data_shelxl _audit_creation_method SHELXL-2013 _chemical_name_systematic ; 'selenium dicyanide difluoride propionitrile-solvate' ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C8 H10 F2 N4 Se' _chemical_formula_weight 279.16 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Se' 'Se' -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_H-M_alt 'I 2/a' _space_group_name_Hall '-I 2ya' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 12.652(3) _cell_length_b 7.3448(18) _cell_length_c 12.726(3) _cell_angle_alpha 90 _cell_angle_beta 97.547(4) _cell_angle_gamma 90 _cell_volume 1172.3(5) _cell_formula_units_Z 4 _cell_measurement_temperature 130(2) _cell_measurement_reflns_used 929 _cell_measurement_theta_min 6.419 _cell_measurement_theta_max 61.088 _exptl_crystal_description 'prism' _exptl_crystal_colour 'colourless' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.582 _exptl_crystal_F_000 552 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.33 _exptl_crystal_size_min 0.35 _exptl_absorpt_coefficient_mu 3.204 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6542 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_process_details 'SADABS-2008/1 (Bruker-AXS)' _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'sealed tube' _diffrn_measurement_device_type 'Bruker AXS Smart CCD' _diffrn_measurement_method 'omega scan' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 5316 _diffrn_reflns_av_unetI/netI 0.0178 _diffrn_reflns_av_R_equivalents 0.0173 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 3.209 _diffrn_reflns_theta_max 30.544 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.990 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.990 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.990 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 1773 _reflns_number_gt 1639 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Smart (Bruker AXS)' _computing_cell_refinement 'Saint (Bruker AXS)' _computing_data_reduction 'Saint (Bruker AXS)' _computing_structure_solution 'SHELXS-2013 (Sheldrick, 2013)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics 'Ortep3v2 for Windows' _computing_publication_material 'publCIF (IUCR)' _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details ; w=1/[\s^2^(Fo^2^)+(0.0271P)^2^+0.1542P] where P=(Fo^2^+2Fc^2^)/3 ; _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens difmap _refine_ls_hydrogen_treatment refall _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 1773 _refine_ls_number_parameters 114 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0198 _refine_ls_R_factor_gt 0.0171 _refine_ls_wR_factor_ref 0.0435 _refine_ls_wR_factor_gt 