data_shelxl _audit_creation_method SHELXL-2013 _chemical_name_systematic ; 'selenium dicyanide difluoride diglyme-solvate' ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C8 H14 F2 N2 O3 Se' _chemical_formula_weight 303.17 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Se' 'Se' -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 7.643(6) _cell_length_b 7.651(6) _cell_length_c 11.962(9) _cell_angle_alpha 84.701(16) _cell_angle_beta 89.908(17) _cell_angle_gamma 63.773(18) _cell_volume 624.2(8) _cell_formula_units_Z 2 _cell_measurement_temperature 133(2) _cell_measurement_reflns_used 879 _cell_measurement_theta_min 5.967 _cell_measurement_theta_max 61.008 _exptl_crystal_description block _exptl_crystal_colour colourless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.613 _exptl_crystal_F_000 304 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.8 _exptl_crystal_size_mid 0.5 _exptl_crystal_size_min 0.4 _exptl_absorpt_coefficient_mu 3.028 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.5892 _exptl_absorpt_correction_T_max 0.7461 _exptl_absorpt_process_details 'SADABS-2008/1 (Bruker-AXS)' _exptl_special_details ; ? ; _diffrn_ambient_temperature 133(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'sealed tube' _diffrn_measurement_device_type 'Bruker AXS Smart CCD' _diffrn_measurement_method 'omega scan' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 2631 _diffrn_reflns_av_unetI/netI 0.0462 _diffrn_reflns_av_R_equivalents 0.1089 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_k_min -7 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_theta_min 1.711 _diffrn_reflns_theta_max 25.027 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.954 _diffrn_measured_fraction_theta_full 0.933 _diffrn_reflns_Laue_measured_fraction_max 0.954 _diffrn_reflns_Laue_measured_fraction_full 0.933 _diffrn_reflns_point_group_measured_fraction_max 0.954 _diffrn_reflns_point_group_measured_fraction_full 0.933 _reflns_number_total 2105 _reflns_number_gt 1954 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Smart (Bruker AXS)' _computing_cell_refinement 'Saint (Bruker AXS)' _computing_data_reduction 'Saint (Bruker AXS)' _computing_structure_solution 'SHELXS-2013 (Sheldrick, 2013)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics 'Ortep3v2 for Windows' _computing_publication_material 'publCIF (IUCR)' _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details ; w=1/[\s^2^(Fo^2^)+(0.0567P)^2^+0.4917P] where P=(Fo^2^+2Fc^2^)/3 ; _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 2105 _refine_ls_number_parameters 147 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0390 _refine_ls_R_factor_gt 0.0360 _refine_ls_wR_factor_ref 0.0930 _refine_ls_wR_factor_gt 0.0909 _refine_ls_goodness_of_fit_ref 1.073 _refine_ls_restrained_S_all 1.073 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.5994(5) 0.7797(5) 0.8418(3) 0.0269(7) Uani 1 1 d . . . . . C2 C 0.6576(5) 0.9764(5) 0.6601(3) 0.0307(7) Uani 1 1 d . . . . . C3 C 0.7939(6) 0.2961(6) 0.9110(3) 0.0390(9) Uani 1 1 d . . . . . H3A H 0.8079 0.2009 0.8580 0.059 Uiso 1 1 calc R U . . . H3B H 0.6572 0.3943 0.9098 0.059 Uiso 1 1 calc R U . . . H3C H 0.8342 0.2285 0.9869 0.059 Uiso 1 1 calc R U . . . C4 C 1.1138(5) 0.2503(5) 0.8824(3) 0.0303(7) Uani 1 1 d . . . . . H4A H 1.1325 0.1534 0.8286 0.036 Uiso 1 1 calc R U . . . H4B H 1.1539 0.1797 0.9586 0.036 Uiso 1 1 calc R U . . . C5 C 1.2356(5) 0.3540(5) 0.8523(3) 0.0297(7) Uani 1 1 d . . . . . H5A H 1.2075 0.4602 0.9011 0.036 Uiso 1 1 calc R U . . . H5B H 1.3759 0.2614 0.8625 0.036 Uiso 1 1 calc R U . . . C6 C 1.2842(5) 0.5494(5) 0.7005(3) 0.0307(7) Uani 1 1 d . . . . . H6A H 1.4276 0.4710 0.7096 0.037 Uiso 1 1 calc R U . . . H6B H 1.2451 0.6628 0.7449 0.037 Uiso 1 1 calc R U . . . C7 C 1.2252(5) 0.6179(5) 0.5796(3) 0.0310(8) Uani 1 1 d . . . . . H7A H 1.2944 0.6938 0.5493 0.037 Uiso 1 1 calc R U . . . H7B H 1.2608 0.5039 0.5361 0.037 Uiso 1 1 calc R U . . . C8 C 0.9520(6) 0.7944(6) 0.4537(3) 0.0376(9) Uani 1 1 d . . . . . H8A H 1.0157 0.8702 0.4178 0.056 