 0 5 9 269.67 26.40 0 5 -9 291.57 31.10 0 5 -9 252.77 24.80 0 -5 9 338.97 32.80 0 -5 -9 280.67 33.40 0 5 -10 261.37 27.80 0 5 10 313.17 32.20 0 5 -10 305.37 35.90 0 -5 -10 231.68 31.10 0 -5 10 395.56 37.80 0 5 -11 19.20 23.10 0 5 -11 22.30 18.20 0 5 11 35.90 19.30 0 -5 11 42.70 22.60 0 -5 -11 32.70 26.90 0 6 0 2466.05 102.99 0 6 0 2518.45 103.09 0 -6 0 2475.35 102.99 0 -6 0 2542.55 103.09 0 6 -1 119.09 6.90 0 6 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547.75 34.00 0 11 7 234.78 23.90 0 11 7 253.37 19.70 0 11 -7 225.38 22.80 0 -11 7 275.37 36.40 0 -11 -7 235.58 17.10 0 -11 -7 244.68 25.50 0 11 8 66.39 17.90 0 11 8 50.19 11.80 0 11 -8 82.09 16.30 0 -11 -8 58.99 18.20 0 -11 8 62.39 18.70 0 -11 -8 79.79 11.10 0 11 9 43.00 20.40 0 11 -9 86.49 37.80 0 11 -9 78.89 20.70 0 11 9 77.59 15.50 0 -11 9 66.19 27.20 0 -11 -9 83.99 12.70 0 11 10 39.20 27.80 0 11 -10 -12.50 19.60 0 11 10 -6.60 15.30 0 -11 -10 -20.50 23.10 0 -11 -10 6.90 11.10 0 -11 10 28.90 24.50 0 12 0 66.09 7.40 0 12 0 79.49 7.30 0 -12 0 90.29 7.80 0 -12 0 78.89 7.20 0 12 -1 266.37 15.30 0 12 -1 265.37 14.60 0 12 1 269.37 14.80 0 -12 -1 265.57 14.90 0 -12 1 265.07 14.70 0 -12 -1 275.87 14.80 0 -12 1 262.27 15.40 0 12 -2 297.97 16.80 0 12 2 306.97 16.50 0 -12 2 301.87 16.70 0 -12 -2 309.27 16.50 0 -12 2 305.87 18.10 0 -12 -2 311.57 17.30 0 12 -3 157.08 12.60 0 12 3 168.58 11.80 0 -12 3 169.08 12.30 0 -12 -3 179.78 13.40 0 -12 3 163.88 14.40 0 -12 -3 174.28 11.60 0 12 -4 52.09 8.80 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37.90 10.00 0 -16 4 59.59 12.90 0 -16 -4 25.50 7.50 0 -16 4 40.80 8.20 0 16 -5 29.70 9.80 0 16 5 34.20 11.70 0 -16 5 27.80 9.10 0 -16 -5 12.90 9.40 0 -16 5 27.10 13.30 0 16 6 1.10 13.00 0 16 6 -1.60 8.80 0 16 -6 10.00 9.80 0 -16 -6 0.70 12.20 0 -16 6 2.80 9.60 0 -16 -6 22.80 8.30 0 -16 6 4.80 12.60 0 16 7 280.67 31.20 0 16 -7 314.57 26.90 0 16 7 310.67 24.70 0 -16 -7 370.06 32.30 0 -16 7 294.17 25.90 0 -16 -7 323.17 22.40 0 -16 7 304.57 34.20 0 16 8 23.00 12.70 0 16 8 19.70 19.30 0 16 -8 14.90 15.80 0 -16 -8 5.10 23.90 0 -16 8 19.50 21.00 0 -16 -8 14.90 10.00 0 16 -9 -24.60 18.30 0 16 9 14.20 21.90 0 16 9 14.80 15.40 0 -16 -9 -22.60 24.10 0 -16 9 -23.20 27.30 0 -16 -9 4.50 12.00 0 17 0 12.70 4.90 0 17 0 5.10 5.40 0 -17 0 7.70 5.80 0 -17 0 1.90 4.80 0 17 -1 3.80 5.00 0 17 1 -4.10 5.10 0 17 -1 4.80 5.70 0 -17 -1 5.60 5.10 0 -17 1 -6.50 6.00 0 -17 -1 2.20 5.20 0 -17 1 1.00 4.40 0 17 -2 111.59 11.40 0 17 2 111.39 11.70 0 -17 -2 123.79 12.20 0 -17 2 108.79 11.60 0 -17 2 100.89 13.50 0 -17 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2.90 22.10 0 -19 8 0.00 15.80 0 -19 8 -22.50 25.20 0 -19 -8 21.30 12.80 0 -19 -8 -18.50 21.30 0 20 0 48.40 8.30 0 20 0 43.60 8.90 0 -20 0 42.50 9.20 0 -20 0 33.90 9.10 0 20 1 14.80 7.40 0 20 -1 6.30 6.20 0 20 -1 2.00 7.90 0 -20 -1 -3.30 7.10 0 -20 1 7.20 6.30 0 -20 -1 3.50 7.40 0 -20 1 2.50 8.20 0 20 2 17.30 8.10 0 20 -2 11.80 6.80 0 -20 -2 10.60 7.70 0 -20 2 25.90 7.90 0 -20 2 4.40 11.20 0 -20 -2 20.80 8.20 0 20 3 111.49 13.90 0 20 -3 105.49 14.00 0 -20 -3 103.59 13.40 0 -20 3 117.69 14.30 0 20 4 -1.50 9.50 0 20 -4 11.60 8.80 0 -20 -4 3.30 10.20 0 -20 4 9.10 13.50 0 -20 -4 5.10 7.70 0 -20 4 12.40 8.70 0 20 5 36.80 15.90 0 20 5 35.80 10.60 0 20 -5 45.10 11.80 0 -20 -5 30.40 10.00 0 -20 -5 43.10 13.60 0 -20 5 33.60 11.20 0 -20 5 27.00 16.10 0 20 6 13.90 11.60 0 20 6 11.50 16.40 0 -20 -6 18.60 10.70 0 -20 6 13.80 11.80 0 -20 -6 4.60 14.30 0 -20 6 20.30 18.80 0 20 7 83.59 15.50 0 20 7 58.69 23.40 0 20 -7 36.60 16.10 0 -20 7 44.80 24.30 0 -20 7 45.10 14.90 0 -20 -7 49.50 13.70 0 -20 -7 51.79 13.30 0 -20 -7 85.19 21.20 0 20 8 10.80 24.00 0 20 8 27.50 15.90 0 20 -8 11.50 18.20 0 -20 8 32.20 28.60 0 -20 -8 40.00 14.90 0 -20 -8 19.50 14.90 0 -20 8 3.90 18.20 0 -20 -8 35.80 23.70 0 21 0 6.60 8.40 0 -21 0 0.30 9.30 0 -21 0 4.00 6.60 0 21 -1 339.87 22.60 0 21 -1 368.66 25.10 0 -21 1 374.06 23.00 0 -21 -1 323.87 23.00 0 -21 1 362.06 25.50 0 -21 -1 457.45 32.10 0 21 -2 4.60 7.20 0 21 2 -4.40 8.00 0 -21 2 2.50 6.80 0 -21 -2 0.90 8.10 0 -21 -2 5.70 8.40 0 21 -3 549.54 31.40 0 -21 -3 499.25 33.60 0 -21 3 621.64 36.60 0 -21 3 577.34 31.60 0 -21 -3 579.94 33.90 0 21 4 -11.90 8.50 0 21 -4 18.60 9.10 0 -21 4 4.90 15.00 0 -21 4 -3.20 8.20 0 -21 -4 15.40 9.70 0 -21 -4 3.40 11.50 0 21 5 21.70 17.30 0 21 -5 50.29 12.60 0 21 5 69.69 12.30 0 -21 -5 53.19 16.10 0 -21 5 47.30 18.60 0 -21 5 61.29 12.90 0 21 -6 193.28 24.40 0 21 6 231.08 31.80 0 21 6 234.38 23.50 0 -21 6 218.98 23.60 0 -21 -6 205.38 23.40 0 -21 6 231.48 29.90 0 21 7 13.00 14.60 0 21 7 -13.70 22.10 0 21 -7 -2.50 14.90 0 -21 -7 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11.90 8 10 -7 35.60 7.80 -8 10 7 -12.10 23.60 8 -10 -7 32.70 7.00 8 -10 -7 41.10 10.80 -8 -10 7 38.80 11.00 -8 -10 7 25.90 5.80 -8 10 6 7.50 19.10 -8 10 6 17.80 6.10 8 -10 -6 5.50 10.60 -8 -10 6 17.70 4.50 -8 -10 6 16.30 9.80 8 -10 -6 17.00 5.60 8 -10 -6 -3.60 12.40 -8 -10 6 1.20 8.40 -8 10 5 137.89 10.90 8 10 -5 139.89 10.10 8 -10 -5 129.79 12.50 -8 -10 5 117.39 13.60 -8 -10 5 123.29 9.00 8 -10 -5 115.59 10.20 -8 -10 5 131.69 16.30 -8 -10 4 100.39 11.40 8 -10 -4 110.09 9.90 -8 -10 4 126.59 15.60 -8 -10 4 106.59 8.70 8 -10 -4 120.49 10.60 8 -10 -3 35.70 5.90 8 -10 -3 38.50 7.30 -8 -10 3 40.20 11.80 -8 -10 3 30.40 8.30 8 10 -2 189.98 11.90 -8 -10 2 192.78 13.40 8 -10 -2 188.18 11.90 -8 -10 2 211.48 20.50 8 -10 -2 175.78 15.00 -8 -10 2 185.38 12.60 8 10 -1 146.89 10.40 -8 10 1 152.68 10.40 8 10 -1 145.99 15.80 -8 -10 1 120.29 13.30 8 -10 -1 149.29 10.80 -8 -10 1 164.18 19.40 -8 -10 1 139.99 10.50 -8 10 0 47.50 6.60 8 10 0 43.30 6.60 8 -10 0 48.40 11.00 -8 -10 0 40.70 6.40 -8 -10 0 51.39 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8 -11 1 15.30 7.20 -8 -11 -1 27.60 11.90 -8 -11 -1 16.60 10.40 8 -11 1 17.50 11.20 8 11 2 52.19 8.80 8 -11 2 40.40 9.00 8 -11 2 34.60 14.40 -8 -11 -2 40.10 14.40 8 11 3 192.78 17.90 8 -11 3 204.88 27.80 -8 -11 -3 132.89 21.20 8 11 4 0.50 10.70 -8 11 -4 5.50 11.70 -8 -11 -4 18.70 15.40 8 -11 4 21.70 15.80 -8 -11 -4 47.20 26.00 8 -11 4 25.60 17.80 -8 11 -5 0.50 14.80 8 11 5 8.00 9.00 8 11 5 24.40 13.60 8 -11 5 11.10 17.90 -8 -11 -5 2.30 15.80 -8 -11 -5 47.80 19.50 8 -11 5 19.50 21.20 -8 12 10 144.59 48.70 -8 12 9 75.09 11.30 8 12 -9 15.20 42.80 8 12 -9 66.99 13.60 -8 12 9 16.60 34.50 8 -12 -9 87.09 18.90 8 -12 -9 52.69 12.80 -8 -12 9 91.79 19.10 -8 12 8 163.98 14.50 8 12 -8 124.39 16.50 -8 12 8 65.79 29.60 8 -12 -8 121.69 15.10 -8 -12 8 119.89 17.30 -8 -12 8 141.69 17.00 8 -12 -8 100.19 17.30 8 12 -7 17.20 7.40 -8 12 7 21.10 23.10 -8 12 7 12.90 7.00 8 -12 -7 34.80 11.40 -8 -12 7 21.10 11.50 -8 -12 7 12.50 11.50 -8 -12 7 -2.40 5.20 8 -12 -7 18.70 