0.0423 _refine_ls_goodness_of_fit_ref 1.068 _refine_ls_restrained_S_all 1.068 _refine_ls_shift/su_max 0.058 _refine_ls_shift/su_mean 0.006 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Se1 Se 0.7500 0.62593(2) 0.5000 0.01803(5) Uani 1 2 d S T P . . F1 F 0.66844(6) 0.59681(11) 0.37056(6) 0.02970(16) Uani 1 1 d . . . . . C4 C 0.46359(10) 1.00584(17) 0.68448(11) 0.0222(2) Uani 1 1 d . . . . . C1 C 0.65957(9) 0.44861(16) 0.54847(9) 0.0218(2) Uani 1 1 d . . . . . C3 C 0.54134(9) 0.90430(15) 0.63213(10) 0.0220(2) Uani 1 1 d . . . . . N3 N 0.60066(9) 0.82252(16) 0.59081(10) 0.0316(2) Uani 1 1 d . . . . . N1 N 0.60555(10) 0.34134(17) 0.57848(10) 0.0345(3) Uani 1 1 d . . . . . C5 C 0.35092(10) 0.9296(2) 0.65884(13) 0.0288(3) Uani 1 1 d . . . . . H2 H 0.4675(15) 1.128(3) 0.6639(16) 0.045(6) Uani 1 1 d . . . . . H1 H 0.4849(11) 0.999(2) 0.7554(13) 0.025(4) Uani 1 1 d . . . . . H3 H 0.3477(11) 0.803(3) 0.6783(13) 0.036(5) Uani 1 1 d . . . . . H5 H 0.3027(13) 1.003(3) 0.6921(13) 0.043(5) Uani 1 1 d . . . . . H4 H 0.3322(13) 0.931(3) 0.5891(18) 0.049(5) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Se1 0.01575(8) 0.01837(8) 0.02059(8) 0.000 0.00468(5) 0.000 F1 0.0264(3) 0.0383(4) 0.0232(4) 0.0037(3) -0.0012(3) 0.0040(3) C4 0.0209(5) 0.0215(5) 0.0249(6) -0.0018(4) 0.0057(4) 0.0016(4) C1 0.0216(5) 0.0229(5) 0.0216(5) -0.0029(4) 0.0057(4) -0.0018(4) C3 0.0202(5) 0.0212(5) 0.0249(5) 0.0003(4) 0.0034(4) -0.0011(4) N3 0.0255(5) 0.0308(5) 0.0400(6) -0.0054(5) 0.0101(4) 0.0019(4) N1 0.0363(6) 0.0333(6) 0.0365(6) -0.0037(4) 0.0139(5) -0.0097(4) C5 0.0189(6) 0.0370(7) 0.0305(7) -0.0005(6) 0.0032(5) 0.0020(5) H2 0.027(11) 0.066(16) 0.047(14) -0.018(10) 0.024(10) 0.016(9) H1 0.015(8) 0.031(10) 0.032(10) -0.001(8) 0.011(7) 0.005(7) H3 0.006(8) 0.054(14) 0.049(13) 0.015(10) 0.013(8) 0.001(8) H5 0.019(9) 0.063(14) 0.049(12) -0.011(10) 0.011(8) -0.001(10) H4 0.015(10) 0.077(15) 0.051(14) -0.011(12) -0.005(10) -0.001(10) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Se1 F1 1.8378(8) 2_656 ? Se1 F1 1.8378(8) . ? Se1 C1 1.8897(12) 2_656 ? Se1 C1 1.8897(12) . ? Se1 N3 2.7502(12) . ? C4 C3 1.4628(17) . ? C4 C5 1.5263(18) . ? C1 N1 1.1412(17) . ? C3 N3 1.1420(17) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F1 Se1 F1 166.64(5) 2_656 . ? F1 Se1 C1 85.39(4) 2_656 2_656 ? F1 Se1 C1 85.41(4) . 