Uiso 1 1 calc R U . . . H8B H 0.8102 0.8742 0.4487 0.056 Uiso 1 1 calc R U . . . H8C H 0.9855 0.6765 0.4154 0.056 Uiso 1 1 calc R U . . . N1 N 0.4858(6) 0.8091(5) 0.9082(3) 0.0454(8) Uani 1 1 d . . . . . N2 N 0.5793(6) 1.1261(6) 0.6136(3) 0.0591(11) Uani 1 1 d . . . . . O1 O 0.9133(4) 0.3901(3) 0.87947(19) 0.0283(5) Uani 1 1 d . . . . . O2 O 1.1889(3) 0.4331(3) 0.73800(17) 0.0262(5) Uani 1 1 d . . . . . O3 O 1.0172(4) 0.7392(4) 0.56900(18) 0.0292(5) Uani 1 1 d . . . . . F1 F 0.8993(3) 0.8353(3) 0.82601(17) 0.0385(5) Uani 1 1 d . . . . . F2 F 0.6357(4) 0.6560(4) 0.65156(18) 0.0435(6) Uani 1 1 d . . . . . Se1 Se 0.79318(5) 0.72174(5) 0.73568(2) 0.02457(15) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0207(16) 0.0312(17) 0.0283(16) -0.0076(14) 0.0121(14) -0.0103(14) C2 0.0305(18) 0.0231(16) 0.0307(17) 0.0049(14) 0.0079(14) -0.0064(15) C3 0.037(2) 0.041(2) 0.052(2) -0.0067(17) 0.0102(17) -0.0283(18) C4 0.0310(19) 0.0341(18) 0.0265(16) -0.0033(13) 0.0042(14) -0.0151(16) C5 0.0292(18) 0.0384(19) 0.0247(16) -0.0033(14) 0.0009(14) -0.0180(16) C6 0.0279(18) 0.042(2) 0.0317(17) -0.0058(15) 0.0049(14) -0.0242(17) C7 0.0279(18) 0.0410(19) 0.0316(17) -0.0065(14) 0.0087(14) -0.0215(17) C8 0.044(2) 0.050(2) 0.0249(17) -0.0057(15) 0.0015(16) -0.026(2) N1 0.043(2) 0.0460(19) 0.0435(18) 0.0003(15) 0.0098(17) -0.0174(17) N2 0.048(2) 0.056(2) 0.057(2) 0.0033(19) 0.0245(19) -0.010(2) O1 0.0281(12) 0.0315(12) 0.0318(12) -0.0034(10) 0.0067(10) -0.0190(11) O2 0.0262(12) 0.0377(13) 0.0218(11) -0.0055(9) 0.0026(9) -0.0201(11) O3 0.0327(13) 0.0383(13) 0.0226(11) -0.0028(10) 0.0033(10) -0.0212(12) F1 0.0429(13) 0.0485(13) 0.0363(11) -0.0130(9) 0.0047(10) -0.0297(11) F2 0.0484(14) 0.0651(15) 0.0370(11) -0.0169(10) 0.0071(10) -0.0412(13) Se1 0.0269(2) 0.0308(2) 0.0226(2) -0.00602(13) 0.00644(13) -0.01817(16) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 N1 1.137(5) . ? C1 Se1 1.876(3) . ? C2 N2 1.121(5) . ? C2 Se1 1.892(3) . ? C3 O1 1.421(4) . ? C4 O1 1.427(4) . ? C4 C5 1.492(5) . ? C5 O2 1.421(4) . ? C6 O2 1.421(4) . ? C6 C7 1.490(5) . ? C7 O3 1.442(5) . ? C8 O3 1.428(4) . ? O1 Se1 2.717(3) . ? O2 Se1 2.848(3) . ? O3 Se1 2.658(3) . ? F1 Se1 1.838(2) . ? F2 Se1 1.829(2) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 C1 Se1 177.7(3) . . ? N2 C2 Se1 178.7(4) . . ? O1 C4 C5 109.2(3) . . ? O2 C5 C4 107.7(3) . . ? O2 C6 C7 107.5(3) . . ? O3 C7 C6 109.2(3) . . ? C3 O1 C4 110.5(3) . . ? C3 O1 Se1 124.0(2) . . ? C4 O1 Se1 118.58(19) . . ? C5 O2 C6 113.6(2) . . ? C5 O2 Se1 104.6(2) . . ? C6 O2 Se1 101.3(2) . . ? C8 O3 C7 111.0(3) . . ? C8 O3 Se1 124.5(2) . . ? C7 O3 Se1 119.78(18) . . ? F2 Se1 F1 167.05(11) . . ? F2 Se1 C1 85.41(14) . . ? F1 Se1 C1 85.15(13) . . ? F2 Se1 C2 86.11(15) . . ? F1 Se1 C2 85.13(14) . . ? C1 Se1 C2 90.59(15) . . ? F2 Se1 O3 95.80(10) . . ? F1 Se1 O3 91.06(10) . . ? C1 Se1 O3 165.02(12) . . ? C2 Se1 O3 74.63(12) . . ? F2 Se1 O1 93.03(10) . . ? F1 Se1 O1 93.10(10) . . ? C1 Se1 O1 75.10(12) . . ? C2 Se1 O1 165.68(12) . . ? O3 Se1 O1 119.65(8) . . ? F2 Se1 O2 110.87(10) . . ? F1 Se1 O2 82.07(10) . . ? C1 Se1 O2 132.90(12) . . ? C2 Se1 O2 132.78(12) . . ? O3 Se1 O2 60.45(8) . . ? O1 Se1 O2 60.66(7) . . ? _refine_diff_density_max 1.331 _refine_diff_density_min -0.538 _refine_diff_density_rms 0.096 _shelxl_version_number 2013-2 _shelx_res_file ; TITL sf194n in P-1 CELL 0.71073 7.6426 7.6511 11.9623 84.701 89.908 63.773 ZERR 2.00 0.0057 0.0058 0.0090 0.016 0.017 0.018 LATT 1 SFAC C H N O F SE UNIT 16 28 4 6 4 2 MERG 2 SHEL 100 0.84 FMAP 2 PLAN 5 BIND SE1 O1 BIND SE1 O2 BIND SE1 O3 ACTA BOND L.S. 12 TEMP -140.00 WGHT 0.056700 0.491700 FVAR 0.47675 C1 1 0.599370 0.779706 0.841842 11.00000 0.02073 0.03115 = 0.02828 -0.00756 0.01212 -0.01026 C2 1 0.657629 0.976432 0.660085 11.00000 0.03054 0.02307 = 0.03069 0.00494 0.00794 -0.00637 C3 1 0.793882 0.296140 0.910977 11.00000 0.03713 0.04092 = 0.05156 -0.00675 0.01018 -0.02826 AFIX 137 H3A 2 0.807943 0.200894 0.857981 11.00000 -1.50000 H3B 2 0.657156 0.394253 0.909795 11.00000 -1.50000 H3C 2 0.834220 0.228493 0.986880 11.00000 -1.50000 AFIX 0 C4 1 1.113751 0.250329 0.882438 11.00000 0.03096 0.03413 = 0.02652 -0.00332 0.00419 -0.01512 AFIX 23 H4A 2 1.132501 0.153357 0.828581 11.00000 -1.20000 H4B 2 1.153857 0.179683 0.958621 11.00000 -1.20000 AFIX 0 C5 1 1.235574 0.354017 0.852271 11.00000 0.02922 0.03841 = 0.02472 -0.00331 0.00093 -0.01804 AFIX 23 H5A 2 1.207468 0.460188 0.901094 11.00000 -1.20000 H5B 2 1.375922 0.261422 0.862452 11.00000 -1.20000 AFIX 0 C6 1 1.284197 0.549391 0.700474 11.00000 0.02792 0.04243 = 0.03166 -0.00577 0.00491 -0.02421 AFIX 23 H6A 2 1.427598 0.470966 0.709569 11.00000 -1.20000 H6B 2 1.245063 0.662844 0.744865 11.00000 -1.20000 AFIX 0 C7 1 1.225208 0.617911 0.579645 11.00000 0.02791 0.04095 = 0.03164 -0.00648 0.00874 -0.02154 AFIX 23 H7A 2 1.294446 0.693761 0.549349 11.00000 -1.20000 H7B 2 1.260803 0.503878 0.536112 11.00000 -1.20000 AFIX 0 C8 1 0.952049 0.794360 0.453686 11.00000 0.04357 0.05019 = 0.02492 -0.00573 0.00149 -0.02581 AFIX 137 H8A 2 1.015674 0.870235 0.417816 11.00000 -1.50000 H8B 2 0.810187 0.874249 0.448665 11.00000 -1.50000 H8C 2 0.985548 0.676478 0.415416 11.00000 -1.50000 AFIX 0 N1 3 0.485791 0.809087 0.908176 11.00000 0.04290 0.04604 = 0.04346 0.00030 0.00981 -0.01735 N2 3 0.579327 1.126087 0.613640 11.00000 0.04840 0.05567 = 0.05674 0.00327 0.02446 -0.01005 O1 4 0.913279 0.390088 0.879472 11.00000 0.02808 0.03151 = 0.03180 -0.00344 0.00669 -0.01900 O2 4 1.188940 0.433127 0.738001 11.00000 0.02625 0.03767 = 0.02182 -0.00552 0.00256 -0.02008 O3 4 1.017222 0.739177 0.569005 11.00000 0.03265 0.03832 = 0.02258 -0.00279 0.00327 -0.02118 F1 5 0.899330 0.835287 0.826009 11.00000 0.04287 0.04854 = 0.03633 -0.01301 0.00467 -0.02968 F2 5 0.635739 0.655997 0.651559 11.00000 0.04838 0.06512 = 0.03701 -0.01690 0.00713 -0.04120 SE1 6 0.793178 0.721738 0.735676 11.00000 0.02694 0.03076 = 0.02262 -0.00602 0.00644 -0.01817 HKLF 4 REM sf194n in P-1 REM R1 = 0.0360 for 1954 Fo > 4sig(Fo) and 0.0390 for all 2105 data REM 147 parameters refined using 0 restraints END WGHT 0.0562 0.5022 REM Highest difference peak 1.331, deepest hole -0.538, 1-sigma level 0.096 Q1 1 0.7025 0.8431 0.7065 11.00000 0.05 1.33 Q2 1 0.8992 0.5657 0.7595 11.00000 0.05 0.63 Q3 1 0.9472 0.6748 0.7412 11.00000 0.05 0.56 Q4 1 0.6872 0.7181 0.8268 11.00000 0.05 0.51 Q5 1 0.8667 0.4633 0.8350 11.00000 0.05 0.43 ; _shelx_res_checksum 65680 _shelx_hkl_file ; 0 0 1 20.07 0.26 0 0 2 1159.55 7.38 0 0 3 18.26 0.47 0 0 4 22.05 0.60 0 0 5 289.29 2.15 0 0 6 439.12 3.05 0 0 7 494.43 3.46 0 0 8 153.97 1.78 0 0 9 68.99 1.45 0 0 10 171.27 2.17 0 0 11 195.51 2.44 0 0 12 63.57 1.86 0 0 13 124.59 2.29 0 0 -16 0.55 1.58 0 0 -17 26.27 2.39 0 1 -16 4.75 1.63 0 1 -14 53.17 2.18 0 1 -13 60.22 1.99 0 1 -12 121.25 2.25 0 1 -11 162.03 2.41 0 1 -10 77.31 1.78 0 1 -9 32.97 1.44 0 1 -6 24.75 0.95 0 1 -5 772.80 4.75 0 1 -4 17.13 0.62 0 1 -3 971.52 5.76 0 1 -2 35.56 0.54 0 1 -1 1010.25 6.40 0 1 0 303.98 2.14 0 1 1 1278.72 8.18 0 1 2 953.92 5.83 0 1 3 761.55 4.62 0 1 4 90.80 1.02 0 1 5 28.66 0.78 0 1 6 201.29 1.82 0 1 7 8.14 0.89 0 1 8 378.29 2.99 0 1 9 18.22 1.15 0 1 10 194.54 2.27 0 1 11 148.53 2.14 0 1 12 149.45 2.26 0 1 13 1.86 1.03 0 1 14 34.82 1.92 0 1 15 7.45 1.41 0 1 16 18.62 2.09 0 2 -16 2.09 1.60 0 2 -15 10.89 1.57 0 2 -13 43.83 1.94 0 2 -12 49.03 1.82 0 2 -11 70.07 1.83 0 2 -10 89.48 1.84 0 2 -9 24.87 1.41 0 2 -8 90.31 1.63 0 2 -7 95.72 1.53 0 2 -6 169.80 1.81 0 2 -5 29.45 0.95 0 2 -4 94.79 1.22 0 2 -3 176.40 1.55 0 2 -2 1849.21 10.47 0 2 -1 23.17 0.67 0 2 0 1536.17 8.86 0 2 1 12.73 0.57 0 2 2 644.03 3.97 0 2 3 43.89 0.79 0 2 4 38.91 0.85 0 2 5 280.21 2.22 0 2 6 456.14 3.23 0 2 7 252.10 2.29 0 2 8 54.08 1.33 0 2 9 112.79 1.77 0 2 10 74.39 1.68 0 2 11 187.94 2.41 0 2 12 6.54 1.02 0 2 13 44.67 1.83 0 2 14 1.47 1.15 0 2 15 20.71 1.87 0 2 16 0.13 1.41 0 3 -15 19.57 2.19 0 3 -14 37.88 2.16 0 3 -13 66.68 2.15 0 3 -12 12.29 1.35 0 3 -11 52.57 1.89 0 3 -10 5.41 1.06 0 3 -9 71.64 1.76 0 3 -8 14.48 1.35 0 3 -7 263.77 2.59 0 3 -6 7.01 0.74 0 3 -5 417.32 3.17 0 3 -4 5.33 0.58 0 3 -3 587.04 3.88 0 3 -2 73.79 1.18 0 3 0 70.52 1.08 0 3 1 