7.10 8 12 -6 396.06 21.80 -8 -12 6 419.86 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8.70 11.60 -8 -14 6 7.80 6.10 8 14 -5 54.99 8.20 -8 14 5 44.50 21.30 8 -14 -5 50.49 8.80 -8 -14 5 51.89 12.90 8 -14 -5 59.19 10.40 -8 -14 5 38.70 7.50 -8 14 4 14.60 17.30 -8 -14 4 -2.50 10.20 -8 -14 4 0.80 5.60 8 -14 -4 0.10 6.90 8 -14 -4 0.20 6.50 -8 14 3 186.28 26.90 8 -14 -3 170.38 16.30 -8 -14 3 199.88 21.60 8 -14 -3 226.88 15.20 -8 -14 3 212.48 15.40 -8 14 2 -19.40 12.70 8 14 -2 -7.20 5.50 -8 -14 2 12.10 12.30 8 -14 -2 0.80 5.40 -8 -14 2 2.90 6.90 8 -14 -2 -3.50 9.20 -8 14 1 -7.20 13.20 -8 14 1 2.20 5.60 8 14 -1 -0.40 5.40 -8 -14 1 2.80 10.30 8 -14 -1 -7.40 9.50 8 -14 -1 0.40 5.60 -8 -14 1 -1.70 7.70 -8 14 0 131.39 21.10 8 -14 0 128.19 16.40 -8 -14 0 115.89 18.40 8 -14 0 106.89 12.60 -8 14 -1 4.20 13.00 8 14 1 14.10 7.00 8 -14 1 -0.50 12.30 -8 -14 -1 -4.40 6.70 -8 -14 -1 6.40 11.80 8 -14 1 -4.80 7.00 -8 -14 -1 -4.40 10.90 -8 14 -2 81.59 18.30 8 14 2 89.59 12.30 8 -14 2 76.09 12.10 -8 -14 -2 54.79 15.40 8 -14 2 111.59 18.90 -8 14 -3 5.20 13.40 -8 14 -3 -3.70 10.50 8 14 3 -6.80 9.30 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8.20 -8 -15 3 91.39 18.70 -8 -15 3 71.29 10.10 8 -15 -3 107.69 12.30 8 15 -2 7.10 6.40 -8 15 2 10.80 14.50 -8 -15 2 2.60 10.40 -8 -15 2 4.10 7.50 8 -15 -2 -4.40 5.80 -8 -15 2 3.20 8.90 8 -15 -2 11.60 10.10 -8 15 1 333.57 31.20 8 15 -1 321.57 19.90 -8 -15 1 271.87 27.10 8 -15 -1 338.97 19.80 8 -15 -1 306.17 24.70 8 15 0 62.99 9.40 -8 15 0 97.79 20.30 8 -15 0 86.89 15.60 -8 -15 0 64.19 15.30 -8 -15 0 76.89 10.20 8 -15 0 99.89 11.40 -8 15 -1 12.30 14.30 8 15 1 12.40 7.30 8 -15 1 22.00 14.00 -8 -15 -1 -2.20 11.70 -8 -15 -1 10.00 12.80 8 -15 1 17.10 8.00 -8 -15 -1 -1.40 7.20 8 15 2 142.59 16.30 -8 15 -2 134.59 23.30 8 -15 2 101.69 13.60 8 -15 2 155.58 22.20 -8 -15 -2 121.29 20.60 -8 -15 -2 158.58 16.20 8 15 3 23.20 11.00 -8 15 -3 -2.40 14.30 -8 15 -3 15.90 11.30 8 -15 3 51.99 20.20 -8 -15 -3 22.90 9.00 8 -15 3 27.10 11.90 -8 -15 -3 34.10 16.50 -8 15 -4 11.30 15.40 8 15 4 17.20 12.80 -8 15 -4 -6.20 13.50 -8 -15 -4 31.70 20.60 8 -15 4 29.10 13.70 -8 -15 -4 74.49 21.30 8 -15 4 86.29 23.50 -8 16 8 2.90 27.30 8 16 -8 0.40 10.50 -8 16 8 -17.80 11.00 -8 -16 8 68.09 20.30 -8 -16 8 5.50 8.90 8 -16 -8 21.80 16.60 -8 -16 8 4.20 14.90 8 -16 -8 12.70 10.20 8 16 -7 212.88 19.20 -8 16 7 197.98 18.80 -8 -16 7 204.58 27.60 -8 -16 7 193.78 24.30 8 -16 -7 190.38 24.70 8 -16 -7 173.08 18.20 -8 16 6 285.07 20.50 8 16 -6 316.47 20.10 -8 16 6 270.67 37.10 8 -16 -6 226.98 23.30 -8 -16 6 227.58 26.70 8 -16 -6 248.18 19.30 -8 -16 6 254.67 26.10 8 16 -5 126.99 14.20 -8 16 5 166.78 30.10 -8 16 5 163.08 16.60 -8 -16 5 110.99 25.00 -8 -16 5 137.49 17.50 8 -16 -5 123.49 17.00 8 -16 -5 117.09 14.40 -8 16 4 270.37 34.20 8 -16 -4 287.87 21.40 -8 -16 4 259.47 25.40 8 -16 -4 307.37 20.60 -8 -16 4 272.97 23.10 -8 16 3 51.49 19.10 -8 -16 3 49.90 14.90 -8 -16 3 27.10 10.20 8 -16 -3 63.19 9.60 8 -16 -3 49.20 10.50 8 16 -2 98.79 13.20 -8 16 2 118.59 26.50 -8 -16 2 56.99 10.80 8 -16 -2 90.59 11.90 8 -16 -2 105.19 13.60 -8 -16 2 63.59 14.70 -8 16 1 21.70 16.40 -8 -16 1 -0.80 9.20 8 -16 -1 22.70 7.40 -8 -16 1 43.60 14.50 8 -16 -1 39.30 12.10 -8 -16 1 30.50 8.30 8 16 0 3.10 7.10 -8 16 0 -0.60 14.60 -8 -16 0 13.60 8.00 8 -16 0 4.80 12.20 8 -16 0 0.40 6.80 -8 -16 0 24.00 13.00 -8 -16 0 -5.70 10.00 -8 16 -1 -5.00 15.70 -8 16 -1 -2.60 9.00 8 16 1 3.80 8.00 -8 -16 -1 -14.30 7.70 8 -16 1 -12.00 7.70 -8 -16 -1 3.60 12.70 8 -16 1 2.40 14.60 -8 -16 -1 1.60 14.70 -8 16 -2 316.57 31.20 8 16 2 333.77 23.10 8 -16 2 387.26 35.50 8 -16 2 366.06 25.20 -8 -16 -2 285.37 32.20 -8 -16 -2 314.47 23.00 -8 16 -3 7.80 12.00 8 16 3 50.59 12.60 8 -16 3 80.79 22.30 -8 -16 -3 77.49 12.00 -8 -16 -3 -0.90 17.80 8 -16 3 33.70 12.10 -8 -16 -3 59.49 18.90 -8 16 -4 5.40 16.20 8 16 4 6.70 15.20 -8 16 -4 8.40 14.00 8 -16 4 -22.70 13.50 -8 -16 -4 11.90 20.70 -8 -16 -4 -8.30 19.20 8 -16 4 25.80 25.00 8 17 -8 82.89 14.60 -8 17 8 31.90 31.00 8 -17 -8 121.79 20.50 8 -17 -8 95.69 14.80 -8 -17 8 122.69 19.90 8 17 -7 -9.80 9.50 -8 17 7 3.40 24.70 -8 17 7 10.60 10.50 8 -17 -7 -0.20 9.30 -8 -17 7 5.90 15.20 -8 -17 7 3.40 8.50 -8 -17 7 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124.49 32.20 10 1 -9 81.69 12.10 10 1 -9 67.99 10.90 10 -1 -9 67.49 26.90 10 -1 -9 91.29 12.20 10 -1 -9 66.19 12.90 10 1 -8 125.79 15.60 10 1 -8 150.48 31.20 10 1 -8 104.69 11.40 10 -1 -8 115.99 26.90 10 -1 -8 123.19 16.40 10 -1 -8 95.59 12.90 10 1 -7 82.99 26.30 10 -1 -7 45.70 22.20 10 -1 -7 35.70 13.70 10 1 -6 172.38 26.90 10 1 -6 199.58 30.80 10 -1 -6 216.68 30.00 10 1 -5 314.07 24.30 10 1 -5 378.86 36.10 10 -1 -5 357.86 26.10 10 -1 -5 368.86 34.20 10 1 -4 366.76 26.80 10 1 -4 431.16 35.40 10 -1 -4 360.26 27.40 10 -1 -4 420.06 33.70 10 1 -3 26.90 11.10 10 -1 -3 11.40 10.60 10 1 -2 198.88 28.00 10 1 -2 186.68 21.20 10 -1 -2 225.88 22.60 10 -1 -2 235.48 24.30 10 1 -1 40.60 12.40 10 1 -1 26.70 4.10 10 1 -1 35.50 13.40 10 -1 -1 37.80 12.80 10 -1 -1 40.50 11.80 10 -1 -1 25.90 4.80 10 1 0 8.90 10.30 10 1 0 -0.60 5.20 10 -1 0 -1.10 5.80 10 -1 0 5.00 8.90 -10 -1 0 -2.20 2.60 10 1 1 -5.30 7.10 -10 1 -1 18.70 6.50 10 1 1 6.70 8.30 10 -1 1 4.30 7.90 -10 -1 -1 6.90 6.40 10 1 2 58.89 11.40 10 1 2 45.80 14.80 10 -1 2 68.69 17.00 10 -1 2 65.59 11.90 10 1 3 44.40 16.50 10 1 3 39.90 12.90 -10 1 -3 -5.80 11.30 10 -1 3 13.30 16.00 -10 -1 -3 -11.50 11.30 10 -1 3 38.80 13.40 -10 1 -4 1.20 14.40 10 1 4 33.10 15.30 10 1 4 41.90 17.00 10 -1 4 -2.20 14.10 -10 -1 -4 11.40 14.50 10 -1 4 38.60 17.00 10 2 -10 53.79 14.20 -10 2 10 64.29 7.70 10 -2 -10 43.50 15.00 -10 -2 10 75.79 8.00 10 2 -9 7.40 26.60 10 2 -9 7.90 8.80 10 -2 -9 7.30 9.30 10 -2 -9 0.60 10.90 10 -2 -9 14.80 22.40 10 2 -8 89.89 11.80 10 2 -8 59.49 7.60 10 2 -8 101.79 28.10 10 -2 -8 61.49 9.50 10 -2 -8 69.09 12.80 10 -2 -8 77.49 24.70 10 2 -7 13.70 16.20 10 2 -7 8.00 20.20 10 -2 -7 57.19 21.10 10 -2 -7 4.90 3.50 10 -2 -7 19.20 11.00 10 2 -6 6.70 19.70 10 -2 -6 9.00 12.20 10 -2 -6 17.90 18.30 10 2 -5 10.80 9.20 10 2 -5 -4.80 17.50 10 -2 -5 8.30 15.60 10 -2 -5 -2.20 10.20 10 2 -4 96.29 22.70 10 2 -4 89.19 13.90 10 -2 -4 90.99 19.20 10 -2 -4 65.19 14.00 10 2 -3 18.50 10.40 10 2 -3 33.60 18.20 10 -2 -3 37.80 12.60 10 2 -2 3.60 10.50 10 -2 -2 9.90 11.00 10 -2 -2 21.30 10.50 10 2 -1 54.79 14.90 10 2 -1 28.80 11.70 10 2 -1 36.40 4.50 10 -2 -1 51.09 14.00 10 -2 -1 44.60 5.30 10 -2 -1 33.60 5.60 10 -2 -1 44.60 12.30 -10 2 0 26.80 3.80 10 2 0 27.80 6.10 10 2 0 26.60 11.50 -10 -2 0 28.00 3.60 10 -2 0 29.00 10.30 10 -2 0 22.30 7.10 10 2 1 46.90 8.70 -10 2 -1 53.29 7.50 10 2 1 62.39 11.80 10 -2 1 50.39 9.90 -10 -2 -1 41.10 8.20 -10 2 -2 -11.00 7.60 10 2 2 0.50 12.50 10 2 2 