2_656 ? F1 Se1 C1 85.41(4) 2_656 . ? F1 Se1 C1 85.39(4) . . ? C1 Se1 C1 92.87(7) 2_656 . ? F1 Se1 N3 91.16(4) 2_656 . ? F1 Se1 N3 95.85(4) . . ? C1 Se1 N3 167.91(4) 2_656 . ? C1 Se1 N3 75.28(5) . . ? C3 C4 C5 112.38(11) . . ? N1 C1 Se1 179.43(12) . . ? N3 C3 C4 178.72(13) . . ? C3 N3 Se1 177.32(10) . . ? _refine_diff_density_max 0.550 _refine_diff_density_min -0.178 _refine_diff_density_rms 0.059 _shelxl_version_number 2013-2 _shelx_res_file ; TITL sf259a in Ia CELL 0.71073 12.6518 7.3448 12.7258 90.000 97.547 90.000 ZERR 4.00 0.0030 0.0018 0.0030 0.000 0.004 0.000 LATT 2 SYMM 1/2 - X, Y, - Z SFAC C H N F SE UNIT 32 40 16 8 4 MERG 2 FMAP 2 PLAN 20 BIND SE1 N3 ACTA BOND L.S. 5 WGHT 0.027100 0.154200 FVAR 0.13083 SE1 5 0.750000 0.625927 0.500000 10.50000 0.01575 0.01837 = 0.02059 0.00000 0.00468 0.00000 F1 4 0.668437 0.596811 0.370556 11.00000 0.02638 0.03828 = 0.02324 0.00367 -0.00124 0.00401 C4 1 0.463591 1.005835 0.684483 11.00000 0.02094 0.02149 = 0.02485 -0.00176 0.00571 0.00155 C1 1 0.659566 0.448614 0.548474 11.00000 0.02163 0.02291 = 0.02163 -0.00293 0.00571 -0.00183 C3 1 0.541343 0.904299 0.632130 11.00000 0.02017 0.02123 = 0.02485 0.00032 0.00338 -0.00111 N3 3 0.600661 0.822516 0.590812 11.00000 0.02549 0.03081 = 0.04000 -0.00540 0.01010 0.00190 N1 3 0.605551 0.341337 0.578483 11.00000 0.03628 0.03334 = 0.03646 -0.00375 0.01387 -0.00974 C5 1 0.350915 0.929636 0.658840 11.00000 0.01885 0.03704 = 0.03052 -0.00051 0.00319 0.00195 H2 2 0.467457 1.128172 0.663901 11.00000 0.02681 0.06578 = 0.04685 -0.01779 0.02440 0.01613 H1 2 0.484853 0.999376 0.755382 11.00000 0.01514 0.03078 = 0.03223 -0.00101 0.01079 0.00526 H3 2 0.347689 0.802631 0.678273 11.00000 0.00620 0.05414 = 0.04904 0.01480 0.01270 0.00071 H5 2 0.302721 1.003469 0.692053 11.00000 0.01942 0.06278 = 0.04926 -0.01098 0.01058 -0.00114 H4 2 0.332227 0.930699 0.589060 11.00000 0.01496 0.07743 = 0.05093 -0.01115 -0.00511 -0.00050 HKLF 4 REM sf259a in Ia REM R1 = 0.0171 for 1639 Fo > 4sig(Fo) and 0.0198 for all 1773 data REM 114 parameters refined using 0 restraints END WGHT 0.0275 0.1512 REM Highest difference peak 0.550, deepest hole -0.178, 1-sigma level 0.059 Q1 1 0.7391 0.5339 0.5076 11.00000 0.05 0.55 Q2 1 0.4112 0.9692 0.6711 11.00000 0.05 0.33 Q3 1 0.6637 0.3722 0.5466 11.00000 0.05 0.33 Q4 1 0.6389 0.4456 0.5869 11.00000 0.05 0.30 Q5 1 0.7500 0.7434 0.5000 10.50000 0.05 0.29 Q6 1 0.5787 0.9087 0.6020 11.00000 0.05 0.28 Q7 1 0.5458 0.8627 0.5843 11.00000 0.05 0.27 Q8 1 0.5582 0.8125 0.6291 11.00000 0.05 0.27 Q9 1 0.6273 0.4164 0.5298 11.00000 0.05 0.27 Q10 1 0.7600 0.6394 0.5666 11.00000 0.05 0.27 Q11 1 0.8013 0.6359 0.5280 11.00000 0.05 0.26 Q12 1 0.6652 0.4668 0.5182 11.00000 0.05 0.23 Q13 1 0.4966 0.9478 0.6606 11.00000 0.05 0.23 Q14 1 0.5983 0.8088 0.5638 11.00000 0.05 0.23 Q15 1 0.6940 0.4697 0.5622 11.00000 0.05 0.23 Q16 1 0.2596 0.8803 0.5172 11.00000 0.05 0.21 Q17 1 0.6779 0.5247 0.3621 11.00000 0.05 0.20 Q18 1 0.6211 0.7981 0.6033 11.00000 0.05 0.19 Q19 1 0.6576 0.5888 