396.40 2.77 0 3 2 79.64 1.14 0 3 3 34.84 0.94 0 3 4 17.23 0.90 0 3 5 110.26 1.49 0 3 6 305.08 2.59 0 3 7 201.34 2.15 0 3 8 501.03 3.81 0 3 9 135.93 2.01 0 3 10 272.05 2.87 0 3 11 38.38 1.64 0 3 12 135.90 2.39 0 3 13 14.28 1.66 0 3 14 23.15 1.87 0 3 15 10.92 1.47 0 3 16 30.87 2.11 0 4 -14 43.02 2.37 0 4 -13 8.87 1.58 0 4 -12 67.73 2.27 0 4 -11 3.47 1.28 0 4 -10 56.72 1.93 0 4 -9 28.61 1.63 0 4 -8 43.83 1.63 0 4 -7 2.16 0.88 0 4 -6 187.02 2.27 0 4 -5 16.63 1.28 0 4 -4 340.46 2.92 0 4 -3 74.66 1.49 0 4 -1 64.45 1.32 0 4 0 111.25 1.51 0 4 1 167.02 1.81 0 4 2 1.25 0.58 0 4 3 294.84 2.52 0 4 4 130.10 1.72 0 4 5 508.93 3.75 0 4 6 46.89 1.45 0 4 7 296.57 2.83 0 4 8 5.36 0.90 0 4 9 236.82 2.65 0 4 10 4.38 1.01 0 4 11 141.38 2.34 0 4 12 23.34 1.84 0 4 13 36.22 1.93 0 4 14 33.02 2.02 0 4 15 33.67 2.17 0 4 16 15.78 1.71 0 5 -13 5.99 1.72 0 5 -12 0.19 1.54 0 5 -10 0.25 1.32 0 5 -9 74.05 2.17 0 5 -7 39.02 1.78 0 5 -6 17.36 1.58 0 5 -5 62.14 1.76 0 5 -4 81.80 1.81 0 5 -3 99.27 1.82 0 5 -2 23.55 1.39 0 5 -1 111.18 1.81 0 5 0 16.48 1.28 0 5 1 19.94 1.31 0 5 2 181.89 2.18 0 5 3 -0.33 0.84 0 5 4 201.32 2.33 0 5 5 22.38 1.47 0 5 6 255.50 2.75 0 5 7 4.58 1.00 0 5 8 185.54 2.55 0 5 9 8.24 1.18 0 5 10 38.99 1.84 0 5 11 6.73 1.26 0 5 12 15.74 1.93 0 5 13 19.95 2.05 0 5 14 6.63 1.53 0 5 15 16.60 1.76 0 6 -12 12.27 1.87 0 6 -11 0.36 1.62 0 6 -9 7.56 1.55 0 6 -8 67.13 2.27 0 6 -7 1.20 1.33 0 6 -6 176.51 2.66 0 6 -5 22.05 1.80 0 6 -4 40.04 1.76 0 6 -3 81.30 1.98 0 6 -2 18.61 1.61 0 6 -1 49.32 1.73 0 6 0 32.30 1.17 0 6 0 30.68 1.60 0 6 1 79.45 1.93 0 6 2 13.74 1.58 0 6 3 132.19 2.19 0 6 4 22.55 1.68 0 6 5 170.88 2.47 0 6 6 2.15 1.18 0 6 7 144.69 2.54 0 6 8 0.09 1.23 0 6 9 65.61 2.27 0 6 10 7.42 1.48 0 6 11 8.81 1.42 0 6 12 17.70 2.13 0 6 13 16.40 1.74 0 6 14 8.99 1.71 0 7 -10 -0.13 1.83 0 7 -9 19.31 2.24 0 7 -8 3.26 1.61 0 7 -7 8.82 1.57 0 7 -6 37.45 2.15 0 7 -5 56.25 2.21 0 7 -4 83.58 2.32 0 7 -3 36.25 2.01 0 7 -2 42.22 2.06 0 7 -1 1.45 1.25 0 7 0 82.23 2.24 0 7 1 1.32 1.31 0 7 2 150.75 2.56 0 7 3 -1.51 1.37 0 7 4 66.01 2.15 0 7 5 5.77 1.46 0 7 6 94.32 2.38 0 7 7 7.10 1.55 0 7 8 80.64 2.48 0 7 10 16.84 1.82 0 7 11 8.31 1.71 0 7 12 10.42 1.57 0 7 13 24.22 2.50 0 8 -8 13.60 2.02 0 8 -7 4.38 1.96 0 8 -6 7.85 1.91 0 8 -5 41.88 2.52 0 8 -4 2.99 1.75 0 8 -3 42.33 2.42 0 8 -2 3.94 1.54 0 8 -1 29.69 2.18 0 8 0 4.45 1.65 0 8 1 54.58 2.40 0 8 2 6.75 1.64 0 8 3 39.50 2.27 0 8 4 5.74 1.69 0 8 5 35.15 2.37 0 8 6 8.92 1.85 0 8 7 30.15 2.33 0 8 8 10.43 1.82 0 8 9 9.47 1.93 0 8 10 12.84 2.00 0 8 11 5.15 1.94 0 9 -4 12.52 2.05 0 9 -3 0.36 1.92 0 9 -2 6.42 1.96 0 9 -1 0.76 1.87 0 9 0 29.20 2.52 0 9 1 -0.20 1.82 0 9 2 37.03 2.50 0 9 3 1.86 1.97 0 9 4 14.09 2.02 0 9 5 3.95 2.04 0 9 6 27.38 2.57 0 9 7 19.04 2.21 -1 9 5 30.50 2.79 -1 9 4 11.75 2.28 -1 9 3 15.66 2.23 -1 9 2 3.25 2.12 -1 9 1 16.22 2.04 -1 9 0 5.62 1.93 -1 9 -1 29.55 2.62 -1 9 -2 2.73 1.97 -1 8 9 6.51 1.99 -1 8 8 5.76 1.91 -1 8 7 9.71 1.96 -1 8 6 25.60 2.39 -1 8 5 19.92 2.44 -1 8 -2 24.60 2.34 -1 8 -3 5.32 1.74 -1 8 -4 10.73 1.90 -1 8 -5 5.23 1.90 -1 8 -6 23.51 2.55 -1 7 12 38.68 2.34 -1 7 11 13.48 1.82 -1 7 10 32.93 2.34 -1 7 9 9.36 1.82 -1 7 8 10.56 1.74 -1 7 7 27.44 2.14 -1 7 6 6.62 1.65 -1 7 5 95.64 2.54 -1 7 4 0.90 1.59 -1 7 3 30.23 2.16 -1 7 2 15.13 1.64 -1 7 1 54.05 2.14 -1 7 0 4.92 1.46 -1 7 -1 47.25 2.07 -1 7 -2 8.97 1.54 -1 7 -3 14.92 1.67 -1 7 -3 15.24 1.64 -1 7 -4 8.05 1.28 -1 7 -4 7.59 1.60 -1 7 -5 28.78 2.13 -1 7 -6 4.40 1.72 -1 7 -7 19.33 2.24 -1 7 -8 9.85 1.78 -1 7 -9 6.05 1.74 -1 6 13 66.75 2.64 -1 6 12 3.25 1.53 -1 6 11 24.58 2.07 -1 6 10 27.68 2.12 -1 6 9 4.14 1.53 -1 6 8 120.89 2.58 -1 6 7 20.64 1.87 -1 6 6 175.16 2.68 -1 6 5 3.86 1.31 -1 6 4 102.50 2.26 -1 6 3 1.73 1.17 -1 6 2 53.76 1.87 -1 6 1 16.68 1.65 -1 6 0 116.00 1.80 -1 6 0 105.82 2.18 -1 6 -1 0.77 0.88 -1 6 -1 -0.48 1.14 -1 6 -2 70.05 1.70 -1 6 -2 61.09 1.91 -1 6 -3 40.86 1.92 -1 6 -4 44.02 1.91 -1 6 -5 31.02 1.86 -1 6 -6 68.33 2.09 -1 6 -7 31.73 2.02 -1 6 -8 16.71 2.03 -1 6 -9 3.83 1.58 -1 6 -10 2.78 1.69 -1 6 -11 14.30 1.93 -1 5 14 8.13 1.68 -1 5 13 29.06 2.09 -1 5 12 50.10 2.28 -1 5 11 60.86 2.08 -1 5 10 5.80 1.28 -1 5 9 41.89 1.90 -1 5 8 3.03 1.20 -1 5 7 202.04 2.63 -1 5 6 4.90 1.09 -1 5 5 278.94 2.91 -1 5 4 2.19 0.96 -1 5 3 91.27 1.84 -1 5 2 0.48 0.60 -1 5 2 -1.06 0.89 -1 5 1 144.50 1.71 -1 5 1 129.28 2.03 -1 5 0 40.87 1.24 -1 5 0 32.49 1.46 -1 5 -1 61.09 1.41 -1 5 -1 49.93 1.56 -1 5 -2 79.72 1.83 -1 5 -3 51.78 1.70 -1 5 -5 132.55 2.24 -1 5 -6 94.59 2.03 -1 5 -7 27.33 1.75 -1 5 -8 82.12 2.19 -1 5 -9 2.43 1.32 -1 5 -10 31.20 2.04 -1 5 -11 1.53 1.51 -1 5 -12 17.87 2.19 -1 5 -13 -0.45 1.71 -1 4 15 31.96 2.22 -1 4 14 14.06 1.59 -1 4 13 15.77 1.87 -1 4 12 18.47 1.85 -1 4 11 1.73 1.18 -1 4 10 95.38 2.12 -1 4 9 1.30 0.99 -1 4 8 194.14 2.54 -1 4 7 5.09 0.91 -1 4 6 101.41 1.82 -1 4 5 0.50 0.75 -1 4 4 111.51 1.72 -1 4 3 0.78 0.47 -1 4 3 1.43 0.72 -1 4 2 174.88 1.60 -1 4 2 155.40 1.88 -1 4 1 2.98 0.53 -1 4 1 1.04 0.62 -1 4 0 164.09 1.70 -1 4 0 132.30 1.74 -1 4 -1 245.90 2.07 -1 4 -1 210.48 2.20 -1 4 -2 14.62 1.18 -1 4 -4 42.91 1.44 -1 4 -5 55.44 1.60 -1 4 -6 76.05 1.75 -1 4 -7 49.24 1.66 -1 4 -8 1.17 1.01 -1 4 -9 36.03 1.71 -1 4 -10 -0.03 1.17 -1 4 -11 63.44 2.08 -1 4 -12 0.65 1.42 -1 4 -13 32.06 2.19 -1 4 -14 5.96 1.70 -1 3 16 7.92 1.59 -1 3 15 21.97 2.01 -1 3 14 28.11 1.98 -1 3 13 49.04 2.04 -1 3 12 56.24 1.92 -1 3 11 117.07 2.18 -1 3 10 5.82 0.97 -1 3 9 163.84 2.24 -1 3 8 9.45 0.92 -1 3 8 13.30 1.28 -1 3 7 301.60 2.31 -1 3 7 297.06 2.74 -1 3 6 38.63 0.93 -1 3 6 36.50 1.29 -1 3 5 298.91 2.18 -1 3 5 270.15 2.42 -1 3 4 20.11 0.74 -1 3 4 20.46 1.02 -1 3 3 275.15 2.01 -1 3 3 264.74 2.26 -1 3 2 9.11 0.66 -1 3 2 8.75 0.60 -1 3 1 526.11 3.37 -1 3 1 435.80 3.08 -1 3 0 260.25 2.00 -1 3 0 206.36 1.86 -1 3 -1 104.56 1.40 -1 3 -2 516.95 3.53 -1 3 -3 130.06 1.65 -1 3 -4 428.79 3.22 -1 3 -5 104.66 1.62 -1 3 -6 98.39 1.67 -1 3 -7 2.70 0.82 -1 3 -8 26.52 1.50 -1 3 -9 -0.08 0.94 -1 3 -10 55.09 1.78 -1 3 -11 0.25 1.12 -1 3 -12 63.64 2.08 -1 3 -13 8.08 1.48 -1 3 -14 46.46 2.25 -1 3 -15 1.61 1.64 -1 2 16 25.74 2.03 -1 2 15 11.94 1.47 -1 2 14 85.56 2.22 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1.16 -1 1 3 106.57 1.07 -1 1 2 845.33 5.22 -1 1 2 688.08 4.22 -1 1 1 111.34 0.96 -1 1 1 88.97 0.85 -1 1 0 731.75 4.54 -1 1 0 497.98 3.21 -1 1 -1 177.63 1.37 -1 1 -2 1538.26 8.97 -1 1 -3 97.26 1.04 -1 1 -4 249.18 1.90 -1 1 -5 26.20 0.81 -1 1 -6 10.44 0.82 -1 1 -7 25.83 1.09 -1 1 -8 163.79 1.96 -1 1 -9 102.93 1.72 -1 1 -10 219.83 2.50 -1 1 -11 55.30 1.74 -1 1 -12 55.12 1.85 -1 1 -13 27.09 1.80 -1 1 -14 20.34 1.78 -1 1 -15 16.16 1.89 -1 1 -16 0.66 1.48 1 0 -17 2.50 1.81 -1 0 14 90.67 2.34 -1 0 13 -0.58 1.07 -1 0 12 102.85 2.10 -1 0 11 17.13 1.43 -1 0 10 236.43 2.53 -1 0 9 112.83 1.73 -1 0 8 25.82 1.11 -1 0 7 12.62 0.91 -1 0 6 117.51 1.38 -1 0 5 10.53 0.66 -1 0 5 9.91 0.68 -1 0 4 673.34 4.13 -1 0 4 592.63 3.71 -1 0 3 1595.89 9.29 -1 0 3 1148.35 6.77 -1 0 2 4.31 0.36 -1 0 2 3.23 0.32 -1 0 1 866.97 5.65 -1 0 1 688.38 5.06 -1 0 0 418.09 2.89 -1 0 0 293.98 3.25 -1 0 -1 856.54 5.50 -1 0 -1 741.15 6.16 1 0 3 5.68 0.41 1 0 4 7.10 0.49 1 0 5 15.84 0.68 1 0 6 128.44 1.40 1 0 7 609.40 4.05 1 0 8 9.42 0.98 1 0 9 96.38 1.57 1 0 10 70.77 1.57 1 0 11 101.79 1.91 -1 0 -13 90.52 2.32 -1 0 -14 29.00 1.90 -1 0 -15 7.01 1.47 -1 0 -16 6.73 1.55 1 1 -16 -1.03 1.55 1 1 -15 59.60 2.40 1 1 -14 4.80 1.40 1 1 -13 106.87 2.42 -1 -1 10 105.05 1.86 -1 -1 9 68.22 1.51 -1 -1 8 30.49 1.19 -1 -1 7 119.46 1.55 -1 -1 6 222.49 1.98 -1 -1 5 380.75 2.69 -1 -1 4 682.36 4.20 -1 -1 3 312.58 2.15 -1 -1 2 311.55 2.11 1 1 -2 258.76 1.79 -1 -1 1 68.93 0.66 1 1 -1 58.59 0.57 1 1 0 2375.21 18.84 1 1 1 197.90 1.58 1 1 2 3683.82 23.01 1 1 3 204.83 1.51 1 1 4 16.71 0.59 1 1 5 13.81 0.64 1 1 6 117.03 1.32 1 1 7 228.04 2.03 1 1 8 1043.22 6.41 1 1 9 254.37 2.45 1 1 10 237.41 2.46 1 1 11 45.05 1.46 1 1 12 33.84 1.60 1 1 13 73.70 1.98 1 1 14 14.46 1.74 1 1 15 71.82 2.26 -1 -1 -17 20.02 1.99 1 2 -16 46.32 2.36 1 2 -15 2.02 1.39 1 2 -14 22.70 1.89 1 2 -13 6.49 1.36 1 2 -12 49.08 1.96 1 2 -11 76.84 1.96 1 2 -10 89.36 1.91 1 2 -9 138.57 2.05 1 2 -8 2.92 0.70 1 2 -7 45.99 1.26 1 2 -6 175.04 1.81 1 2 -5 1069.97 6.37 1 2 -4 64.26 0.99 