12.10 9.40 -10 -2 -2 1.10 8.90 10 -2 2 -7.70 13.90 10 -2 2 -1.00 10.50 10 2 3 302.47 26.40 10 2 3 289.37 30.00 10 -2 3 324.37 31.90 10 -2 3 328.37 28.50 10 2 4 47.80 16.00 10 2 4 61.39 19.10 10 -2 4 86.59 20.00 10 -2 4 57.69 16.50 -10 -2 -4 6.10 14.80 -10 3 10 0.50 6.10 10 3 -10 7.00 12.00 -10 -3 10 21.30 6.80 10 -3 -10 9.10 8.90 10 -3 -10 7.50 14.40 10 3 -9 35.70 9.70 10 3 -9 74.09 29.70 10 -3 -9 47.40 25.50 10 -3 -9 39.80 10.70 10 -3 -9 29.80 12.10 10 3 -8 11.20 8.70 10 3 -8 15.70 5.80 10 3 -8 6.70 23.40 10 -3 -8 15.20 10.80 10 -3 -8 23.80 21.00 10 -3 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10 -4 -1 18.30 12.60 10 4 0 189.58 12.20 -10 4 0 162.68 10.00 10 4 0 202.28 22.90 10 -4 0 144.99 15.70 -10 -4 0 198.68 10.00 -10 -4 0 152.18 10.90 10 4 1 -1.30 10.40 -10 4 -1 20.10 6.30 10 4 1 6.50 7.10 10 -4 1 0.20 14.90 10 -4 1 12.30 9.80 -10 -4 -1 -10.20 7.30 10 4 2 25.30 12.30 -10 4 -2 -1.80 8.20 10 4 2 12.30 8.70 10 4 2 23.60 9.30 10 -4 2 6.70 14.90 -10 -4 -2 -14.40 9.60 10 -4 2 10.20 11.50 10 4 3 6.80 11.40 -10 4 -3 -21.80 10.30 10 4 3 6.90 14.40 10 -4 3 5.20 16.40 -10 -4 -3 -28.70 12.00 10 -4 3 16.80 14.50 10 4 4 36.50 14.00 -10 4 -4 -11.60 13.80 10 4 4 12.60 16.20 10 -4 4 16.90 19.90 10 -4 4 -3.90 16.10 -10 -4 -4 11.60 16.00 10 5 -10 15.90 12.20 -10 5 10 19.70 7.30 10 -5 -10 14.00 10.70 -10 -5 10 24.10 8.60 10 -5 -10 19.40 16.60 10 5 -9 13.10 29.00 10 5 -9 25.40 9.10 10 -5 -9 37.10 23.60 10 -5 -9 -3.60 13.30 10 -5 -9 42.30 12.60 10 5 -8 21.80 7.90 10 5 -8 -17.20 24.90 10 -5 -8 5.40 19.90 10 -5 -8 0.20 12.00 10 -5 -8 12.80 10.50 10 -5 -8 -1.50 4.70 10 5 -7 67.29 28.90 10 5 -7 128.09 15.50 10 5 -7 75.89 8.80 10 -5 -7 139.99 13.90 10 -5 -7 97.79 7.70 10 -5 -7 142.39 20.40 10 -5 -7 118.49 25.40 10 5 -6 -0.20 8.80 10 5 -6 28.20 24.00 10 -5 -6 17.00 11.30 10 -5 -6 1.70 16.20 10 5 -5 5.00 8.80 10 5 -5 -6.20 21.60 10 -5 -5 17.40 12.60 10 -5 -5 -9.30 13.10 10 5 -4 272.07 21.90 10 -5 -4 305.77 26.40 10 -5 -4 278.97 27.80 10 5 -3 209.28 20.40 10 -5 -3 253.17 24.50 10 -5 -3 196.98 23.20 10 5 -2 10.00 17.60 10 5 -2 15.00 10.30 10 5 -2 17.70 2.70 10 -5 -2 20.20 5.30 10 -5 -2 32.20 14.90 10 -5 -2 16.70 12.70 10 -5 -2 22.60 3.80 10 5 -1 358.36 27.00 10 5 -1 346.07 17.00 10 -5 -1 430.06 31.60 10 -5 -1 370.36 18.10 10 -5 -1 324.17 20.40 10 5 0 5.50 5.00 -10 5 0 -0.10 3.90 10 5 0 -10.90 13.90 10 -5 0 -2.10 8.00 10 -5 0 0.20 5.70 -10 -5 0 4.90 3.60 10 5 1 221.68 16.00 -10 5 -1 186.88 13.80 10 5 1 239.88 23.30 10 -5 1 184.08 20.20 -10 -5 -1 199.98 16.90 10 5 2 16.00 9.80 -10 5 -2 8.60 8.50 10 5 2 13.30 12.50 10 5 2 1.60 9.00 10 -5 2 17.20 15.70 -10 -5 -2 -2.10 10.70 10 -5 2 6.50 11.80 10 5 3 109.69 17.90 10 5 3 70.09 14.00 10 -5 3 149.79 23.00 10 -5 3 80.99 18.20 -10 5 -4 -8.30 13.60 10 5 4 10.60 16.10 10 5 4 11.00 14.00 10 -5 4 1.90 20.30 10 -5 4 -35.30 17.10 -10 -5 -4 -27.20 16.20 10 6 -9 17.90 33.80 10 6 -9 32.00 9.20 -10 6 9 30.00 6.20 10 -6 -9 39.60 14.40 10 -6 -9 20.60 14.80 -10 -6 9 29.10 3.90 10 -6 -9 17.10 7.90 10 -6 -9 49.20 25.70 10 6 -8 -1.50 5.40 10 6 -8 -36.40 28.60 10 -6 -8 2.10 10.70 10 -6 -8 10.40 19.90 10 -6 -8 -3.90 5.20 10 -6 -8 -0.20 15.60 10 6 -7 15.30 4.80 10 6 -7 -17.30 26.20 10 -6 -7 18.60 12.80 10 -6 -7 3.10 8.70 10 -6 -7 8.20 4.30 10 -6 -7 26.10 18.40 10 6 -6 18.80 8.90 10 6 -6 -20.50 21.80 10 -6 -6 20.10 6.60 10 -6 -6 34.60 13.20 10 -6 -6 31.20 17.30 10 6 -5 25.00 9.20 10 6 -5 19.80 22.80 10 -6 -5 16.80 15.20 10 -6 -5 4.10 12.20 10 6 -4 247.98 20.50 10 -6 -4 244.28 26.70 10 -6 -4 241.68 25.00 10 6 -3 -19.60 19.40 10 6 -3 22.30 9.70 10 -6 -3 40.90 13.40 10 -6 -3 26.70 12.20 10 6 -2 977.50 43.30 10 6 -2 1036.80 52.09 10 -6 -2 1048.60 54.69 10 -6 -2 1041.10 55.99 10 -6 -2 1055.79 44.10 10 6 -1 85.09 7.10 10 6 -1 77.29 14.20 10 -6 -1 65.79 10.20 10 -6 -1 45.00 16.00 10 6 0 5.60 5.10 10 6 0 -6.40 15.60 10 6 0 8.20 15.30 -10 6 0 7.60 4.10 10 -6 0 -1.90 5.90 -10 -6 0 6.80 6.30 10 -6 0 17.80 9.50 -10 -6 0 1.30 4.20 10 6 1 14.60 11.30 -10 6 -1 31.10 7.00 10 6 1 27.00 14.80 10 -6 1 38.60 15.70 10 6 2 71.39 14.60 10 6 2 83.69 11.70 10 6 2 90.79 14.60 10 -6 2 74.89 18.30 10 -6 2 75.29 15.30 10 6 3 8.10 11.60 10 6 3 33.70 15.10 -10 6 -3 -3.60 10.80 -10 -6 -3 12.70 14.30 10 -6 3 18.90 16.30 10 -6 3 55.49 19.70 -10 6 -4 -5.20 13.70 10 6 4 20.90 18.90 10 6 4 10.80 14.20 10 -6 4 -13.30 18.90 -10 -6 -4 30.40 18.00 10 -6 4 19.80 20.70 10 7 -9 9.80 8.70 -10 7 9 -6.00 5.90 10 7 -9 -4.10 33.10 10 -7 -9 10.20 7.50 10 -7 -9 -6.60 13.80 -10 -7 9 1.50 6.00 10 -7 -9 20.60 25.90 10 -7 -9 1.80 15.10 10 7 -8 0.30 5.70 10 7 -8 23.60 30.60 10 -7 -8 0.40 5.70 10 -7 -8 -2.40 11.20 10 -7 -8 8.20 21.50 10 -7 -8 -3.10 13.00 10 7 -7 62.79 7.70 10 7 -7 -2.50 27.50 10 -7 -7 68.59 15.50 10 -7 -7 59.09 7.80 10 -7 -7 74.79 11.60 10 -7 -7 62.49 22.70 10 7 -6 100.69 13.50 10 -7 -6 67.69 7.70 10 -7 -6 93.59 16.70 10 -7 -6 66.89 20.20 10 7 -5 7.20 8.90 10 7 -5 33.40 26.30 10 -7 -5 28.90 12.90 10 -7 -5 4.50 14.50 10 -7 -5 14.50 6.20 10 7 -4 62.29 11.60 10 7 -4 46.80 26.60 10 -7 -4 39.80 5.70 10 -7 -4 62.09 15.70 10 -7 -4 38.20 5.90 10 -7 -4 60.19 14.80 10 7 -3 -26.60 21.50 10 7 -3 4.50 9.10 10 -7 -3 2.40 4.20 10 -7 -3 8.80 11.50 10 -7 -3 -14.70 11.60 10 -7 -3 -1.40 5.60 10 7 -2 140.29 19.50 10 7 -2 156.18 9.60 10 -7 -2 178.38 10.50 10 -7 -2 214.78 24.50 10 -7 -2 152.08 13.60 10 7 -1 3.20 4.00 10 7 -1 -5.00 19.90 10 7 -1 9.00 10.20 10 -7 -1 6.60 4.80 -10 -7 1 1.70 2.90 10 -7 -1 10.70 8.60 10 -7 -1 14.80 13.70 -10 7 0 74.99 8.70 10 7 0 50.09 20.10 10 7 0 98.09 15.70 10 7 0 99.39 9.80 10 -7 0 97.59 10.80 -10 -7 0 84.79 9.80 10 7 1 -2.80 15.40 -10 7 -1 -1.20 6.20 10 7 1 -6.40 10.60 10 7 1 1.80 6.90 -10 -7 -1 11.30 5.50 10 -7 1 0.70 7.50 -10 -7 -1 1.30 9.30 10 -7 1 7.70 15.20 10 -7 1 16.70 12.00 10 7 2 11.50 12.80 10 7 2 -5.70 12.60 10 7 2 -3.00 8.90 -10 7 -2 10.20 8.80 -10 -7 -2 21.00 12.70 10 -7 2 -0.60 13.70 10 -7 2 24.90 16.20 -10 7 -3 8.00 11.80 10 7 3 0.60 14.50 10 7 3 30.60 11.90 10 -7 3 28.40 19.40 -10 -7 -3 8.40 15.80 -10 7 -4 5.50 14.20 -10 8 9 34.40 7.20 10 8 -9 -55.79 42.70 10 8 -9 18.10 9.20 10 -8 -9 43.40 15.10 10 -8 -9 42.20 9.40 -10 -8 9 44.70 8.60 10 -8 -9 22.00 27.60 10 8 -8 6.60 30.20 10 8 -8 32.20 7.40 -10 8 8 34.00 6.40 10 -8 -8 41.20 21.20 10 -8 -8 39.40 7.40 10 -8 -8 30.70 15.40 10 -8 -8 31.80 12.90 10 8 -7 8.80 31.00 10 8 -7 7.50 4.80 10 -8 -7 13.90 13.70 10 -8 -7 -11.30 17.10 10 -8 -7 -6.70 10.10 10 -8 -7 -3.40 4.70 10 8 -6 15.10 28.10 -10 8 6 37.20 32.10 10 -8 -6 76.59 20.60 10 -8 -6 77.09 15.90 10 -8 -6 65.69 9.90 10 -8 -6 58.69 7.00 10 8 -5 51.19 30.90 10 8 -5 154.68 17.00 10 -8 -5 156.78 24.20 10 -8 -5 111.89 10.50 10 -8 -5 173.98 23.00 -10 8 4 16.90 27.80 10 8 -4 25.00 25.40 10 8 -4 61.39 11.50 10 -8 -4 109.59 18.30 