0.3415 11.00000 0.05 0.17 Q20 1 0.4605 1.0526 0.6718 11.00000 0.05 0.17 ; _shelx_res_checksum 49098 _shelx_hkl_file ; 0 0 2 357.79 6.46 0 0 -2 356.06 6.22 0 0 -2 356.59 6.32 0 0 -4 21.14 0.45 0 0 4 20.72 0.42 0 0 -4 20.92 0.42 0 0 -6 135.20 2.45 0 0 -6 128.68 2.35 0 0 6 134.18 2.40 0 0 -8 97.84 1.89 0 0 8 97.78 1.81 0 0 -8 98.93 1.79 0 0 -10 43.12 0.89 0 0 -10 43.16 0.98 0 0 10 43.03 0.86 0 0 -12 33.92 0.76 0 0 -12 35.06 0.88 0 0 -14 33.73 0.93 0 1 -1 176.39 3.27 0 1 1 185.53 3.26 0 -1 1 181.74 3.16 0 -1 -1 180.03 3.16 0 1 3 500.57 8.69 0 1 -3 481.96 8.44 0 1 -3 480.96 8.63 0 -1 3 492.17 9.05 0 -1 -3 491.82 8.45 0 1 -5 14.68 0.34 0 1 5 13.65 0.35 0 1 -5 13.65 0.36 0 -1 5 13.13 0.27 0 -1 -5 13.61 0.30 0 1 -7 42.05 0.89 0 1 7 41.46 0.85 0 1 -7 42.27 0.84 0 -1 7 40.19 0.78 0 -1 -7 41.70 0.88 0 -1 -7 42.64 0.81 0 1 9 59.80 1.17 0 1 -9 58.98 1.15 0 1 -9 57.49 1.23 0 -1 -9 58.90 1.22 0 -1 -9 58.27 1.12 0 1 -11 2.54 0.26 0 1 11 2.77 0.21 0 1 -11 2.82 0.22 0 -1 -11 2.84 0.20 0 1 -13 10.94 0.49 0 1 -13 12.19 0.44 0 1 -15 15.98 0.63 0 1 -17 7.46 0.53 0 2 0 132.04 2.40 0 -2 0 129.38 2.32 0 2 2 21.80 0.51 0 2 -2 21.45 0.48 0 2 -2 22.52 0.46 0 -2 -2 22.78 0.45 0 2 -4 1.43 0.14 0 2 4 1.36 0.16 0 2 -4 1.29 0.10 0 -2 -4 1.44 0.11 0 2 6 34.08 0.77 0 2 -6 34.70 0.77 0 2 -6 35.73 0.75 0 -2 -6 35.15 0.69 0 2 8 0.47 0.16 0 2 -8 0.45 0.15 0 2 -8 0.41 0.15 0 -2 -8 0.36 0.11 0 2 -10 7.17 0.33 0 2 10 7.08 0.34 0 2 -10 7.40 0.39 0 -2 -10 7.07 0.27 0 2 -12 3.26 0.31 0 2 12 3.52 0.29 0 2 -12 3.49 0.27 0 2 -14 0.12 0.27 0 2 -14 0.59 0.22 0 2 -16 1.88 0.41 0 3 -1 97.26 1.80 0 3 1 95.20 1.82 0 -3 -1 97.04 1.74 0 -3 1 92.95 1.75 0 3 -3 24.06 0.53 0 3 3 24.39 0.61 0 3 -3 24.34 0.56 0 -3 -3 23.72 0.52 0 3 5 100.49 1.96 0 3 -5 101.16 1.89 0 3 -5 100.55 1.84 0 -3 -5 99.25 1.82 0 3 -7 43.96 0.98 0 3 7 44.66 1.00 0 3 -7 43.39 0.95 0 -3 -7 45.55 0.88 0 3 -9 24.70 0.68 0 3 -9 22.38 0.62 0 3 9 23.54 0.66 0 -3 -9 22.51 0.54 0 3 11 37.67 0.91 0 3 -11 35.82 0.86 0 3 -11 36.60 0.94 0 3 13 14.17 0.54 0 3 -13 14.86 0.53 0 3 -13 14.59 0.59 0 3 -15 12.28 0.59 0 3 -17 6.80 0.54 0 4 0 280.26 5.11 0 -4 0 282.13 4.95 0 4 2 192.67 3.55 0 4 -2 189.86 3.50 0 -4 -2 189.02 3.40 0 -4 2 190.84 3.42 0 4 4 17.19 0.55 0 4 -4 17.00 0.49 0 4 -4 16.38 0.44 0 -4 -4 17.27 0.44 0 4 -6 50.74 1.11 0 4 6 51.96 1.18 0 4 -6 52.32 1.02 0 -4 -6 52.72 1.04 0 4 -8 127.28 2.50 0 4 8 128.35 2.53 0 4 -8 131.24 2.45 0 -4 -8 126.34 2.34 0 4 -10 32.06 0.82 0 4 10 31.75 0.87 0 4 -10 33.20 0.88 0 4 -12 23.18 0.68 0 4 -12 21.57 0.74 0 4 12 20.38 0.69 0 4 -14 36.24 0.96 0 4 -14 36.41 1.04 0 4 14 36.40 0.98 0 4 -16 11.55 0.66 0 5 -1 76.44 1.59 0 5 1 76.36 1.61 0 -5 1 80.14 1.55 0 -5 -1 80.29 1.54 0 5 3 