1 2 -3 1426.61 8.18 1 2 -2 106.41 1.06 1 2 -1 268.80 1.90 1 2 0 135.18 1.14 1 2 1 1029.41 6.17 1 2 2 331.87 2.24 1 2 3 404.46 2.67 1 2 4 191.50 1.60 1 2 5 799.47 4.89 1 2 6 132.50 1.48 1 2 7 450.69 3.26 1 2 8 620.59 4.26 1 2 9 4.51 0.71 1 2 10 323.43 2.98 1 2 11 47.36 1.51 1 2 12 109.61 2.06 1 2 13 18.81 1.57 1 2 14 25.22 1.75 1 2 15 6.75 1.35 1 2 16 22.08 2.09 1 3 -15 8.66 1.62 1 3 -14 5.20 1.44 1 3 -13 15.92 1.79 1 3 -12 12.83 1.37 1 3 -11 25.68 1.66 1 3 -10 31.23 1.65 1 3 -9 28.23 1.47 1 3 -8 58.47 1.55 1 3 -7 95.14 1.63 1 3 -6 433.72 3.32 1 3 -5 52.87 1.23 1 3 -4 522.81 3.57 1 3 -3 3.65 0.46 1 3 -2 302.20 2.28 1 3 -1 95.05 1.14 1 3 0 500.63 3.25 1 3 1 30.87 0.77 1 3 2 120.13 1.26 1 3 3 32.04 0.84 1 3 4 24.95 0.88 1 3 5 244.76 2.12 1 3 6 514.57 3.60 1 3 7 375.39 2.97 1 3 8 353.32 2.97 1 3 9 168.87 2.08 1 3 10 13.21 1.36 1 3 11 20.25 1.51 1 3 12 0.82 0.98 1 3 13 67.58 1.93 1 3 14 0.29 1.15 1 3 15 27.72 2.00 1 3 16 0.00 1.36 1 4 -15 -0.23 1.68 1 4 -14 15.41 1.75 1 4 -13 25.06 2.06 1 4 -12 18.48 1.88 1 4 -11 52.12 1.93 1 4 -10 20.01 1.62 1 4 -9 83.21 1.92 1 4 -8 21.86 1.53 1 4 -7 187.37 2.32 1 4 -6 154.88 2.04 1 4 -5 601.04 4.26 1 4 -4 1.60 0.65 1 4 -3 278.00 2.44 1 4 -2 114.06 1.53 1 4 -1 168.54 1.76 1 4 0 26.26 1.00 1 4 1 442.09 3.13 1 4 2 172.16 1.77 1 4 3 140.33 1.61 1 4 4 39.50 1.13 1 4 5 257.90 2.36 1 4 6 99.08 1.61 1 4 7 102.36 1.72 1 4 8 268.04 2.70 1 4 9 19.68 1.39 1 4 10 98.16 1.92 1 4 11 43.65 1.67 1 4 12 51.93 1.92 1 4 13 0.23 1.16 1 4 14 27.40 1.91 1 4 15 7.04 1.44 1 4 16 36.42 2.26 1 5 -14 13.38 1.87 1 5 -13 8.65 1.70 1 5 -12 59.13 2.37 1 5 -11 12.26 1.50 1 5 -10 99.83 2.35 1 5 -9 0.55 1.17 1 5 -8 148.83 2.38 1 5 -7 6.87 1.05 1 5 -6 226.30 2.62 1 5 -5 4.96 0.93 1 5 -4 192.38 2.32 1 5 -3 23.30 1.37 1 5 -2 110.84 1.76 1 5 -1 107.42 1.70 1 5 0 115.05 1.70 1 5 1 136.76 1.83 1 5 2 136.85 1.85 1 5 3 232.83 2.35 1 5 4 107.27 1.74 1 5 5 271.83 2.69 1 5 6 174.43 2.27 1 5 7 197.59 2.42 1 5 8 7.66 1.01 1 5 9 99.85 2.03 1 5 10 9.89 1.12 1 5 11 72.66 2.01 1 5 12 3.53 1.23 1 5 13 100.51 2.45 1 5 14 2.86 1.41 1 5 15 39.44 2.27 1 6 -12 -0.60 1.63 1 6 -11 28.68 2.20 1 6 -10 0.76 1.46 1 6 -9 107.85 2.50 1 6 -8 0.90 1.27 1 6 -7 90.12 2.22 1 6 -6 1.13 1.15 1 6 -5 29.02 1.71 1 6 -4 101.62 2.03 1 6 -3 6.00 0.99 1 6 -2 93.41 1.98 1 6 -1 63.84 1.72 1 6 0 11.96 1.01 1 6 1 90.86 1.84 1 6 2 78.37 1.79 1 6 3 23.81 1.51 1 6 4 165.55 2.29 1 6 5 41.37 1.74 1 6 6 180.27 2.48 1 6 7 4.81 1.13 1 6 8 103.88 2.22 1 6 9 7.76 1.31 1 6 10 48.43 1.99 1 6 11 4.92 1.33 1 6 12 36.57 2.14 1 6 13 11.21 1.54 1 6 14 24.96 2.25 1 7 -11 2.77 1.85 1 7 -10 18.18 2.21 1 7 -9 1.29 1.60 1 7 -8 35.58 2.17 1 7 -7 4.37 1.55 1 7 -6 49.87 2.09 1 7 -5 -0.91 1.30 1 7 -4 38.03 1.96 1 7 -3 29.97 1.89 1 7 -2 8.55 1.27 1 7 -1 93.37 2.14 1 7 0 26.27 1.73 1 7 1 37.90 1.89 1 7 2 108.12 2.20 1 7 3 51.89 1.93 1 7 4 21.02 1.77 1 7 5 76.59 2.11 1 7 6 0.41 1.28 1 7 7 89.48 2.39 1 7 8 4.48 1.45 1 7 9 75.96 2.47 1 7 10 6.39 1.59 1 7 11 28.44 2.19 1 7 12 2.17 1.50 1 7 13 20.39 2.36 1 8 -8 3.91 1.72 1 8 -7 6.30 1.75 1 8 -6 4.22 1.81 1 8 -5 14.22 1.79 1 8 -4 57.78 2.38 1 8 -3 61.93 2.45 1 8 -2 42.79 2.20 1 8 -1 43.83 2.09 1 8 0 28.37 2.11 1 8 1 6.33 1.54 1 8 2 123.16 2.57 1 8 3 -2.18 1.55 1 8 4 104.04 2.58 1 8 5 0.34 1.64 1 8 6 39.57 2.28 1 8 7 3.85 1.67 1 8 8 43.50 2.38 1 8 9 15.50 1.90 1 8 10 46.50 2.65 1 8 11 7.53 1.85 1 9 -6 7.36 1.94 1 9 -5 5.92 1.99 1 9 -4 3.13 1.80 1 9 -3 56.41 2.67 1 9 -2 2.56 1.84 1 9 -1 62.25 2.63 1 9 0 16.09 1.88 1 9 1 26.51 2.29 1 9 2 3.66 1.82 1 9 3 42.71 2.54 1 9 4 34.15 2.43 1 9 5 26.43 2.50 1 9 6 17.33 2.08 1 9 7 30.65 2.63 1 9 8 7.54 1.96 1 9 9 16.37 2.14 1 10 -1 -1.06 2.02 1 10 0 10.07 2.11 1 10 1 1.91 1.92 1 10 2 38.60 2.80 1 10 3 1.54 1.99 1 10 4 10.13 2.11 -2 8 7 3.32 1.93 -2 8 6 17.41 2.07 -2 8 5 13.63 2.06 -2 8 4 21.12 2.45 -2 8 3 25.32 2.52 -2 8 2 9.83 2.00 -2 8 1 13.32 1.96 -2 8 0 8.77 1.83 -2 8 -1 13.22 1.79 -2 8 -2 10.76 1.99 -2 8 -3 26.60 2.50 -2 8 -4 1.16 1.94 -2 7 10 3.07 1.84 -2 7 9 17.28 1.92 -2 7 8 15.66 1.90 -2 7 7 -0.36 1.67 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6.40 1.36 -2 5 8 82.61 2.22 -2 5 7 16.82 1.78 -2 5 6 132.93 2.35 -2 5 5 149.57 2.34 -2 5 4 130.97 2.25 -2 5 3 1.69 0.79 -2 5 3 1.67 1.06 -2 5 2 51.01 1.38 -2 5 2 44.94 1.73 -2 5 1 6.25 0.88 -2 5 1 4.98 1.07 -2 5 0 146.94 1.99 -2 5 0 120.14 2.03 -2 5 -1 0.26 0.88 -2 5 -1 -0.03 0.93 -2 5 -2 154.67 2.16 -2 5 -2 122.81 2.10 -2 5 -3 11.70 1.45 -2 5 -3 11.81 1.23 -2 5 -4 48.74 1.65 -2 5 -4 39.08 1.74 -2 5 -5 28.43 1.69 -2 5 -6 51.03 1.89 -2 5 -7 16.42 1.79 -2 5 -8 35.92 1.96 -2 5 -9 6.99 1.52 -2 5 -10 2.91 1.58 -2 5 -11 10.29 1.73 -2 5 -12 1.04 1.69 -2 4 15 5.61 1.67 -2 4 14 13.15 1.68 -2 4 13 38.87 2.13 -2 4 12 32.82 2.02 -2 4 11 109.02 2.41 -2 4 10 67.90 1.98 -2 4 9 89.79 2.03 -2 4 8 11.47 1.17 -2 4 7 82.48 1.86 -2 4 6 1.14 0.68 -2 4 6 -0.61 0.93 -2 4 5 305.02 2.48 -2 4 5 288.90 2.86 -2 4 4 7.25 0.73 -2 4 4 7.99 0.95 -2 4 3 422.63 3.09 -2 4 3 401.61 3.33 -2 4 2 1.26 0.67 -2 4 2 0.95 0.83 -2 4 1 129.31 1.67 -2 4 1 110.37 1.78 -2 4 0 54.43 1.37 -2 4 0 34.33 1.29 -2 4 -1 142.52 1.89 -2 4 -1 105.41 1.73 -2 4 -2 171.03 2.08 -2 4 -2 131.39 1.92 -2 4 -3 82.89 1.57 -2 4 -3 66.43 1.60 -2 4 -5 55.42 1.65 -2 4 -6 5.08 1.05 -2 4 -7 113.14 2.15 -2 4 -8 57.08 1.85 -2 4 -9 6.20 1.27 -2 4 -10 53.86 2.04 -2 4 -11 -0.30 1.37 -2 4 -12 22.96 2.05 -2 4 -13 0.07 1.56 -2 3 15 25.57 2.11 -2 3 14 43.04 2.15 -2 3 13 23.81 1.96 -2 3 12 63.77 2.01 -2 3 10 149.29 2.36 -2 3 9 18.68 1.23 -2 3 9 18.38 1.52 -2 3 8 144.19 1.76 -2 3 8 127.97 2.02 -2 3 7 23.79 1.10 -2 3 7 20.54 1.35 -2 3 6 129.50 1.60 -2 3 6 115.75 1.83 -2 3 5 41.11 1.10 -2 3 5 35.26 1.28 -2 3 4 102.44 1.37 -2 3 4 87.37 1.48 -2 3 3 241.17 2.04 -2 3 3 221.87 2.16 -2 3 2 175.80 1.72 -2 3 2 157.29 1.80 -2 3 1 96.97 1.36 -2 3 1 70.21 1.32 -2 3 0 447.86 3.17 -2 3 0 347.35 2.69 -2 3 -1 43.30 1.15 -2 3 -1 35.32 1.12 -2 3 -2 57.77 1.28 -2 3 -2 41.12 1.17 -2 3 -4 2.91 0.73 -2 3 -5 81.55 1.58 -2 3 -6 63.31 1.54 -2 3 -7 26.97 1.43 -2 3 -8 26.71 1.50 -2 3 -9 52.23 1.73 -2 3 -10 -0.36 1.09 -2 3 -11 64.34 2.03 -2 3 -12 0.90 1.32 -2 3 -13 41.98 2.21 -2 3 -14 1.87 1.54 -2 2 16 9.70 1.59 -2 2 15 24.64 2.06 -2 2 14 20.87 1.91 -2 2 13 99.00 2.29 -2 2 12 38.00 1.75 -2 2 11 107.27 2.09 -2 2 10 16.77 1.47 -2 2 9 83.61 1.54 -2 2 9 81.99 1.69 -2 2 8 15.14 1.08 -2 2 8 14.41 1.28 -2 2 7 115.49 1.53 -2 2 7 96.95 1.57 -2 2 6 0.39 0.53 -2 2 6 0.84 0.58 -2 2 5 279.56 2.23 -2 2 5 228.37 2.12 -2 2 4 49.29 0.98 -2 2 4 40.09 1.09 -2 2 3 369.06 2.61 -2 2 3 319.51 2.43 -2 2 2 73.88 1.06 -2 2 2 60.20 1.05 -2 2 1 136.48 1.39 -2 2 1 86.96 1.14 -2 2 0 183.95 1.68 -2 2 0 138.08 1.39 -2 2 -1 375.69 2.71 -2 2 -1 259.70 2.03 -2 2 -2 178.62 1.72 -2 2 -3 159.56 1.63 -2 2 -4 72.66 1.24 -2 2 -5 92.58 1.42 -2 2 -6 45.46 1.29 -2 2 -7 54.68 1.43 -2 2 -8 150.62 2.06 -2 2 -9 5.50 0.94 -2 2 -10 65.56 1.78 -2 2 -11 0.02 1.04 -2 2 -12 51.65 1.91 -2 2 -13 0.69 1.28 -2 2 -14 42.26 2.10 -2 2 -15 7.98 1.60 -2 1 16 30.70 2.20 -2 1 15 5.02 1.45 -2 1 14 120.20 2.46 -2 1 13 1.60 1.11 -2 1 12 105.85 2.09 -2 1 11 19.79 1.48 -2 1 10 146.26 2.16 -2 1 9 6.69 0.81 -2 1 8 248.74 2.31 -2 1 8 234.38 2.38 -2 1 7 4.89 0.61 -2 1 7 4.16 0.59 -2 1 6 453.21 3.18 -2 1 6 353.38 2.73 -2 1 5 154.56 1.55 -2 1 5 126.58 1.45 -2 1 4 534.10 3.46 -2 1 4 407.08 2.82 -2 1 3 836.42 5.04 -2 1 3 667.12 4.13 -2 1 2 1055.54 6.20 -2 1 2 851.83 5.11 -2 1 1 95.20 1.06 -2 1 1 67.29 0.84 -2 1 0 951.64 5.65 -2 1 0 649.62 4.02 -2 1 -1 241.98 1.88 -2 1 -1 181.13 1.43 -2 1 -2 30.71 0.79 -2 1 -2 26.37 0.69 -2 1 -3 481.79 3.14 -2 1 -4 159.21 1.50 -2 1 -5 323.06 2.46 -2 1 -6 105.10 1.44 -2 1 -7 312.27 2.65 -2 1 -8 2.01 0.69 -2 1 -9 292.75 2.78 -2 1 -10 16.22 1.36 -2 1 -11 101.34 1.97 -2 1 -12 13.01 1.53 -2 1 -13 28.69 1.74 -2 1 -14 7.63 1.39 -2 1 -15 27.19 2.04 -2 1 -16 7.85 1.62 -2 0 15 81.05 2.40 -2 0 14 2.22 1.33 -2 0 13 97.50 2.22 -2 0 12 3.54 1.02 -2 0 11 47.39 1.65 -2 0 10 2.09 0.76 -2 0 9 149.82 1.97 -2 0 8 24.60 1.14 -2 0 8 23.32 1.12 -2 0 7 287.09 2.42 -2 0 7 259.47 2.30 -2 0 6 23.69 0.95 -2 0 6 20.47 0.90 -2 0 5 693.38 4.35 -2 0 5 557.94 3.63 -2 0 4 614.97 3.88 -2 0 4 432.61 2.88 -2 0 3 1037.43 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1 