10 -8 -4 81.39 17.20 10 -8 -4 77.59 9.40 -10 8 3 -12.00 22.90 10 8 -3 13.30 24.90 10 8 -3 -4.60 8.90 10 -8 -3 4.10 12.90 10 -8 -3 2.30 6.50 10 -8 -3 -8.20 4.40 10 8 -2 373.46 25.30 10 8 -2 311.37 15.80 10 -8 -2 342.97 29.70 10 -8 -2 301.47 18.60 10 -8 -2 295.97 20.40 10 8 -1 24.40 24.80 10 8 -1 39.80 12.00 10 8 -1 32.60 5.30 10 -8 -1 27.40 9.50 -10 -8 1 40.50 5.00 10 -8 -1 28.10 5.90 10 -8 -1 31.30 14.50 -10 8 0 49.99 6.80 10 8 0 38.10 22.60 10 8 0 68.69 7.90 10 8 0 53.29 13.10 10 -8 0 45.70 7.80 -10 -8 0 41.00 9.20 10 -8 0 48.20 11.60 10 -8 0 2.00 17.30 -10 8 -1 -2.00 6.40 10 8 1 -24.20 10.20 10 8 1 29.50 20.00 10 8 1 -3.80 6.60 -10 -8 -1 4.60 10.40 10 -8 1 -8.30 7.60 -10 -8 -1 -3.90 5.60 10 -8 1 14.50 15.30 10 8 2 201.58 18.00 10 8 2 184.28 23.90 10 -8 2 216.88 28.20 -10 -8 -2 173.28 15.90 10 -8 2 194.88 23.00 10 8 3 144.69 20.20 10 8 3 176.78 22.30 10 8 3 208.88 19.20 10 -8 3 226.18 29.30 10 9 -9 62.29 11.00 -10 9 9 69.49 9.20 10 -9 -9 54.79 16.80 10 -9 -9 67.99 17.50 10 -9 -9 66.19 10.60 -10 -9 9 52.89 10.30 10 9 -8 25.70 7.40 -10 9 8 27.10 7.10 10 9 -8 -1.20 35.60 10 -9 -8 26.50 21.70 10 -9 -8 24.90 7.30 10 -9 -8 12.30 13.40 10 -9 -8 40.30 15.30 10 9 -7 18.20 5.80 -10 9 7 -0.70 34.20 10 9 -7 -31.00 31.40 10 -9 -7 12.90 5.80 10 -9 -7 -1.60 10.20 10 -9 -7 16.80 18.70 10 -9 -7 32.70 14.60 10 9 -6 264.97 47.40 -10 9 6 208.38 42.50 10 -9 -6 279.17 16.30 10 -9 -6 300.97 20.90 10 -9 -6 307.87 32.40 10 9 -5 -3.20 28.30 -10 9 5 15.10 28.80 10 -9 -5 23.80 6.70 10 -9 -5 43.70 17.40 10 -9 -5 45.70 7.90 10 9 -4 52.79 11.20 10 9 -4 9.80 27.00 10 -9 -4 45.90 7.80 10 -9 -4 45.50 7.70 10 9 -3 5.00 9.50 -10 9 3 23.50 25.50 10 9 -3 3.30 24.40 10 -9 -3 -0.20 5.00 10 -9 -3 9.50 7.40 -10 -9 3 -6.50 11.90 -10 9 2 24.40 23.80 10 9 -2 10.00 4.50 10 9 -2 8.30 9.50 10 -9 -2 17.80 5.10 -10 -9 2 3.80 12.70 10 -9 -2 31.90 9.70 10 9 -1 22.30 5.20 10 9 -1 12.10 10.50 -10 9 1 -4.30 22.10 10 -9 -1 8.10 13.80 -10 -9 1 8.70 6.60 -10 -9 1 17.80 5.30 10 -9 -1 -1.10 9.90 10 -9 -1 15.00 5.60 -10 -9 1 27.70 15.00 10 9 0 374.96 28.00 10 9 0 299.97 45.90 10 9 0 361.16 19.60 -10 -9 0 382.46 33.40 10 -9 0 367.06 27.00 -10 -9 0 304.27 22.10 10 -9 0 394.16 21.20 10 9 1 44.80 8.70 10 9 1 36.30 13.40 -10 9 -1 11.70 7.10 10 9 1 13.20 22.10 10 -9 1 35.80 8.80 -10 -9 -1 31.20 7.30 10 -9 1 34.30 16.80 10 -9 1 44.00 13.90 10 9 2 95.69 12.20 10 9 2 69.49 16.30 10 -9 2 61.29 21.00 10 -9 2 64.99 17.80 -10 -9 -2 71.49 10.20 10 -9 2 81.29 12.50 10 9 3 13.90 15.00 10 9 3 17.40 14.70 10 9 3 10.00 11.50 -10 9 -3 12.10 11.90 10 -9 3 25.40 18.80 10 -9 3 -18.10 18.70 -10 -9 -3 -12.70 16.30 -10 10 9 0.00 8.00 10 10 -9 8.30 9.30 10 -10 -9 -18.20 15.80 10 -10 -9 20.70 9.30 10 -10 -9 31.30 17.10 -10 -10 9 -10.10 10.80 10 10 -8 47.10 9.20 -10 10 8 11.00 42.10 -10 10 8 75.49 9.00 10 10 -8 19.70 36.50 10 -10 -8 83.29 17.80 10 -10 -8 71.49 23.00 10 -10 -8 68.39 9.60 10 -10 -8 63.69 15.20 -10 -10 8 66.19 9.00 10 10 -7 7.30 5.90 -10 10 7 25.10 34.10 10 10 -7 18.50 34.10 10 -10 -7 3.40 6.10 10 -10 -7 -12.70 17.50 10 -10 -7 -0.60 11.20 -10 10 6 10.10 29.00 10 10 -6 4.10 32.90 10 10 -5 63.49 33.50 -10 10 5 25.20 29.20 10 -10 -5 22.50 7.90 -10 -10 5 12.90 16.70 10 -10 -5 19.40 6.80 -10 10 4 37.00 26.30 10 -10 -4 54.09 9.20 10 -10 -4 67.49 8.40 -10 -10 4 66.59 15.70 10 -10 -3 68.39 9.40 -10 -10 3 100.39 17.30 10 -10 -3 81.99 10.60 -10 10 2 -4.50 22.40 10 10 -2 6.00 10.60 10 10 -2 1.20 4.80 10 -10 -2 0.70 9.20 -10 -10 2 9.20 4.90 -10 -10 2 10.50 14.10 10 -10 -2 0.20 4.90 10 10 -1 122.49 10.60 -10 10 1 74.49 26.40 10 10 -1 129.49 17.10 10 -10 -1 138.59 11.40 10 -10 -1 143.19 19.30 -10 -10 1 90.99 18.40 -10 -10 1 98.69 12.90 -10 10 0 97.79 25.10 -10 -10 0 155.28 11.50 10 -10 0 131.79 20.90 -10 -10 0 100.29 13.00 -10 10 -1 -0.20 7.20 10 10 1 18.30 7.80 10 10 1 8.00 11.30 10 -10 1 22.40 15.60 -10 -10 -1 -15.90 13.70 -10 -10 -1 2.40 11.60 -10 -10 -1 -1.90 6.50 10 -10 1 -1.00 12.90 10 -10 1 -18.00 7.50 10 10 2 -8.20 9.10 10 10 2 19.40 22.50 10 10 2 1.20 13.40 -10 10 -2 -1.20 9.10 10 -10 2 6.50 16.90 10 -10 2 38.50 19.60 10 -10 2 17.80 10.10 -10 -10 -2 18.00 14.20 -10 -10 -2 20.00 8.40 -10 10 -3 -13.60 11.70 10 10 3 -14.30 18.40 10 10 3 5.00 17.80 10 -10 3 -26.00 18.50 -10 -10 -3 24.70 18.50 10 -10 3 11.60 22.80 10 11 -8 164.98 15.80 -10 11 8 87.89 44.40 -10 11 8 141.69 14.80 -10 -11 8 193.88 16.80 10 -11 -8 150.58 18.70 10 -11 -8 148.79 14.60 10 11 -7 107.49 46.50 -10 11 7 83.59 37.00 10 11 -7 192.78 13.90 10 -11 -7 167.88 21.20 10 -11 -7 158.98 13.90 10 11 -6 105.79 40.10 -10 11 6 50.49 32.20 10 -11 -6 72.49 11.50 -10 -11 6 93.19 18.40 10 -11 -6 70.19 9.00 -10 11 5 23.80 27.40 10 -11 -5 28.80 8.40 10 -11 -5 17.70 7.10 -10 -11 5 46.60 16.40 -10 11 4 -16.10 22.10 10 -11 -4 3.80 7.70 -10 -11 4 7.80 13.80 10 -11 -4 2.00 6.60 -10 11 3 -5.40 27.50 10 -11 -3 -11.90 8.20 -10 -11 3 21.90 14.80 10 -11 -3 -4.40 5.50 -10 11 2 2.90 22.60 10 11 -2 46.40 6.90 10 -11 -2 41.80 11.10 -10 -11 2 30.70 15.50 10 -11 -2 37.90 7.10 -10 11 1 -1.00 21.50 10 11 -1 3.70 5.50 10 -11 -1 14.50 11.80 10 -11 -1 5.40 5.60 -10 -11 1 1.10 6.00 -10 -11 1 8.80 15.10 -10 -11 1 10.90 8.30 -10 11 0 -2.70 22.80 10 11 0 45.50 7.70 -10 -11 0 23.50 15.90 10 -11 0 29.90 7.70 -10 -11 0 3.80 9.50 -10 -11 0 34.80 7.40 10 -11 0 33.40 14.30 10 11 1 204.18 17.00 10 -11 1 198.08 23.00 10 -11 1 219.18 28.80 10 -11 1 220.88 18.50 -10 -11 -1 228.58 30.60 -10 -11 -1 193.48 15.80 -10 11 -2 -4.80 9.70 10 11 2 4.60 9.40 -10 -11 -2 35.00 17.20 10 -11 2 13.10 10.90 -10 -11 -2 7.30 15.20 -10 -11 -2 12.00 8.20 10 -11 2 14.30 20.30 10 -11 2 27.20 17.80 -10 11 -3 -8.20 12.10 10 11 3 37.00 22.60 10 -11 3 26.50 13.20 10 -11 3 11.60 20.80 -10 -11 -3 20.20 18.50 -10 12 8 44.50 40.20 -10 12 8 131.29 15.60 10 12 -8 151.78 15.90 -10 -12 8 139.09 18.20 10 -12 -8 153.08 19.40 10 -12 -8 123.59 15.30 -10 12 7 61.09 36.00 10 12 -7 -1.50 6.70 10 12 -7 -10.90 41.10 10 -12 -7 6.90 7.40 -10 -12 7 1.50 8.80 10 -12 -7 10.30 11.50 -10 12 6 -20.60 31.10 10 -12 -6 -6.10 6.90 10 -12 -6 6.10 9.70 -10 12 5 -18.90 26.50 -10 -12 5 18.20 4.70 10 -12 -5 52.39 9.40 -10 -12 5 42.60 16.40 10 -12 -4 181.28 17.60 10 -12 -4 197.68 15.90 -10 -12 4 223.08 25.90 -10 -12 4 219.78 13.50 -10 12 3 -6.20 22.40 -10 -12 3 3.70 14.30 -10 -12 3 21.00 9.00 10 -12 -3 20.30 6.70 10 -12 -3 19.20 9.90 10 12 -2 240.28 15.40 10 -12 -2 246.78 15.70 -10 -12 2 254.17 29.00 10 -12 -2 216.88 22.00 -10 -12 2 213.98 16.50 10 12 -1 43.10 7.70 -10 12 1 17.80 22.30 10 -12 -1 44.40 13.40 -10 -12 1 32.60 17.20 -10 -12 1 42.50 8.00 -10 -12 1 23.80 9.50 10 -12 -1 47.70 8.30 -10 12 0 7.30 23.00 10 12 0 44.50 8.30 10 -12 0 57.59 15.20 -10 -12 0 47.50 8.50 -10 -12 0 14.10 11.10 10 -12 0 44.10 8.90 -10 -12 0 41.90 17.90 -10 12 -1 -11.90 23.20 10 12 1 39.50 9.50 10 -12 1 32.50 9.70 -10 -12 -1 39.70 8.30 10 -12 1 44.30 18.00 -10 -12 -1 -1.70 12.90 -10 -12 -1 62.79 20.30 10 12 2 70.79 12.40 -10 -12 -2 74.99 20.50 10 -12 2 39.00 21.40 10 -12 2 58.49 12.90 -10 -12 -2 61.69 11.20 -10 13 8 -4.00 10.00 -10 13 8 10.90 39.10 10 13 -8 15.00 9.20 -10 -13 8 6.90 12.80 10 -13 -8 2.50 14.90 10 -13 -8 4.90 9.30 10 13 -7 209.08 52.89 10 13 -7 240.48 17.40 10 -13 -7 259.07 24.20 10 -13 -7 210.68 17.70 -10 -13 7 211.88 20.10 -10 13 6 10.30 27.80 10 -13 -6 16.10 10.70 -10 -13 6 18.00 16.30 10 -13 -6 28.80 8.60 -10 -13 6 18.00 9.50 -10 13 5 7.20 25.90 10 -13 -5 83.39 11.60 10 -13 -5 86.39 11.40 -10 -13 5 93.19 18.80 -10 13 4 11.70 23.50 -10 -13 4 44.70 16.40 10 -13 -4 17.90 8.20 10 -13 -4 22.60 9.70 10 -13 -3 110.49 12.40 -10 -13 3 93.79 20.20 10 -13 -3 80.49 13.30 -10 -13 3 103.99 12.60 10 13 -2 10.70 6.80 -10 13 2 23.40 25.40 -10 -13 2 17.30 16.80 10 -13 -2 14.90 11.80 10 -13 -2 8.50 6.80 -10 -13 2 -1.60 7.80 -10 -13 2 17.80 8.60 10 13 -1 121.29 13.10 -10 -13 1 119.69 21.50 10 -13 -1 122.99 13.50 -10 -13 1 135.19 13.80 10 -13 -1 139.19 17.90 10 13 0 180.58 15.50 10 -13 0 182.58 16.30 10 -13 0 202.78 23.00 -10 -13 0 166.48 15.30 -10 -13 0 208.58 27.20 10 13 1 92.99 11.90 -10 13 -1 21.00 23.10 -10 -13 -1 24.60 14.70 10 -13 1 83.39 11.80 -10 -13 -1 20.60 19.40 10 -13 1 90.29 20.80 -10 -13 -1 55.19 10.10 10 13 2 7.50 10.70 -10 13 -2 12.30 10.80 10 -13 2 15.60 20.60 -10 -13 -2 0.10 16.30 -10 -13 -2 29.30 20.80 10 -13 2 -0.80 11.10 -10 14 7 38.50 36.50 10 14 -7 20.00 8.30 10 -14 -7 -18.90 12.80 -10 -14 7 11.80 12.30 -10 -14 7 -16.90 17.60 10 -14 -7 -6.60 8.70 -10 -14 7 12.70 12.10 -10 14 6 -33.80 27.30 -10 -14 6 8.30 16.40 10 -14 -6 31.20 11.80 10 -14 -6 -3.10 8.50 -10 -14 6 -6.90 10.90 -10 -14 5 120.19 21.80 10 -14 -5 100.69 12.90 10 -14 -5 90.69 12.80 -10 -14 5 126.09 13.70 -10 14 4 47.70 26.50 10 -14 -4 113.19 14.20 -10 -14 4 112.29 14.00 10 -14 -4 111.39 14.90 -10 -14 4 103.09 19.70 -10 -14 4 121.59 13.00 -10 14 3 17.60 22.50 10 -14 -3 1.80 10.90 -10 -14 3 0.70 9.10 -10 -14 3 -2.10 15.20 10 -14 -3 9.20 7.70 -10 -14 3 8.20 8.50 10 14 -2 23.80 8.00 -10 14 2 -10.40 22.50 -10 -14 2 -2.20 8.80 10 -14 -2 -4.20 11.60 -10 -14 2 -6.90 9.20 10 -14 -2 5.60 7.10 -10 -14 2 -24.50 15.40 10 14 -1 72.69 10.10 10 -14 -1 79.49 10.40 10 -14 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261.27 26.30 -10 -16 3 274.17 22.50 10 16 -2 7.80 9.50 -10 16 2 -13.50 22.50 -10 -16 2 28.90 10.70 -10 -16 2 -11.80 17.50 10 -16 -2 13.30 8.80 10 -16 -2 1.40 13.80 -10 -16 2 20.00 11.90 10 16 -1 17.70 9.50 -10 16 1 26.90 23.40 -10 -16 1 13.50 10.50 10 -16 -1 9.20 8.80 -10 -16 1 41.50 19.10 -10 -16 1 9.90 13.00 10 -16 -1 18.40 16.30 -10 16 0 -0.70 10.00 10 16 0 23.40 10.00 -10 16 0 32.20 28.30 10 -16 0 23.00 9.70 -10 -16 0 -24.10 14.20 10 -16 0 -6.70 18.10 -10 -16 0 22.10 10.20 -10 -16 0 23.60 19.50 -10 -17 5 139.49 17.70 -10 -17 5 95.69 23.70 10 -17 -5 115.89 16.40 10 -17 -5 157.48 21.00 -10 17 4 14.20 26.20 10 -17 -4 0.30 10.80 10 -17 -4 8.60 13.10 -10 -17 4 4.90 13.30 -10 -17 4 12.70 18.70 -10 -17 4 11.40 10.90 -10 17 3 -3.80 25.20 -10 -17 3 18.90 12.50 10 -17 -3 29.50 10.20 -10 -17 3 16.10 11.60 -10 -17 3 45.90 20.10 10 -17 -3 33.40 14.50 -10 17 2 24.50 24.40 10 17 -2 19.40 10.80 10 -17 -2 28.90 9.60 -10 -17 2 12.70 19.00 -10 -17 2 27.20 12.80 10 -17 -2 30.70 16.20 -10 -17 2 31.20 12.30 -10 17 1 39.70 25.90 10 17 -1 59.19 12.10 10 -17 -1 53.19 11.40 -10 -17 1 41.80 12.60 -10 -17 1 -2.80 14.80 10 -17 -1 33.20 17.90 -10 -17 1 43.30 21.20 -10 17 0 -23.80 23.70 -10 17 0 7.80 10.90 -10 -17 0 4.50 20.90 -10 18 4 83.89 32.80 -10 -18 4 182.68 34.80 10 -18 -4 161.48 20.90 -10 -18 4 194.38 27.30 10 -18 -4 183.28 25.10 -10 18 3 61.89 27.90 -10 -18 3 26.30 20.80 10 -18 -3 41.70 12.00 10 -18 -3 42.10 16.30 -10 -18 3 41.30 14.90 -10 18 2 78.99 29.00 10 18 -2 42.90 13.00 10 -18 -2 55.59 11.80 -10 -18 2 46.50 15.10 10 -18 -2 58.79 18.40 -10 -18 2 49.40 20.80 -10 -18 2 85.39 15.60 11 0 -9 -0.30 6.50 11 0 -8 473.15 30.50 11 0 -8 458.05 48.30 11 0 -7 -13.60 22.80 11 0 -7 -0.20 11.30 11 0 -6 312.97 25.90 11 0 -6 303.87 36.90 11 0 -5 3.80 17.70 11 0 -5 18.20 11.80 11 0 -4 5.90 11.90 11 0 -4 29.10 16.90 11 0 -3 26.10 12.70 11 0 -3 -1.10 14.50 11 0 -2 216.28 25.80 11 0 -1 9.60 14.10 11 0 -1 -3.80 12.00 11 0 -1 -0.90 3.50 11 0 0 93.39 11.80 11 0 0 94.09 16.10 11 0 0 138.69 20.30 -11 0 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8.40 11 1 1 11.40 9.30 -11 1 -1 12.20 6.40 11 1 1 25.30 16.10 -11 -1 -1 5.40 6.50 11 -1 1 24.60 17.10 11 -1 1 17.70 9.50 11 1 2 107.49 20.70 11 1 2 87.59 14.20 11 -1 2 69.89 14.40 11 -1 2 83.79 21.50 11 1 3 86.59 16.70 11 -1 3 98.89 17.90 -11 -1 -3 15.50 13.90 11 2 -9 5.20 5.90 11 -2 -9 9.00 8.40 11 -2 -9 14.70 5.40 11 -2 -9 42.60 13.10 11 2 -8 -9.60 26.80 11 2 -8 -22.20 10.70 11 -2 -8 24.00 13.10 11 -2 -8 5.40 23.20 11 2 -7 107.79 14.90 11 2 -7 79.59 26.80 11 -2 -7 101.79 16.50 11 -2 -7 68.39 24.50 11 2 -6 8.40 11.00 11 2 -6 -2.40 20.80 11 -2 -6 -1.00 11.70 11 -2 -6 -1.60 18.70 11 2 -5 36.80 12.20 11 2 -5 27.30 21.80 11 -2 -5 32.10 14.00 11 -2 -5 1.20 17.80 11 2 -4 -2.40 11.30 11 2 -4 1.40 17.40 11 -2 -4 9.10 15.90 11 -2 -4 -14.70 12.40 11 2 -3 268.47 32.10 11 2 -3 294.97 26.30 11 -2 -3 304.97 28.50 11 -2 -3 289.57 29.60 11 2 -2 8.40 13.10 11 2 -2 -10.10 15.90 11 -2 -2 20.60 14.00 11 2 -1 93.59 17.80 11 2 -1 166.68 27.40 11 2 -1 125.49 7.80 11 -2 -1 158.18 22.30 11 -2 -1 141.79 9.80 11 -2 -1 117.39 19.60 11 2 0 24.90 6.70 11 2 0 32.70 14.00 11 2 0 41.50 14.40 11 -2 0 49.00 12.70 11 -2 0 37.80 15.60 11 -2 0 41.70 8.30 -11 2 -1 84.29 10.30 11 2 1 101.99 11.50 11 2 1 100.79 18.30 11 2 1 101.59 15.90 11 -2 1 91.29 20.20 11 -2 1 87.19 12.40 -11 -2 -1 96.19 9.80 11 2 2 94.39 13.90 11 2 2 92.89 19.20 11 -2 2 72.69 14.70 11 -2 2 72.19 21.10 11 2 3 6.80 13.90 -11 2 -3 11.10 12.60 -11 -2 -3 5.10 13.40 11 -2 3 -18.70 14.30 11 3 -9 -2.60 5.50 11 -3 -9 4.40 8.90 11 -3 -9 -13.90 15.40 11 -3 -9 -4.00 5.30 11 3 -8 99.39 15.00 11 3 -8 94.89 33.00 11 -3 -8 120.79 17.00 11 -3 -8 113.69 30.60 11 3 -7 7.80 25.10 11 3 -7 -7.50 10.20 11 -3 -7 27.70 13.60 11 -3 -7 -10.00 19.90 11 3 -6 9.40 25.60 11 3 -6 21.60 12.00 11 -3 -6 25.70 14.30 11 -3 -6 27.90 20.30 11 3 -5 26.20 21.00 11 3 -5 14.40 11.10 11 -3 -5 25.90 18.50 11 -3 -5 26.30 13.30 11 3 -4 142.29 18.60 11 3 -4 164.18 27.80 11 -3 -4 176.68 26.20 11 -3 -4 138.59 20.40 11 3 -3 24.10 18.50 11 3 -3 54.79 13.90 11 -3 -3 48.10 17.60 11 -3 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11 4 -4 18.50 20.50 11 -4 -4 35.60 14.70 11 -4 -4 5.50 15.30 11 4 -3 70.79 14.50 11 -4 -3 64.89 17.10 11 -4 -3 104.59 19.30 11 4 -2 12.60 18.20 11 4 -2 -2.90 