19.35 0.63 0 5 -3 19.33 0.57 0 5 -3 18.73 0.54 0 -5 -3 19.01 0.50 0 5 -5 30.29 0.71 0 5 5 29.86 0.83 0 5 -5 29.57 0.76 0 -5 -5 30.99 0.70 0 5 -7 19.62 0.61 0 5 7 20.39 0.67 0 -5 -7 19.51 0.52 0 5 9 26.13 0.80 0 5 -9 25.82 0.75 0 5 -9 25.72 0.75 0 -5 -9 25.19 0.64 0 5 11 21.10 0.73 0 5 -11 20.80 0.67 0 5 -11 21.40 0.72 0 5 -13 3.36 0.43 0 5 -13 2.85 0.36 0 5 13 2.26 0.37 0 5 -15 7.50 0.50 0 5 -15 6.34 0.52 0 6 0 0.66 0.25 0 -6 0 0.31 0.19 0 6 -2 0.35 0.22 0 6 -2 0.76 0.23 0 6 2 0.90 0.26 0 -6 -2 0.59 0.20 0 6 -4 5.88 0.38 0 6 -4 6.47 0.36 0 6 4 6.15 0.43 0 -6 -4 5.75 0.32 0 6 6 4.94 0.40 0 6 -6 4.98 0.38 0 -6 -6 5.23 0.31 0 6 8 11.21 0.56 0 6 -8 11.00 0.51 0 -6 -8 11.50 0.42 0 6 -10 8.74 0.52 0 6 10 7.98 0.51 0 6 -10 8.24 0.47 0 6 -12 6.15 0.51 0 6 -12 5.96 0.47 0 6 12 5.91 0.47 0 6 -14 0.40 0.34 0 6 -14 0.59 0.40 0 6 14 0.46 0.34 0 7 -1 24.63 0.75 0 7 1 24.36 0.76 0 -7 -1 26.27 0.72 0 7 -3 22.10 0.68 0 7 3 22.50 0.75 0 7 -3 22.04 0.71 0 -7 -3 23.30 0.66 0 7 -5 9.72 0.52 0 7 5 9.28 0.53 0 -7 -5 10.23 0.44 0 7 -7 19.90 0.72 0 7 7 21.09 0.77 0 -7 -7 21.57 0.64 0 7 9 14.58 0.70 0 7 -9 15.52 0.64 0 7 -11 7.97 0.56 0 7 -11 8.29 0.55 0 7 11 7.07 0.54 0 7 13 14.58 0.73 0 7 -13 13.69 0.68 0 7 -13 13.59 0.71 0 8 0 20.50 0.72 0 8 0 18.88 0.68 0 8 2 16.96 0.69 0 8 -2 16.53 0.65 0 8 -2 16.90 0.63 0 -8 -2 16.35 0.58 0 8 -4 31.93 0.96 0 8 4 31.94 1.01 0 -8 -4 35.07 0.90 0 8 6 35.30 1.08 0 8 -6 34.87 1.03 0 -8 -6 34.60 0.91 0 8 8 18.11 0.77 0 8 -8 18.16 0.74 0 8 -10 19.19 0.80 0 8 -10 20.23 0.79 0 8 10 19.36 0.81 0 9 -1 4.02 0.46 0 9 1 4.20 0.44 0 9 1 5.18 0.47 0 9 -1 4.05 0.44 0 9 -3 7.80 0.56 0 -9 -3 7.86 0.49 0 9 5 4.55 0.51 0 9 -5 4.68 0.50 0 -9 -5 4.53 0.42 0 9 7 10.15 0.65 0 9 -7 10.92 0.66 0 9 -9 8.20 0.64 0 9 9 9.64 0.64 0 10 0 0.41 0.38 0 10 0 0.58 0.38 0 10 2 1.53 0.41 0 10 -2 2.16 0.45 0 10 2 2.73 0.48 0 10 4 2.43 0.47 0 10 -4 1.96 0.44 0 10 4 2.29 0.42 1 0 -15 0.09 0.29 1 0 -13 0.09 0.21 1 0 -11 0.11 0.18 1 0 -11 -0.11 0.13 1 0 -9 0.04 0.15 1 0 -9 0.17 0.11 -1 0 9 0.03 0.10 1 0 -7 -0.02 0.08 -1 0 7 0.01 0.08 1 0 -7 0.01 0.10 -1 0 5 -0.09 0.05 1 0 -5 -0.02 0.07 1 0 -5 -0.03 0.05 -1 0 3 0.02 0.04 1 0 -3 0.03 0.05 1 0 -3 0.02 0.04 -1 0 1 -0.09 0.03 1 0 -1 0.02 0.03 -1 0 -1 -0.01 0.04 -1 0 -1 -0.01 0.04 -1 0 -1 -0.01 0.04 -1 0 -3 -0.09 0.06 -1 0 -3 -0.14 0.05 -1 0 -5 0.06 0.08 -1 0 -5 0.01 0.07 1 0 5 -0.05 0.07 -1 0 -7 -0.03 0.11 -1 0 -7 -0.01 0.09 1 0 7 -0.11 0.08 -1 0 -9 -0.10 0.12 1 0 9 -0.07 0.09 -1 0 -9 -0.03 0.16 -1 0 -11 -0.12 0.18 -1 0 -11 0.14 0.15 -1 0 -13 -0.06 0.24 -1 0 -13 0.03 0.18 -1 0 -15 -0.12 0.31 1 1 -18 5.19 0.50 1 1 -16 11.63 0.56 1 1 -14 11.07 0.53 1 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