6 35.97 0.87 2 1 7 232.38 2.02 2 1 8 14.68 0.94 2 1 9 196.97 2.09 2 1 10 24.20 1.26 2 1 11 16.88 1.31 2 1 12 43.37 1.62 2 1 13 17.82 1.59 -2 -1 -15 36.68 2.29 -2 -1 -16 13.45 1.67 2 2 -16 9.22 1.64 2 2 -15 64.89 2.52 2 2 -14 0.05 1.46 2 2 -13 72.87 2.30 2 2 -12 11.85 1.27 2 2 -11 104.61 2.12 2 2 -10 3.55 0.93 2 2 -9 291.17 2.86 2 2 -8 154.03 1.99 2 2 -7 129.88 1.71 2 2 -6 327.88 2.62 2 2 -5 304.17 2.37 -2 -2 4 876.01 5.31 2 2 -4 775.98 4.74 -2 -2 3 577.39 3.66 2 2 -3 491.41 3.16 -2 -2 2 677.10 4.15 2 2 -2 576.86 3.60 -2 -2 1 26.70 0.59 2 2 -1 23.87 0.55 -2 -2 0 92.17 0.89 -2 -2 -1 131.76 1.09 2 2 1 126.37 1.05 -2 -2 -2 1065.34 6.66 2 2 2 961.11 5.88 -2 -2 -3 10.11 0.48 2 2 3 6.99 0.51 2 2 4 1361.55 7.85 2 2 5 23.60 0.79 2 2 6 210.97 1.85 2 2 7 18.72 0.93 2 2 8 357.90 2.85 2 2 9 93.56 1.50 2 2 10 150.10 1.99 2 2 11 9.02 0.90 2 2 12 31.69 1.53 2 2 13 16.65 1.53 2 2 14 13.94 1.30 2 2 15 59.25 2.19 2 2 16 14.18 1.52 2 3 -15 5.42 1.50 2 3 -14 48.89 2.14 2 3 -13 1.01 1.33 2 3 -12 6.11 1.27 2 3 -11 25.34 1.71 2 3 -10 107.94 2.04 2 3 -9 365.79 3.31 2 3 -8 162.47 2.12 2 3 -7 301.13 2.72 2 3 -6 96.13 1.50 2 3 -5 390.01 2.93 2 3 -4 65.36 1.13 2 3 -3 724.54 4.51 2 3 -2 30.99 0.82 -2 -3 1 120.36 1.14 2 3 -1 119.03 1.21 -2 -3 0 169.44 1.34 2 3 0 161.58 1.41 2 3 1 145.90 1.29 2 3 2 7.76 0.63 2 3 3 1185.50 6.90 2 3 4 36.48 0.88 2 3 5 1091.96 6.47 2 3 6 172.75 1.76 2 3 7 396.32 3.03 2 3 8 79.63 1.44 2 3 9 99.33 1.62 2 3 10 214.83 2.40 2 3 11 1.91 0.85 2 3 12 112.09 2.05 2 3 13 38.28 1.76 2 3 14 42.90 1.94 2 3 15 17.16 1.86 2 3 16 54.26 2.29 2 4 -15 16.86 1.88 2 4 -14 29.31 2.20 2 4 -13 6.69 1.45 2 4 -12 20.78 1.87 2 4 -11 14.84 1.78 2 4 -10 15.98 1.62 2 4 -9 40.53 1.73 2 4 -8 191.54 2.44 2 4 -7 8.19 0.88 2 4 -6 231.80 2.42 2 4 -5 86.95 1.53 2 4 -4 242.17 2.25 2 4 -3 1.20 0.56 2 4 -2 41.36 1.07 2 4 0 26.42 0.95 2 4 1 10.20 0.83 2 4 2 970.82 5.84 2 4 3 91.64 1.30 2 4 4 363.53 2.74 2 4 5 106.39 1.51 2 4 6 105.90 1.59 2 4 7 123.26 1.74 2 4 8 164.36 2.02 2 4 9 181.02 2.23 2 4 10 2.26 0.84 2 4 11 56.80 1.70 2 4 12 4.77 1.07 2 4 13 79.69 2.11 2 4 14 0.35 1.18 2 4 15 70.95 2.30 2 4 16 -0.11 1.41 2 5 -14 3.74 1.74 2 5 -13 1.23 1.55 2 5 -12 6.43 1.52 2 5 -11 78.93 2.24 2 5 -10 38.31 1.89 2 5 -9 106.83 2.18 2 5 -8 30.07 1.63 2 5 -7 30.99 1.61 2 5 -6 37.87 1.56 2 5 -5 139.75 2.00 2 5 -4 33.76 1.40 2 5 -3 157.29 1.97 2 5 -2 3.11 0.74 2 5 -1 98.40 1.62 2 5 0 53.25 1.33 2 5 1 483.30 3.49 2 5 3 690.41 4.60 2 5 4 131.54 1.82 2 5 5 106.18 1.73 2 5 6 83.22 1.68 2 5 7 20.55 1.36 2 5 8 51.29 1.57 2 5 9 10.69 1.02 2 5 10 122.84 2.15 2 5 11 0.97 1.02 2 5 12 45.54 1.87 2 5 13 16.84 1.87 2 5 14 37.15 2.09 2 5 15 -0.14 1.38 2 6 -13 9.20 1.82 2 6 -12 14.83 1.77 2 6 -11 17.18 2.15 2 6 -10 70.66 2.35 2 6 -9 20.21 1.95 2 6 -8 185.34 2.72 2 6 -7 0.23 1.12 2 6 -6 109.24 2.15 2 6 -5 0.74 1.00 2 6 -4 99.52 1.95 2 6 -3 7.19 0.99 2 6 -2 110.26 1.92 2 6 -1 49.11 1.59 2 6 0 273.11 2.73 2 6 1 68.25 1.65 2 6 2 462.99 3.68 2 6 3 213.22 2.42 2 6 4 102.32 1.92 2 6 5 104.57 1.96 2 6 6 20.63 1.59 2 6 7 101.69 2.07 2 6 8 1.97 1.06 2 6 9 111.36 2.19 2 6 10 2.04 1.13 2 6 11 58.65 1.99 2 6 12 4.32 1.31 2 6 13 74.19 2.33 2 6 14 2.44 1.43 2 6 15 35.82 2.35 2 7 -11 43.74 2.47 2 7 -10 2.62 1.66 2 7 -9 43.64 2.27 2 7 -8 0.35 1.45 2 7 -7 80.31 2.25 2 7 -6 4.55 1.36 2 7 -5 68.67 2.07 2 7 -4 26.26 1.75 2 7 -3 20.16 1.81 2 7 -2 108.98 2.27 2 7 -1 68.03 2.00 2 7 0 88.00 1.98 2 7 1 142.29 2.27 2 7 2 29.52 1.70 2 7 3 33.20 1.69 2 7 4 114.63 2.15 2 7 5 0.02 1.18 2 7 6 109.99 2.24 2 7 7 1.11 1.26 2 7 8 60.63 2.10 2 7 9 -0.78 1.33 2 7 10 68.31 2.33 2 7 11 2.32 1.41 2 7 12 36.88 2.17 2 7 13 -0.51 1.49 2 8 -9 0.92 1.81 2 8 -8 32.15 2.37 2 8 -7 3.04 1.56 2 8 -6 9.46 1.64 2 8 -5 5.50 1.53 2 8 -4 32.39 2.13 2 8 -3 19.70 2.07 2 8 -2 31.67 2.05 2 8 -1 51.88 2.06 2 8 0 19.02 1.87 2 8 1 56.30 2.11 2 8 2 28.82 1.91 2 8 3 24.33 1.97 2 8 4 5.63 1.50 2 8 5 9.44 1.53 2 8 6 1.99 1.50 2 8 7 51.13 2.22 2 8 8 2.51 1.56 2 8 9 69.50 2.47 2 8 10 -0.82 1.65 2 8 11 38.20 2.46 2 8 12 -0.08 1.56 2 9 -7 19.73 2.21 2 9 -6 6.48 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