11.70 11 -4 -2 -11.10 14.60 11 -4 -2 4.90 13.90 11 4 -1 -2.00 12.20 11 4 -1 8.30 3.50 11 4 -1 10.20 17.00 11 -4 -1 8.80 11.60 11 -4 -1 13.00 4.60 11 -4 -1 27.30 16.40 11 -4 -1 -0.30 6.00 11 4 0 20.40 13.20 11 4 0 20.90 5.90 11 4 0 19.20 14.70 11 -4 0 14.80 6.90 11 -4 0 12.10 8.50 11 -4 0 37.70 15.40 11 4 1 74.19 15.90 11 4 1 49.60 15.90 11 4 1 53.29 9.60 -11 -4 -1 34.70 8.40 -11 -4 -1 59.69 7.20 11 -4 1 68.19 12.70 11 -4 1 81.09 20.10 11 4 2 216.58 28.70 11 4 2 153.68 16.00 11 4 2 120.09 14.20 11 -4 2 147.69 18.30 11 -4 2 127.39 24.80 11 5 -9 -0.80 5.80 11 -5 -9 -7.60 6.00 11 -5 -9 -7.20 14.50 11 -5 -9 9.00 11.20 11 5 -8 48.60 30.80 11 -5 -8 15.80 23.30 11 -5 -8 36.60 15.50 11 -5 -8 36.40 6.80 11 5 -7 -1.10 10.20 11 5 -7 41.70 27.90 11 -5 -7 8.30 14.80 11 -5 -7 -2.00 21.30 11 5 -6 -7.00 10.30 11 5 -6 24.60 25.80 11 -5 -6 13.40 13.90 11 -5 -6 11.80 18.80 11 5 -5 6.30 23.40 11 5 -5 4.90 10.40 11 -5 -5 -8.90 13.20 11 -5 -5 -2.40 17.10 11 5 -4 196.18 21.70 11 -5 -4 228.68 27.00 11 -5 -4 207.38 27.80 11 5 -3 64.79 14.20 11 -5 -3 80.09 17.10 11 -5 -3 94.29 19.90 11 5 -2 312.17 27.30 11 -5 -2 294.77 31.30 11 -5 -2 298.57 26.80 11 5 -1 135.89 19.60 11 5 -1 144.19 9.00 11 -5 -1 139.89 13.40 11 -5 -1 108.69 20.60 11 -5 -1 141.19 10.10 11 5 0 -4.30 15.00 11 5 0 14.80 5.80 11 5 0 7.40 12.80 11 -5 0 14.40 9.50 11 -5 0 9.10 6.70 11 -5 0 -2.80 15.10 11 5 1 76.79 16.00 11 5 1 88.69 18.40 11 5 1 59.59 9.60 11 -5 1 76.89 14.10 11 -5 1 60.29 22.20 -11 -5 -1 62.19 7.30 11 5 2 11.90 11.00 -11 5 -2 9.80 9.40 11 5 2 25.40 10.30 11 5 2 14.70 16.90 11 -5 2 14.60 14.10 -11 -5 -2 22.10 11.60 11 -5 2 -0.10 21.10 11 6 -8 114.39 8.20 11 -6 -8 91.19 18.90 11 -6 -8 68.89 28.90 11 -6 -8 88.89 11.50 11 6 -7 6.30 28.00 11 -6 -7 22.30 15.40 11 -6 -7 -3.40 20.40 11 6 -6 285.87 23.20 11 -6 -6 239.58 28.40 11 -6 -6 252.47 42.40 11 6 -5 111.09 16.00 11 -6 -5 115.19 24.50 11 -6 -5 117.49 19.20 11 6 -4 5.80 10.50 11 6 -4 -19.80 21.50 11 -6 -4 -1.40 14.10 11 -6 -4 15.40 15.10 11 6 -3 10.40 21.30 11 6 -3 15.30 12.40 11 -6 -3 -4.80 13.70 11 -6 -3 1.70 15.10 11 6 -2 28.50 13.20 11 6 -2 4.40 20.60 11 -6 -2 24.70 6.10 11 -6 -2 31.70 16.20 11 -6 -2 28.80 5.20 11 6 -1 16.50 13.10 11 6 -1 21.10 4.50 11 -6 -1 -0.90 15.30 11 -6 -1 17.70 5.30 11 -6 -1 18.50 8.50 11 6 0 4.70 5.50 11 6 0 -12.90 11.90 11 6 0 14.80 17.10 11 -6 0 -3.50 10.10 11 -6 0 10.90 16.20 11 -6 0 1.10 6.60 11 6 1 4.20 13.80 -11 6 -1 4.90 6.60 11 6 1 14.10 7.90 11 6 1 -11.00 14.80 11 -6 1 32.70 19.10 -11 -6 -1 -2.70 8.60 -11 -6 -1 -2.40 5.60 11 -6 1 -8.10 8.20 11 -6 1 13.00 12.20 -11 6 -2 10.80 9.20 11 6 2 28.60 12.60 11 6 2 -17.80 10.00 11 6 2 3.10 18.80 -11 -6 -2 9.50 12.30 11 -6 2 9.70 15.70 11 -6 2 12.50 21.40 -11 -6 -2 -2.10 7.50 11 7 -8 19.50 35.00 11 7 -8 50.29 6.00 11 -7 -8 44.30 6.40 11 -7 -8 49.30 17.90 11 -7 -8 27.90 11.70 11 -7 -8 51.19 26.90 11 7 -7 -29.40 29.80 11 -7 -7 -2.90 15.60 11 -7 -7 2.30 7.20 11 -7 -7 29.00 22.20 11 7 -6 149.69 17.60 11 -7 -6 206.88 37.00 11 -7 -6 152.08 21.80 11 7 -5 162.28 20.20 11 -7 -5 193.18 23.90 11 -7 -5 160.88 25.70 11 7 -4 28.40 11.50 11 7 -4 26.50 27.80 11 -7 -4 -11.00 14.50 11 -7 -4 17.40 16.10 11 7 -3 23.80 24.70 11 7 -3 68.09 14.30 11 -7 -3 51.29 17.80 11 -7 -3 36.20 15.40 11 7 -2 47.70 14.00 11 7 -2 18.00 22.30 11 -7 -2 59.99 19.40 11 -7 -2 63.09 7.40 11 -7 -2 51.19 8.40 11 7 -1 121.19 17.80 11 7 -1 149.99 10.20 11 -7 -1 163.28 11.40 11 -7 -1 138.49 16.50 11 -7 -1 130.09 22.50 -11 7 0 76.09 9.20 11 7 0 89.59 16.90 11 7 0 82.59 10.20 11 -7 0 97.99 12.40 11 -7 0 92.89 20.10 11 -7 0 73.69 13.70 -11 7 -1 4.70 7.00 11 7 1 43.90 18.20 11 7 1 1.10 15.00 11 7 1 7.70 8.10 11 -7 1 15.00 8.90 -11 -7 -1 32.90 6.60 11 -7 1 11.00 18.50 11 -7 1 18.10 13.80 -11 -7 -1 -1.30 9.50 11 7 2 11.80 9.90 -11 7 -2 -8.00 9.40 11 7 2 4.10 13.30 -11 -7 -2 17.10 8.60 11 -7 2 16.80 15.80 -11 -7 -2 10.80 13.10 11 8 -8 28.80 6.00 11 8 -8 14.20 50.19 11 -8 -8 63.19 19.20 11 -8 -8 35.20 24.60 11 -8 -8 14.70 6.20 11 -8 -8 9.80 11.90 11 8 -7 0.80 34.40 11 -8 -7 8.50 5.40 11 -8 -7 12.90 9.20 11 -8 -7 4.10 21.70 11 -8 -7 -3.70 16.50 11 8 -6 -4.00 31.40 11 -8 -6 6.10 16.10 11 -8 -6 -6.30 17.30 11 -8 -6 -1.30 6.40 11 8 -5 22.70 12.20 11 8 -5 28.40 33.40 11 -8 -5 11.00 16.40 11 -8 -5 21.60 16.70 11 8 -4 41.80 30.50 11 8 -4 -0.20 11.10 11 -8 -4 -18.00 14.60 11 -8 -4 9.60 14.90 11 8 -3 9.60 11.20 11 8 -3 -2.00 27.10 11 -8 -3 -3.00 16.10 11 -8 -3 3.30 5.30 11 8 -2 -10.70 25.00 11 8 -2 12.30 4.50 11 8 -2 16.60 12.10 11 -8 -2 10.10 8.20 11 -8 -2 -16.80 16.30 11 -8 -2 9.90 5.10 11 8 -1 196.08 23.80 11 8 -1 202.28 12.70 11 -8 -1 192.38 20.40 11 -8 -1 211.08 13.80 11 -8 -1 222.38 28.00 11 8 0 45.40 7.60 11 8 0 24.90 14.50 -11 -8 0 53.79 6.60 11 -8 0 44.80 13.30 11 -8 0 53.79 20.30 11 -8 0 50.89 8.60 11 8 1 14.70 19.60 -11 8 -1 4.50 7.20 11 8 1 29.30 15.80 11 8 1 10.90 8.20 11 -8 1 17.40 9.30 -11 -8 -1 6.20 10.90 11 -8 1 11.60 14.80 11 -8 1 22.40 20.80 -11 -8 -1 12.80 6.70 -11 8 -2 -5.90 9.70 11 8 2 20.80 10.60 11 8 2 10.10 15.50 11 -8 2 -14.60 10.80 -11 -8 -2 1.80 8.20 11 -8 2 -3.60 17.40 -11 -8 -2 10.70 14.40 11 9 -8 114.29 11.10 11 -9 -8 88.29 11.70 11 -9 -8 110.99 15.60 11 -9 -8 92.19 21.30 11 9 -7 -8.10 33.10 11 -9 -7 40.20 7.20 11 -9 -7 39.00 23.20 11 -9 -7 46.40 11.70 11 -9 -7 52.89 19.20 11 9 -6 12.00 35.10 11 -9 -6 -4.50 17.80 11 -9 -6 -12.80 16.40 11 -9 -6 7.60 8.70 11 -9 -6 12.10 6.00 11 9 -5 -2.80 32.80 11 -9 -5 21.60 16.50 11 -9 -5 25.50 7.60 11 -9 -5 18.40 6.30 11 9 -4 64.89 14.60 11 9 -4 -44.80 30.30 11 -9 -4 35.60 7.10 11 -9 -4 53.59 19.00 11 -9 -4 46.60 7.60 11 9 -3 11.20 12.20 11 9 -3 47.40 31.60 11 -9 -3 14.90 16.60 11 -9 -3 19.50 8.00 11 -9 -3 20.20 6.60 11 9 -2 1.60 28.10 11 9 -2 5.10 4.90 11 9 -2 -0.20 11.20 11 -9 -2 -16.00 15.30 11 -9 -2 15.30 9.10 11 -9 -2 6.20 5.50 11 9 -1 26.40 26.70 11 9 -1 0.20 12.30 11 9 -1 8.60 5.30 11 -9 -1 20.40 18.10 11 -9 -1 10.50 6.30 11 -9 -1 24.00 11.10 11 9 0 4.60 14.00 11 9 0 -15.30 27.50 11 9 0 5.60 6.70 -11 9 0 -3.70 5.90 11 -9 0 22.90 20.00 11 -9 0 -1.40 6.80 -11 -9 0 17.10 6.10 -11 9 -1 -3.10 7.50 11 9 1 5.60 14.50 11 9 1 -6.10 7.90 11 9 1 -9.60 21.80 11 -9 1 22.70 15.70 11 -9 1 30.60 21.30 -11 -9 -1 14.30 7.00 11 -9 1 -0.20 8.80 -11 -9 -1 4.60 11.50 11 10 -8 8.00 6.80 11 -10 -8 1.10 19.50 11 -10 -8 15.40 7.50 11 -10 -8 13.10 14.10 11 10 -7 36.70 42.20 11 -10 -7 42.70 8.00 11 -10 -7 39.40 12.70 11 -10 -7 70.69 20.20 -11 10 6 -28.90 37.00 11 10 -6 73.39 38.90 11 -10 -6 61.59 8.80 11 -10 -6 63.49 11.40 11 -10 -6 71.39 20.10 11 10 -5 41.90 38.70 -11 10 5 35.20 33.40 11 -10 -5 84.09 9.80 11 -10 -5 105.09 21.20 11 -10 -5 101.19 13.20 -11 10 4 11.60 31.50 11 10 -4 -37.20 30.90 11 -10 -4 31.20 7.90 11 -10 -4 17.70 17.60 11 -10 -4 39.80 8.70 -11 10 3 -1.40 30.60 11 10 -3 104.49 16.30 11 10 -3 21.10 33.60 11 -10 -3 71.89 20.50 11 -10 -3 76.69 10.60 11 -10 -3 80.89 11.30 11 10 -2 8.60 12.30 11 10 -2 5.00 5.50 11 10 -2 17.30 31.60 11 -10 -2 -1.70 10.00 11 -10 -2 -2.30 5.70 11 -10 -2 38.10 19.20 11 10 -1 334.07 18.80 11 10 -1 288.17 46.50 11 10 -1 362.16 29.10 11 -10 -1 326.97 26.20 11 -10 -1 366.86 37.20 11 -10 -1 349.07 19.90 -11 10 0 4.80 6.50 11 10 0 20.70 7.40 11 10 0 28.50 29.20 11 10 0 11.20 14.70 -11 -10 0 19.20 11.90 -11 -10 0 23.10 7.00 11 -10 0 39.90 20.40 11 -10 0 26.50 8.10 11 -10 0 32.80 14.40 -11 11 7 -5.20 40.80 11 11 -7 3.50 46.20 11 -11 -7 -4.10 7.60 11 -11 -7 14.20 12.40 11 -11 -7 6.30 19.20 -11 11 6 40.50 39.70 11 11 -6 31.60 39.90 11 -11 -6 10.30 8.00 11 -11 -6 5.20 10.00 -11 11 5 107.79 40.50 11 11 -5 40.90 37.30 11 -11 -5 103.59 14.30 11 -11 -5 137.79 16.00 -11 11 4 -4.90 31.70 11 11 -4 53.59 37.70 -11 -11 4 15.40 17.50 11 -11 -4 46.50 8.40 11 -11 -4 34.20 9.40 -11 11 3 18.20 31.30 11 11 -3 13.80 33.10 -11 -11 3 -2.10 16.70 11 -11 -3 12.10 9.80 11 -11 -3 10.80 7.10 11 11 -2 35.60 7.10 11 11 -2 1.30 26.00 11 -11 -2 41.60 19.30 -11 -11 2 22.30 17.30 11 -11 -2 32.10 12.10 11 -11 -2 31.80 7.70 11 11 -1 14.00 6.50 11 11 -1 -16.90 29.30 -11 -11 1 37.50 19.70 11 -11 -1 6.10 7.00 11 -11 -1 -3.10 18.00 -11 -11 1 6.30 6.80 11 -11 -1 1.60 12.90 -11 11 0 -6.30 6.90 11 11 0 -2.30 29.70 11 11 0 11.60 7.40 11 -11 0 98.49 24.30 11 -11 0 30.90 15.60 -11 -11 0 48.40 19.50 -11 -11 0 -15.10 10.40 11 -11 0 3.60 8.00 -11 -11 0 13.70 7.00 11 11 1 179.98 17.30 11 -11 1 204.48 19.10 -11 -11 -1 159.28 16.70 11 -11 1 183.58 23.00 -11 12 7 17.10 44.10 11 -12 -7 43.70 10.10 11 -12 -7 60.99 14.40 11 12 -6 120.49 48.60 -11 12 6 136.99 44.10 11 -12 -6 251.57 21.50 11 -12 -6 262.27 18.60 11 12 -5 51.19 44.00 11 -12 -5 147.09 16.80 -11 -12 5 174.68 24.50 11 -12 -5 126.69 16.20 -11 12 4 58.99 33.10 11 -12 -4 2.60 8.20 -11 -12 4 -2.40 16.60 11 -12 -4 9.60 9.80 -11 12 3 4.00 31.10 11 -12 -3 21.00 11.30 -11 -12 3 31.30 17.60 11 -12 -3 24.40 8.20 11 12 -2 108.79 12.90 -11 12 2 110.59 37.20 11 -12 -2 134.69 17.00 11 -12 -2 106.09 12.70 -11 -12 2 101.19 22.60 11 12 -1 13.20 7.20 -11 12 1 2.10 30.70 -11 -12 1 2.00 19.30 -11 -12 1 11.10 7.80 11 -12 -1 14.80 14.80 11 -12 -1 22.80 8.00 11 12 0 77.09 10.80 11 -12 0 83.89 11.80 -11 -12 0 82.29 10.10 11 -12 0 128.49 20.00 -11 -12 0 96.59 23.70 11 13 -6 10.10 46.20 -11 13 6 7.00 36.70 11 -13 -6 21.50 9.70 11 -13 -6 31.10 11.70 -11 -13 6 36.50 19.60 -11 13 5 86.49 36.30 -11 -13 5 165.78 25.10 11 -13 -5 158.08 18.60 11 -13 -5 146.79 18.70 -11 13 4 -4.40 31.90 11 -13 -4 -0.30 9.00 -11 -13 4 17.70 18.50 11 -13 -4 -15.00 10.70 -11 -13 3 208.28 27.70 11 -13 -3 153.78 17.90 11 -13 -3 183.08 16.20 -11 13 2 -28.70 30.50 11 13 -2 31.20 8.60 -11 -13 2 36.20 8.70 -11 -13 2 33.00 9.10 -11 -13 2 78.09 22.20 11 -13 -2 39.20 8.80 11 -13 -2 27.10 14.10 -11 13 1 44.10 37.90 11 13 -1 169.78 15.10 -11 -13 1 155.38 27.00 11 -13 -1 153.58 15.30 11 -13 -1 160.08 21.40 -11 -13 1 135.59 15.10 -11 13 0 -5.10 30.20 11 13 0 -4.70 8.40 -11 13 0 -4.90 8.60 11 -13 0 5.00 18.10 11 -13 0 4.70 9.00 -11 -13 0 -0.70 21.00 -11 -13 0 1.10 12.90 -11 -13 0 7.50 8.70 -11 14 6 33.00 39.90 -11 -14 6 55.99 21.80 -11 14 5 33.00 35.30 -11 -14 5 47.50 20.70 11 -14 -5 40.60 12.20 11 -14 -5 42.10 12.30 -11 14 4 -12.60 32.10 11 -14 -4 24.00 10.60 -11 -14 4 24.90 19.90 11 -14 -4 16.40 12.30 -11 14 3 63.79 31.30 11 -14 -3 49.70 10.40 11 -14 -3 81.79 15.30 -11 -14 3 80.29 23.20 -11 -14 3 76.89 9.60 11 14 -2 17.90 9.40 -11 14 2 -10.10 28.60 11 -14 -2 6.30 14.90 11 -14 -2 13.30 8.50 -11 -14 2 24.00 9.50 -11 -14 2 16.90 20.60 -11 14 1 -22.70 30.90 11 14 -1 19.80 9.10 -11 -14 1 7.50 10.00 11 -14 -1 -4.40 17.10 11 -14 -1 23.30 9.00 -11 -14 1 -12.00 20.20 -11 15 5 -12.70 32.70 -11 -15 4 188.48 16.50 11 -15 -4 190.88 19.90 11 -15 -4 152.18 19.10 -11 -15 4 188.68 29.10 -11 15 3 46.90 31.20 -11 -15 3 120.09 12.60 11 -15 -3 128.69 13.90 -11 -15 3 116.39 24.20 -11 -15 3 112.79 12.50 11 -15 -3 119.59 17.80 11 15 -2 110.29 13.50 -11 15 2 42.00 30.90 11 -15 -2 104.49 12.70 -11 -15 2 101.19 23.40 -11 -15 2 87.89 12.70 11 -15 -2 86.09 19.20 12 0 -8 224.58 26.40 12 0 -7 4.60 26.90 12 0 -7 0.00 14.00 12 0 -6 75.69 18.60 12 0 -6 50.99 25.00 12 0 -5 18.40 22.60 12 0 -5 19.30 15.10 12 0 -4 409.16 41.40 12 0 -4 431.96 34.30 12 0 -3 26.50 16.20 12 0 -3 11.40 18.00 12 0 -2 299.37 32.20 12 0 -2 304.07 32.00 12 0 -1 -20.00 15.20 12 0 -1 18.30 17.70 12 0 0 10.20 19.50 12 0 0 23.80 7.40 12 0 0 41.00 14.40 12 0 1 -0.10 10.20 12 1 -8 45.70 15.00 12 -1 -8 63.89 16.30 12 1 -7 242.28 39.50 12 1 -7 229.78 26.00 12 -1 -7 224.08 38.90 12 -1 -7 201.88 26.80 12 1 -6 204.88 34.30 12 1 -6 186.38 25.80 12 -1 -6 237.48 37.20 12 -1 -6 180.28 23.60 12 1 -5 183.28 31.40 12 1 -5 178.18 22.00 12 -1 -5 136.09 21.00 12 -1 -5 185.48 31.30 12 1 -4 20.20 15.60 12 1 -4 -4.10 20.00 12 -1 -4 3.40 18.60 12 -1 -4 -0.30 15.10 12 1 -3 39.80 20.80 12 1 -3 24.70 15.80 12 -1 -3 52.59 17.60 12 -1 -3 40.10 19.20 12 1 -2 173.88 26.40 12 1 -2 151.58 22.40 12 -1 -2 175.58 26.00 12 -1 -2 145.59 23.90 12 1 -1 205.68 31.00 12 1 -1 241.78 30.30 12 -1 -1 203.88 25.90 12 -1 -1 175.08 9.50 12 -1 -1 225.98 27.70 12 1 0 69.39 8.70 12 1 0 95.49 21.60 12 1 0 79.49 17.80 12 -1 0 66.79 9.00 12 -1 0 60.59 20.80 12 1 1 95.79 13.00 12 -1 1 89.59 13.40 -12 -1 -1 113.39 8.80 12 2 -8 173.38 24.10 12 -2 -8 207.98 27.10 12 2 -7 17.20 27.40 12 2 -7 0.80 14.20 12 -2 -7 29.90 16.30 12 -2 -7 -25.20 24.70 12 2 -6 31.40 26.30 12 2 -6 61.19 16.00 12 -2 -6 16.80 22.40 12 -2 -6 44.50 17.50 12 2 -5 22.20 24.40 12 2 -5 4.50 13.80 12 -2 -5 34.60 16.80 12 -2 -5 18.50 20.80 12 2 -4 247.28 36.00 12 2 -4 218.78 27.40 12 -2 -4 239.28 29.40 12 -2 -4 230.98 32.60 12 2 -3 2.70 14.10 12 2 -3 -4.70 19.60 12 -2 -3 9.90 17.80 12 -2 -3 9.90 16.60 12 2 -2 184.28 24.20 12 2 -2 173.28 29.70 12 -2 -2 182.28 26.70 12 -2 -2 214.68 26.60 12 2 -1 2.20 15.50 12 -2 -1 15.20 4.30 12 -2 -1 43.10 19.00 12 -2 -1 21.40 15.30 12 2 0 25.40 18.40 12 2 0 18.10 6.30 12 2 0 2.50 14.90 12 -2 0 9.90 8.00 12 -2 0 18.70 7.50 12 -2 0 -1.90 18.30 12 2 1 -2.80 9.50 12 2 1 -5.80 11.30 12 -2 1 -5.30 10.80 -12 -2 -1 5.20 4.80 12 3 -8 -16.80 13.80 12 -3 -8 18.80 17.00 12 3 -7 0.70 13.50 12 3 -7 28.50 29.30 12 -3 -7 4.70 24.70 12 -3 -7 -11.40 16.10 12 3 -6 348.47 44.30 12 3 -6 254.37 26.60 12 -3 -6 233.98 37.70 12 -3 -6 248.98 30.20 12 3 -5 14.60 13.70 12 3 -5 46.00 26.30 12 -3 -5 48.90 22.10 12 -3 -5 54.09 18.90 12 3 -4 48.60 24.90 12 3 -4 5.40 14.00 12 -3 -4 19.20 17.30 12 -3 -4 0.50 17.50 12 3 -3 28.30 21.60 12 3 -3 -9.90 14.30 12 -3 -3 23.10 17.80 12 -3 -3 22.60 16.10 12 3 -2 42.70 20.90 12 3 -2 21.90 14.90 12 -3 -2 27.60 18.80 12 -3 -2 24.70 16.50 12 3 -1 35.00 22.40 12 3 -1 23.00 16.30 12 -3 -1 19.60 5.40 12 -3 -1 30.20 19.60 12 -3 -1 40.00 17.60 12 -3 -1 31.90 4.70 12 3 0 88.89 8.90 12 3 0 96.69 19.30 12 3 0 72.99 20.40 12 -3 0 78.59 9.60 12 -3 0 74.89 10.50 12 -3 0 47.50 20.20 12 3 1 4.30 12.20 12 3 1 1.00 9.40 -12 3 -1 3.90 5.60 12 -3 1 2.60 12.10 -12 -3 -1 -3.00 4.80 12 4 -7 40.00 14.40 12 4 -7 44.00 32.70 12 -4 -7 53.19 18.80 12 -4 -7 10.60 26.10 12 4 -6 -4.70 27.70 12 4 -6 19.90 13.70 12 -4 -6 12.70 17.20 12 -4 -6 13.30 20.80 12 4 -5 26.00 26.40 12 4 -5 15.20 13.90 12 -4 -5 38.30 18.30 12 -4 -5 23.80 22.10 12 4 -4 50.39 27.10 12 4 -4 34.60 15.10 12 -4 -4 56.69 18.20 12 -4 -4 50.59 20.30 12 4 -3 114.29 19.40 12 4 -3 124.29 29.30 12 -4 -3 96.39 20.20 12 -4 -3 119.19 23.80 12 4 -2 197.18 29.70 12 4 -2 114.59 19.20 12 -4 -2 133.99 22.10 12 -4 -2 158.68 25.80 12 4 -1 26.50 3.80 12 4 -1 33.40 19.60 12 4 -1 38.40 16.70 12 -4 -1 36.40 20.60 12 -4 -1 33.60 5.00 12 -4 -1 15.30 6.10 12 4 0 46.20 20.70 12 4 0 55.69 7.50 12 4 0 66.69 20.90 12 -4 0 47.90 8.40 12 -4 0 35.30 10.50 12 -4 0 48.10 22.90 -12 4 -1 6.50 6.50 -12 -4 -1 19.20 5.50 12 5 -7 5.30 34.70 12 5 -7 31.80 14.60 12 -5 -7 26.60 23.80 12 -5 -7 31.30 18.30 12 5 -6 210.38 25.00 12 5 -6 187.28 39.50 12 -5 -6 210.28 27.20 12 -5 -6 213.08 34.30 12 5 -5 38.90 14.20 12 5 -5 34.20 29.20 12 -5 -5 38.10 18.30 12 -5 -5 26.00 21.40 12 5 -4 33.20 14.60 12 5 -4 43.90 26.40 12 -5 -4 37.80 20.40 12 -5 -4 36.70 17.20 12 5 -3 -2.00 13.90 12 5 -3 31.50 24.30 12 -5 -3 17.40 17.90 12 -5 -3 -19.30 15.60 12 5 -2 4.10 14.70 12 5 -2 21.40 22.20 12 -5 -2 4.50 20.70 12 5 -1 -1.10 15.50 12 5 -1 29.80 21.50 12 5 -1 24.30 4.10 12 -5 -1 13.90 20.40 12 -5 -1 11.30 7.30 12 -5 -1 26.00 5.30 12 5 0 -2.30 5.90 12 -5 0 12.20 10.20 12 -5 0 -4.10 7.00 12 6 -7 -28.00 34.50 12 6 -7 15.20 13.90 12 -6 -7 32.20 26.10 12 -6 -7 24.50 20.50 12 6 -6 -10.40 13.20 12 6 -6 83.69 34.40 12 -6 -6 12.30 19.00 12 -6 -6 -13.40 20.50 12 6 -5 28.70 30.80 12 6 -5 22.40 14.70 12 -6 -5 -2.50 17.60 12 -6 -5 1.90 19.80 12 6 -4 328.97 29.00 12 -6 -4 325.57 34.80 12 -6 -4 332.67 34.70 12 6 -3 42.50 16.40 12 6 -3 34.70 27.10 12 -6 -3 30.10 18.20 12 -6 -3 46.00 18.00 12 6 -2 139.79 21.00 12 -6 -2 189.98 28.20 12 6 -1 2.30 4.10 12 6 -1 -2.00 21.80 12 6 -1 0.60 16.00 12 -6 -1 4.90 19.90 12 -6 -1 -0.30 7.80 12 -6 -1 3.30 5.20 12 6 0 6.90 6.40 12 6 0 0.60 19.80 12 -6 0 -9.40 10.90 12 -6 0 -4.70 7.20 12 7 -7 -32.60 34.90 12 -7 -7 43.40 28.00 12 -7 -7 44.90 21.30 12 7 -6 -0.80 34.90 12 7 -6 33.50 14.40 12 -7 -6 27.10 19.00 12 -7 -6 52.79 23.60 12 7 -5 -34.20 30.40 12 7 -5 28.40 14.70 12 -7 -5 -12.10 17.80 12 -7 -5 36.90 20.90 12 7 -4 11.60 14.00 12 7 -4 16.00 30.60 12 -7 -4 11.90 19.20 12 -7 -4 42.40 18.80 12 7 -3 -10.30 27.00 12 7 -3 3.10 14.80 12 -7 -3 2.90 18.30 12 7 -2 54.89 16.70 12 7 -2 -3.40 25.80 12 -7 -2 104.99 23.90 12 -7 -2 58.89 7.90 12 -7 -2 46.10 6.70 12 7 -1 161.28 23.30 12 7 -1 213.68 12.50 12 -7 -1 231.88 14.10 12 -7 -1 186.18 18.40 12 -7 -1 201.38 29.10 12 7 0 26.60 7.20 12 -7 0 25.30 8.20 12 -7 0 22.00 12.70 12 -8 -7 -14.60 27.40 12 8 -6 3.40 34.00 12 -8 -6 17.50 21.40 12 -8 -6 48.20 21.20 12 8 -5 15.40 14.00 12 8 -5 -3.50 32.80 12 -8 -5 -21.20 18.50 12 -8 -5 -2.20 17.90 12 8 -4 62.99 16.20 12 8 -4 38.20 31.70 12 -8 -4 55.59 21.20 12 8 -3 39.50 15.90 12 8 -3 -11.30 29.80 12 -8 -3 68.69 22.10 12 8 -2 22.60 15.30 12 8 -2 -11.90 27.90 12 -8 -2 20.80 8.30 12 -8 -2 34.70 6.20 12 -8 -2 21.00 22.00 12 8 -1 16.20 18.50 12 8 -1 -31.90 24.50 12 8 -1 15.80 5.30 12 -8 -1 4.50 6.20 12 -8 -1 8.30 11.00 12 8 0 34.00 24.50 12 9 -6 18.70 38.90 12 -9 -6 47.90 21.20 12 -9 -6 53.49 26.40 12 9 -5 -10.90 33.50 12 -9 -5 31.40 21.00 12 9 -4 19.10 35.80 12 9 -4 13.00 14.40 12 -9 -4 5.30 20.70 12 9 -3 15.60 34.80 12 9 -3 -15.00 13.90 12 -9 -3 -0.30 6.50 12 -9 -3 -1.70 6.20 12 -9 -3 0.60 21.60 12 9 -2 119.29 20.60 12 -9 -2 143.19 17.40 12 -9 -2 166.58 12.60 12 -9 -2 148.39 28.50 12 9 -1 41.50 28.40 12 9 -1 34.10 6.90 12 -9 -1 34.80 7.70 12 -9 -1 29.30 12.80 12 10 -6 20.70 40.90 12 -10 -6 -10.50 21.10 12 10 -5 97.19 45.20 12 -10 -5 179.78 27.60 12 10 -4 -49.20 35.50 12 -10 -4 28.70 21.40 12 -10 -4 1.50 6.80 12 10 -3 -18.20 35.80 12 10 -3 76.49 17.90 12 -10 -3 74.79 8.90 12 -10 -3 75.59 25.40 12 10 -2 22.90 35.60 12 10 -2 11.20 16.80 12 -10 -2 80.29 41.90 12 -10 -2 16.70 7.30 12 10 -1 -20.80 32.60 12 10 -1 -0.40 6.30 12 -10 -1 0.50 13.40 12 -10 -1 8.80 7.40 12 11 -5 -1.30 42.90 12 -11 -5 3.60 7.90 12 -11 -5 -19.30 21.30 12 -11 -5 6.10 8.70 12 11 -4 -36.10 39.80 12 -11 -4 14.20 9.50 12 -11 -4 20.70 8.40 12 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312.27 44.90 13 -3 -4 233.48 37.30 13 -3 -4 200.68 29.10 13 3 -3 -11.10 24.40 13 3 -3 2.30 18.40 13 -3 -3 13.70 22.90 13 -3 -3 -3.80 20.20 13 4 -5 39.80 32.20 13 -4 -5 53.99 25.60 13 4 -4 73.09 20.50 13 4 -4 74.09 32.60 13 -4 -4 60.69 25.50 13 -4 -4 45.00 24.90 13 4 -3 -24.10 18.40 13 4 -3 3.20 26.00 13 -4 -3 48.60 32.70 13 -4 -3 0.70 20.30 13 5 -4 6.50 17.40 13 5 -4 5.60 29.30 13 -5 -4 7.90 23.50 13 -5 -4 5.90 21.90 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 16491 #============================================================================== _publ_requested_journal '??????' _publ_contact_author ; Prof. Dr.Christian M\"uller Freie Universit\"at Berlin Institut f\"ur Chemie und Biochemie Anorganische Chemie Fabeckstr. 34-36 14195 Berlin Germany ; _publ_contact_letter ; ; _publ_requested_coeditor_name ? _publ_contact_author_phone '+49/(0)3083854004' _publ_contact_author_fax '+49/(0)3083852440' _publ_contact_author_email c.mueller@fu-berlin.de loop_ _publ_author_name _publ_author_address 'M\"uller, Christian' ; Freie Universit\"at Berlin Institut f\"ur Chemie und Biochemie Anorganische Chemie Fabeckstr. 34-36 14195 Berlin Germany ; 'Rigo, Massimo' ; Freie Universit\"at Berlin Institut f\"ur Chemie und Biochemie Anorganische Chemie Fabeckstr. 34-36 14195 Berlin Germany ; 'Kleoff, Merlin' ; Freie Universit\"at Berlin Institut f\"ur Chemie und Biochemie Anorganische Chemie Fabeckstr. 34-36 14195 Berlin Germany ; 'Weber, Manuela' ; Freie Universit\"at Berlin Institut f\"ur Chemie und Biochemie Anorganische Chemie Fabeckstr. 34-36 14195 Berlin Germany ; 'Wiecko, Jelena' ; Freie Universit\"at Berlin Institut f\"ur Chemie und Biochemie Anorganische Chemie Fabeckstr. 34-36 14195 Berlin Germany ; _publ_section_title ; ... see the published paper. ; _publ_section_abstract ; ... and following paragraphs: see the published paper. ; _publ_section_experimental ; ; _publ_section_comment ; ; _publ_section_references ; ; _publ_section_figure_captions ; ; #END====================================================